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The effect of reaction temperature,reaction time,materials ratio on the synthesis of piperidine alcohol benzoate ,hindered amine light stabilizer,from piperidine alcohol and benzoyl chloride by direct condensation were studied,and the proper technological conditions were given as follows:the reaction temperature is 95℃;reaction time is 4 h; the mole ratio of reactants,n∶n is 1∶1.4,the amounts of solvent is 40 mL(based 0.1mol piperidine alcohol),the arerage yield ...

王树清,高崇,苯甲酸哌啶醇酯HALS的合成工艺研究研究了以苯甲酰氯和哌啶醇为原料直接缩合合成苯甲酸哌啶醇酯受阻胺光稳定剂时反应温度、反应时间、原料配比等条件对合成反应的影响,确定了最佳工艺条件。最适宜的工艺条件是:反应温度95℃、反应时间6h、原料摩尔比n∶n为1∶1.4,溶剂用量为70mL(相对于0.1mol哌啶醇),苯甲酸哌啶醇酯的收率为91.05%,产品纯度98.5%。

In other cases, the detection results of the WLE chart and the WLC chart have narrow difference, but the implementation and computation of the WLE chart is comparatively simpler.

通过与WLC图的比较,可以看出WLE图在均值和方差漂移比较小时要优于WLC图,其他情况下的检测效果与WLC图相差不大,而且操作相对于WLC图要更简便,计算要更简洁。

The results show that the difference between upper magnitude threshold Mt used in the calculation and the maximum magnitude extrapolated from the linear relation of log N-M has an influence on the distribution of Y.

结果表明,计算样本的震级上限Mt 相对于logN-M关系中拟合线性外推最大震级MT的变化对Y的异常分布有一定影响,其影响随地震样本量从小到大而明显减小。

Compared to MA, BSAP has the following advantages: cancels the open operation of MA and adds the traffic operation primitive between ambients and their sub- ambients; adds operation and adds password to operation; adds the operation primitive of ambient reclamation.

相对于MA,BSAP做了如下几点改进:1、取消了MA中的操作,增加了父子环境间的通信操作原语;2、增加了操作,并在操作中加入了密码;3、增加了环境回收操作原语。

Interaction between processes, and the scope and details of any exclusions to

质量手册,包括所涉及的程序、程序间相互关系的描述以及相对于ISO9

That was compared to an approval rate of fifty-five percent in May.

这是相对于5月份的55﹪的支持率来说的。

The result show that the position of free surface is higher because of frusta of brake, especial obvious in the head of frusta of brake; flux coefficient and pressure on dam are quite influenced by type of frusta and 3 A type frusta of brake relative to 2 type frusta of brake has bigger flux coefficient and smaller pressure on dam; Obvious influence of ability of discharge flow for different ratio of thickness of frusta and breadth of brake and pressure on dam reduces with increasing ration of thickness of frusta and breadth of brake, while bigger flux coefficient is obtained when tlb = 0.2.(7)The 3D free surface turbulent model established in the paper is comparatively well and truly simulates 3D flow over spillway with frusta of brake and series waterpower computation can be completed aim at different type of dam, type of frusta and disposal on the dam and different water height on peak of

结果表明,闸墩河海大学博士论文的存在抬高了水面线的位置,其中在闸墩头部尤其明显;墩型对流量系数和坝面压力影响较大,3A型闸墩相对于2型闸墩具有更大的流量系数和更小的坝面压力:不同的墩厚闸宽比t/b对泄流能力也将产生显著的影响,随着墩厚闸宽比的增加,坝面压力降低,而当t/b二0.2时溢流坝具有更大的流量系数。7本文建立的三维自由面湍流场模型能够比较准确地模拟带闸墩溢流坝三维过坝水流湍流场,可以针对不同的坝型、墩型、坝面布置形式以及不同的坝顶水头完成系列水力计算,为泄水工程建筑物的设计提供可靠的分析依据

The ionization constant of H2CO3 is much higher than that of H2S in the solution , whereas the mole of CO2 is much lower than that of H2S in the sour gas of Feixianguan Formation.

在溶液中碳酸的电离常数大大高于氢硫酸,飞仙关组高含硫气藏天然气组分中的CO2相对于H2S的质量亏损和储层中有富轻碳的高温方解石充填晚期溶孔、裂缝表明储层中的晚期溶解作用是由硫酸盐热还原过程中生成的CO2引起的。

It is most likely that only a part of the karst caves could be detected if the boundary of the karsts cave has a certain horizontal extension respectively to measurement layout, but the interface of the karsts caves is not completely smooth plane, and its normal direction is not perpendicular to the tunnel axis.

如果溶洞的边界相对于TSP测量布线有一定的横向延伸性,其边界面不一定是完全平滑的表面,但其法线方向与隧道轴线不完全垂直,这类溶洞有可能被部分探测,但探测精度还与溶洞界面两侧的波阻抗差、对地下水的探测、操作人员的数据采集经验和数据处理水平等有关。

It is most likely that only a part of the karst caves could be detected if the boundary of the karsts cave has a certain horizontal extension respectively to measurement layout, but the interface of the karsts caves is not completely smooth plane, and its normal direction is not perpendicular to the tunnel axis. However, the precision of the cave detection is related to interface wave impedance difference of the karst caves, groundwater detection, operator's data acquisition experience and data processing level and so on.

如果溶洞的边界相对于TSP测量布线有一定的横向延伸性,其边界面不一定是完全平滑的表面,但其法线方向与隧道轴线不完全垂直,这类溶洞有可能被部分探测,但探测精度还与溶洞界面两侧的波阻抗差、对地下水的探测、操作人员的数据采集经验和数据处理水平等有关。

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Neither the killing of Mr Zarqawi nor any breakthrough on the political front will stop the insurgency and the fratricidal murders in their tracks.

在对危险的南部地区访问时,他斥责什叶派民兵领导人对中央集权的挑衅行为。

In fact,I've got him on the satellite mobile right now.

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The enrich the peopling of Deng Xiaoping of century great person thought, it is the main component in system of theory of Deng Xiaoping economy, it is a when our country economy builds basic task important facet.

世纪伟人邓小平的富民思想,是邓小平经济理论体系中的重要组成部分,是我国经济建设根本任务的一个重要方面。