盐酸盐

Keywords amino acid methyl ester hydrochloride;amino acids;methanol solution of thionyl chloride;thionyl chloride;synthesis

氨基酸甲酯盐酸盐；氨基酸；二氯亚砜-甲醇溶液；二氯亚砜；合成

The influentical factors on the synthesis of L-serine methyl ester hydrochloride with thionyl chloride were studied and optimized.

对亚硫酰氯法制备L-丝氨酸甲酯盐酸盐的影响因素进行试验及优化，较佳工艺条件下酯化收率可达85.0%以上，产品含量≥98.0%。

Results show that, by using thionyl chloride and N,N-dimethyl formamide as chlorinating reagent and dichloromethane as solvent and taking -15℃ as reaction temperature, Z-iomer crystals with pale white color and stable to temperature can be obtained with an overall yield of 70%.

以2-（2-氨基噻唑－4-基）－2-甲氧亚氨基乙酸为原料，经盐酸化、氯代等反应合成了Z-2-（2-氨基噻唑－4-基）－2-甲氧亚氨基乙酰氯盐酸盐；氯代时以用亚硫酰氯和N，N-二甲基甲酰胺的混合物代替五氯化磷作氯化剂，并考察了温度和溶剂对氯代产物中Z-异构体和E-异构体收率的影响。

It is very improtant to cut down the production costs of AKD by means of recycle triethylamine of from by－product triethylaminehydrochloride.

摘 要：从副产物三乙胺盐酸盐中回收三乙胺对降低AKD生产成本至关重要。

With 1-methylte-trazole-5-thiol and 7-ACA as the material and acetonitrile-boron trifluoride complex as Catalysts, 7-TMCAHCl was preparated and the yield could reach 91.80%.

以1-甲基－5-巯基四氮唑和7-ACA为原料，三氟化硼乙腈配合物为催化剂合成了7-TMCA盐酸盐，反应收率可达91.80%。

Chloro-2-hydroxypropyl trimethylammonium chloride was synthesized by using trimethylamine hydrochloride and epichlorohydrin as the raw materials and anhydrous as solvent.

以无水乙醇作溶剂、三甲胺盐酸盐和环氧氯丙烷为原料合成了3-氯-2-羟丙基三甲基氯化铵，探索出最佳合成条件为：n∶n为0.95∶1，反应温度为40~50℃，反应时间为30m in，所得产品质量分数大于98%，收率达90%。

Yoo and Li communicated the successful oxidative amidation of aldehydes with amine hydrochloride salts and Cu/Ag catalysts J.

柳、李沟通成功的醛胺氧化酰胺盐酸盐、铜/银催化剂 J时。

A new nonaqueous titration method for the determination of aminocaproic acid and aminocaproic acid hydrochloride was established, for technology-controlling of nylon 6 waste recycling by HCl de-polymerization.

本文针对盐酸酸解尼龙-6废弃物回收6-氨基己酸单体的工艺控制问题，首次建立了非水滴定法测定中间体6-氨基己酸盐酸盐及终产品6-氨基己酸含量的分析方法。

Nonaqueous titration;Aminocaproic acid;Hydrochloride;Hyperehloric acid-acetic acid;Potentiometric titration

非水滴定；6-氨基己酸；6-氨基己酸盐酸盐；冰乙酸-高氯酸；电位滴定

Amino-6-methoxy Benzothiazole 99%、2-Amino Benzothiazole 99%、Veratraldehyde 99%、Veratric Acid 99%、1,2- Dimethoxy Benzene 99%、6-Nitroveratric Acid 97%、2,5-Dichlorobenzoic Acid 99%、4-Chloro-3-Nitrobenzoic Acid 99%、 3-Nitrobenzole Acid 98%、p-Methoxybenzoie Acid 99%、Anisole 99.5%、p-Methoxyacetophenonc 99%、(2'-Chloroethyl) Benzene 99%、(2'-Bromoethyl) Benzene 99%、N,N-Diethyi-m-Toiuamide 99%、Aminoacetonitrile Hydrochloride 98%、 Alkyl Diphenyl Phosphate Estrel 98%、5-Chloro-2-benzothiazolone 99%、6-bromo-2-naphthol 98%、6-Nitro-Veretric Acid Estrel 97%、4-chloro phenoxyaeetic 99

2-氨基-6-甲氧基苯骈噻唑、2-氨基苯骈噻唑、藜芦醛、藜芦酸、藜芦醚、6-硝基藜芦酸、2，5-二氯苯甲酸、3-硝基-4-氯苯甲酸、3-硝基苯甲酸、对甲氧基苯甲酸、苯甲醚、对甲氧基苯乙酮、β-氯代苯乙烷、β-溴代苯乙烷、N，N-二乙基间甲苯甲酰胺、氨基乙腈盐酸盐、磷酸二苯月桂酯、5-氯-2-苯骈噻唑酮、6-溴-2-萘酚、6-硝基藜芦酸甲酯、4-氯苯氧乙酸

Breath, muscle contraction of the buttocks; arch body, as far as possible to hold his head, right leg straight towards the ceiling (peg-leg knee in order to avoid muscle tension).

呼气，收缩臀部肌肉；拱起身体，尽量抬起头来，右腿伸直朝向天花板（膝微屈，以避免肌肉紧张）。

The cost of moving grain food products was unchanged from May, but year over year are up 8%.

粮食产品的运输费用与5月份相比没有变化，但却比去年同期高8％。