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Glass ceramics with α cordierite(2MgO·2Al 2O 3·5SiO 2) as main crystal phase, having excellent dielectric property, are perfect materials for microwave parts of a medium apparatus However, the thermal expansion coefficient of the material is not high enough for some special applications Now, a novel glass ceramics with suitable thermal expansion coefficient (47 7×10 -7 / C) and excellent dielectric property (ε=5 1,tgδ0 -3 ) was developed Crystallization process and the th...

本文以堇青石微晶玻璃为研究对象,首次研制得到了一种低介(ε= 51)、低损耗(tgδ<10- 3)、热膨胀系数(46 ~48 ×10- 7' C)能与其它器件相匹配的新型微晶玻璃介质材料通过 X射线衍射分析,扫描电镜观察等测试手段,研究了该材料的晶化过程和热膨胀系数的变化规律发现样品的热膨胀系数随温度的变化行为是与样品中析出的晶相种类及析出量随温度的变化规律相对应的

The phase transition temperature increases and the transition ranges tends to be broad when PNIPA brushes were substituted with P or P(NIPA-co-NVP) brushes obtained by the copolymerization of NIPA with AA and NVP, respectively. However, the phase transition is not obvious if adding excessive hydrophilic comonomer.

结果表明,纯PNIPA刷的相变温度在29℃~33℃之间,通过共聚所得的单一P或P(NIPA-co-NVP)刷均使相转变温度提高,转变区域拓宽,当亲水性共单体的量过多时会导致相变过程不明显。

It separates the network into symmetrical parts and unsymmetrical parts,synthetically uses sequence compo nents an d phase components.In the sequence domain,it equals the symmetrical parts to its boundary nod es;in the phase domain,with the po lym orphic calculationtechnique,it deals wi th all kinds of faults directly without huge calculating work as it is in the conventional phase compo nents methood.The example shows the advantages of this improved method.

该方法以相分量故障处理方法为依据,在序坐标下化简对称部分,等效到其边界节点,在相坐标下对化简后的网络处理各种简单和复杂故障,采用多态计算技术,以矩阵变换代替传统的数值方程的计算,避免了相分量法计算量大的缺点。

Furthermore, the experimental k values were used to determine the associated activation energy, Ea, for the formation of La2/3TiO3-type phase using the Arrhenius plot and the following least-square equation, ln =-Ea/RT + A, where T is the annealing temperature, R is the universal gas constant, and A is a constant, resulting in Ea ~ 607 ?

第二部分则是以微观的方式来解析Pb2+离子与La4Ti9O24陶瓷以及La2/3TiO3-type相晶格之间的关系;利用化学共沉法来合成不同Pb2+离子添加量的La4Ti9O24陶瓷起始粉体,再以900 oC /1h的条件热处理;藉由选区电子绕射图谱以及X-ray绕射分析所生成之La2/3TiO3-type相结构;结果显示La2/3TiO3-type相之结晶结构为斜方晶之钙钛矿结构,符合空间群IbmmNo。

In this paper, according to the equation of voltage vector of single-phase motor operating at symmetrical condition, author presents a new voltage-vector PWM method of variable frequency control for single-phase motor. In system, the voltage vector is used as a control parameter.

本文根据单相电动机对称运行时的合成电压矢量方程,提出了以合成电压矢量为控制量的单相电动机电压矢量式PWM变频调速控制方法,并进行了计算机仿真及制作了单相变频器。

The chemical structure of the product was characterized by means of the melting point and IR. The results show that tetraethylammonium bromide which was used as a phase transfer catalyst in this reaction had optimization effect on the interfacial diffusive reaction of BTC and PNP. Higher concentration of sodium hydroxide, lower temperature and a higher dosage of BTC produced a small amount of 4-nitrophenyl chloroformate, while lower concentration of sodium hydroxide and a lower dosage of BTC made reaction incomplete, which affected the yield.

结果表明,在碳酸二(4-硝基苯基)酯合成中使用的相转移催化剂四乙基溴化铵对受界面扩散控制的BTC气与对硝基酚钠反应有良好的相转移催化效果;氢氧化钠质量分数较低时,酚钠盐向溶有BTC的油相扩散速度较小,较高时会产生氯甲酸对硝基苯酯;温度较低、BTC量较高时,会产生少量氯甲酸对硝基苯酯,BTC用量较低会使反应不完全,这些都影响着收率。

According to the improved J-H algorithm of ICA which based on higher order statistics, the reliability of the method was conformed using given modulate signals and different fluid flow of monophase of oil, gas and water response signals to emulate tow-phase and three-phase mixed up signal sources.

根据基于高阶统计量的改进J-H ICA求解算法,利用给定仿真信号及不同流量油、气、水单相流体响应信号,模拟两相、三相混合信源进行分离实验,验证该方法的可靠性,并对生产井实测气液两相流体多路传感器响应信号进行分离。

Differential scanning calorimetry and polarizing microscope were used to study their liquid properties. Among them, nine are found to exhibit liquid crystal properties, and most of them displayed as heating monotropic liquid crystals. There are one or two mesophases and certain phase transition temperature,Δ H and temperature range of liquid crystal.

用差示扫描量热仪和偏光显微镜研究了其液晶性,发现其中九个配合物具有液晶性,多为升温单变液晶,有一至两个中介相,有确定的相转变温度、热焓和相变区间。

2Before the addition of Ni-Ti alloy, hard phase was nearly spherical shape; the shape of hard phase became multiangular with the increasing of Ni-Ti alloy, the interface between hard phase and binder phase presented line.

2未加Ni-Ti合金以前,陶瓷相多为球形;而随着Ni-Ti合金加入量的增多,Ti基金属陶瓷中出现了多边形的陶瓷相,陶瓷相与粘结相的界面呈现直线关系。

Oxygen was found to depress their fcc-sctransition temperature Tc from the normal value of 260K,as indicated by theminimum in the temperature-dependent permittivity ε′,and also enlarge the drop in ε′at the transition.The magnitudes of the downward shift in Tc and the drop in ε′were roughly proportional to the O2 occupance at octahedral lattice sites,as estimatedfrom the resonance heights distribution.

发现氧的存在降低了以介电常数ε'温度谱极小值为标志的有序无序相变温Tc(正常相变温度为260K),并且增大了ε'在相变前后的变化幅度,Tc的下降值和ε'的变化量Δε'近似比例于八面体位置氧的占据率,氧的占据率可以从核磁共振峰高的分布获得。

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