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The results showed that the four stereoisomers of soman were well separated under the defined chromatographic conditions. CP-)soman was only detected stereoisomer in the intoxicated rabbit blood and eliminated rapidly, the toxicokinetics could be described by a two-compartment model after rabbits received soman via vein.

结果可见梭曼4个异构体在确定的气相色谱条件下得到了较好地分离;给兔iv梭曼43.2 μg·kg-1后,血中仅测到一对CP梭曼,其消除过程符合二室开放模型, V d=2.1 L·kg-1, t 1/2α=4.5 s, t 1/2β=72 s, AUC(15~300 s)=2.08 mg·s·L-1, CL =21 mL·kg-1·s-1,血中CP梭曼在血中消除过程反映了机体对梭曼毒性异构体的解毒过程。

Secondly, comparative experiments were carried out in different phase regions to probe the influence of pressure and the phase behavior of the mixed solvents on the tautomerism.

将紫外光谱及热力学方法相结合,测定了CO〓+乙醇、CO〓+正戊烷混合流体中EAA的异构化平衡常数,研究了超临界区、临界区和亚临界区EAA的异构化平衡常数随压力等因素的变化规律。

The hybrid composite PW11Co/PAMAM was characterized by FT-IR, UV-Vis diffuse reflectance spectra, XPS, XRD and TG/DTA, indicating that the PW11Co was chemically anchored to PAMAM. The morphologies of the title composite were characterized by scanning electron microscopy and transmission electron microscopy. The catalytic activity was evaluated by oxidation of isobutyraldehyde to isobutyric acid in MeCN under mild conditions (20 ℃, ambient pressure), showing that the title compound is a more effective and recoverable catalyst than corresponding PW11Co.

通过FT-IR、DR-UV-Vis、XRD、TEM、SEM、TG/DTA等手段对其进行了表征,并考察了其对异丁醛转化异丁酸的催化活性,实验结果表明,多金属氧酸盐通过配位键与聚酰胺-胺作用形成的无机-有机复合物可望成为一种催化活性高且易于分离和重复使用的多相催化剂。

In this paper, quantum chemistry methods were used to investigate themicrocosmic reaction mechanisms and dynamics of a series of activatenitrogen-, sulfur- and halogen-containing radicals and some smallmolecules in the gas phase theoretically, including isocyanic acid,isothiocyanic acid and ketenyl radical.

本研究论文是采用量子化学理论和计算方法,对异氰酸 HNCO、异硫氰酸 HNCS 及其自由基、乙烯酮自由基 HCCO 与若干气相含氮、硫、卤素的活性小分子自由基反应的微观反应动力学进行理论计算研究。

In this paper, quantum chemistry methods were used to investigate the microcosmic reaction mechanisms and dynamics of a series of activate nitrogen-, sulfur-and halogen-containing radicals and some small molecules in the gas phase theoretically, including isocyanic acid , isothiocyanic acid and ketenyl radical .

本研究论文是采用量子化学理论和计算方法,对异氰酸HNCO、异硫氰酸HNCS及其自由基、乙烯酮自由基HCCO与若干气相含氮、硫、卤素的活性小分子自由基反应的微观反应动力学进行理论计算研究。

Firstly by using volume exclusion chromatography and cation exchange column,sugar molecular-weight distribution and the contents of monosaccharide, disaccharide andtrisaccharide in rice wine were determined. And then by using amino-bonding phasecolumn,the contents of three functional oligosaccharide (isomaltose, panose, isomaltotriose)in shaoxing rice wine of different years and different processes were determined andstudied.

在应用体积排阻色谱柱和钙型阳离子交换柱测定了黄酒样中糖分的分子量分布和单、双、三糖含量的基础上,利用氨基键合相柱对不同年份和不同工艺的绍兴黄酒样中异麦芽糖、潘糖、异麦芽三糖三种功能性低聚糖进行了定量分析研究。

The main lithofacies feature of East Part rockbody contains large plagioclase,while there locally exists little(or doesn\'t exist) plagioclase-bearing lherzolite in the West Part rockbody.

东段岩体以出现大量的含斜长石岩相为主要特征,西段岩体以不出现或只局部出现斜长二辉橄榄岩异离体与东段岩体相区别。

Adduct G is isomerized by F. The isomerization energies are relatively high (in the gas phase: 244.77 kJ/mol; in solvent of water: 234.83 kJ/mol), which is consistent with the experiment that adduct F is the primary alkylation product.

加合物G由F异构形成,且有相对高的异构化能(气相:244.77 kJ/mol;水溶剂中:234.83 kJ/mol),这与实验上得到加合物G是主要癌变物的结果一致。

In order to escplore the new models of cultivating in school, the essay tightly connects cultivating with teaching and research activities, based on developing teachers vacational level by modern information technoledge. Besides, during the process of founding the system of trainning teachers in school, we decide on our cultive target—promote the element educational reform by school internet, combing the facts of different schools. The cultive contnet should suit measures to different conditions, trying to synthesise and stress its practical function. When carrying out the cultive plan, we should sum up different models and explain its essence, steps and function so that we make the best choice. As to evaluational methods, we can take varied evaluational ways, including self-evaluation and evaluating each other by combination of fixing quality and quantity. At last, it is very necessary to found a special organization in order to form cultive web, make entire standarization, pay attention to develop resource and provide cultive guarantee.

本文在构建网络环境下中小学教师校本培训体系时,把以教师专业发展为本,以学校为主要研究基地,以现代信息技术为手段,以新课程的学习和实施为抓手,把培训和教研活动紧密结合、溶为一体,探索校本培训的新模式作为目标;把以基础教育新课程改革为出发点,在总目标的框架下,结合学校的具体实际,以校园网络为依托,来确定相应的培训任务,以促进基础教育课程改革的顺利进行作为任务;培训内容因人而异、因校而异,力求综合化,强调实用性与实践性;就相关的网络环境下校本培训模式进行了归纳整理,就每种模式的基本内涵、实施步骤加以说明,并对其功能列表进行比较,以便使用时更好地选择;运用多元评价和多样化评价方式,采取定性和定量相结合、自评和互评相结合、学校整体和教师个人发展相结合等灵活多样的评价方法,认真地进行科学的全方位的评价;建立一个专门的机构进行组织与管理:建立组织机构,形成培训网络,进行整体规划,优化培训机制,注重资源开发,提供培训保障。

The dehydrogenation of vapor phase methyl isobutyl carbinol to produce methyl isobutyl ketone over a CuO-ZnO-Al2O3 catalyst prepared by co-precipitation method under the atmospheric pressure was studied.

采用共沉淀法制备的铜系CuO/ZnO/Al_2O_3脱氢催化剂,在常压下进行了甲基异丁基甲醇的气相脱氢制备甲基异丁基酮的反应实验。

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The split between the two groups can hardly be papered over.

这两个团体间的分歧难以掩饰。

This approach not only encourages a greater number of responses, but minimizes the likelihood of stale groupthink.

这种做法不仅鼓励了更多的反应,而且减少跟风的可能性。

The new PS20 solar power tower collected sunlight through mirrors known as "heliostats" to produce steam that is converted into electricity by a turbine in Sanlucar la Mayor, Spain, Wednesday.

聚光:照片上是建在西班牙桑路卡拉马尤城的一座新型PS20塔式太阳能电站。被称为&日光反射装置&的镜子将太阳光反射到主塔,然后用聚集的热量产生蒸汽进而通过涡轮机转化为电力