盐酸化的

2 The analysis step by 25.0mL sample lixivium, moved in the direction of arsenic in the bottle, plus 10 ml of hydrochloric acid and 10 ml of potassium iodide solution and 5 drop acid stannochlor solution, shake the place 10min, together with 2 g of arsenic-free zinc metal, immediately mounted a good lead acetate paper turns red cotton and mercury bromide from log that arsenic tube placed in the 25-38, f μh of the dark side, remove the test strip and standard mercury bromide a color not deeper than standard.

7.2 分析步骤取25.0mL样品浸泡液，移入测砷瓶中，加5mL盐酸、5mL碘化钾溶液及5滴酸性氯化亚锡溶液，摇匀后放置10min，加2g无砷金属锌，立即将已装好乙酸铅棉花及溴化汞试纸的测砷管装上，放置于25～30℃的暗处1h，取出溴化汞试纸和标准比较，其色斑不得深于标准。

Use nitrite and the Sulfanilic acid diazotization in acidic conditions,with dinitroaniline coupling formation color reaction,established the method of using the color reaction Determination Chinese cabbage s Nitrite content.

在酸性条件下亚硝酸盐与对氨基苯磺酸重氮化后，再与盐酸萘乙二胺偶合形成颜色反应，建立了用比色法测定大白菜中亚硝酸盐的方法。

The results show that the compound conductive fiber has typical structure of sheath-core consists of black greened polyaniline electric conductive deposition as the skin and the white polypropylene matrix fiber as the core, which makes the compound fiber preferable physical mechanical property. The intensity and the elongation ratio of the electric conductive fiber are decreased but the thermal stability is enhanced after modified. The compound fiber has the good acid resistance but poor base resistance. The thermal stability of the compound fiber prepared by 4-methyl-benzene sulfonic acid is better than that prepared by hydrochloride acid. Moreover, the compound fiber can be re-doped by other organic or inorganic acid after freed from the adsorbed acid. Furthermore, the electric conductivity of the compound fiber decreases with the temperature increasing but hardly changed with the humidity. The adsorptive ability and therefore the content of the polyaniline, the constant of electric conduction, and the durability of the compound fiber can be enhanced by thinning the diameter, section heteromorphosis, section heteromorphosis and plasma treatment of the surface or blending with COPET of the fiber.

结果表明：复合纤维是聚丙烯与聚苯胺的共混体系，具有典型的皮芯型结构，皮层为墨绿色的聚苯胺沉积层，形成连续的导电通道，芯层为白色的聚丙烯基质纤维，提供物理机械性能；导电改性后纤维的强度、强力和伸长率均有下降，但热稳定性得到提高；复合纤维的耐酸性比耐碱性好，以对甲苯磺酸做掺杂酸比盐酸掺杂聚苯胺热稳定性好，脱掺杂后的复合纤维，可用其它无机酸或有机酸进行再掺杂；复合导电纤维的电导率随温度升高降低幅度较大，但几乎不受湿度影响；基质纤维细旦化、截面异形化、表面等离子体处理或共混COPET等改性处理均能提高纤维的吸附性，进而提高复合纤维表面聚苯胺含量、电导率和耐久性。

Results The best experimental conditions for the new method were as follows: hydrochloric acid concentration 5%; sodium borohydride solution, potassium bromate and potassium bromide solution, 2ml each; flow rate 0.6L/min.

结果］本法的最佳实验条件为盐酸溶液浓度5%，硼氢化钠溶液和澳化剂的用量各为2ml，载气流量0.6L/min。

Objective To observe the clinical efficiency of Terbinafine and Traditional Medicine Solution Compound in Treating Keratotic Tinea Pedis.

目的观察盐酸特比萘芬口服联合中药复方透骨草浸泡治疗角化过度型足癣的临床疗效。

A new production technology,using witherite,hydrochloric acid and industrial refined salt as raw materials,to produce liquid barium chloride with low strontium by crystallization method was put forward.

比较了氯化钡的各种生产方法，提出了以毒重石、盐酸和工业精制盐为原料，结晶法生产液体低锶氯化钡新工艺，并对酸化反应、锶钡分离原理、饱和盐水洗涤及母液处理进行了分析和讨论。

Seven 1-phenyl-(4-pyridinyl)acetylene derivatives were conveniently synthesized in this paper using corresponding styrylpyridines as starting materials by bromination, rearrangement and debromination.

本文采用简单易行的方法从苯乙烯基吡啶类衍生物通过溴化、重排和脱溴化反应合成了7种苯乙炔基吡啶类单体，研究了它们在1mol/L盐酸水溶液中的光环加成反应。

The graft polymerization of acrylonitrile on Crosslinked polyvinyl alcohol microspheres CPVA microspheres was performed by using cerium ammonium sulfate as initiator, and grafted microspheres CPVA-g-PAN were prepared. Subsequently, the grafted PAN was converted into poly via amidoximation reaction with hydroxylamine hydrochloride as reagent, resulting in the functional microspheres CPVA-g-PAO. The chemical structure and physicochemistry characters were adequately characterized with infrared spectrum, scanning electron microscope and determining Zeta potential. The effects of main factors on the amidoximation transform reaction of the grafted PAN were researched with emphasis, and the adsorption property of the functional microspheres CPVA-g-PAO for some biomolecules was examined preliminarily with uric acid as a model biomolecule.

以硫酸铈铵为引发剂，实施了丙烯腈在交联聚乙烯醇微球表面的接枝聚合，制备了接枝微球CPVA-g-PAN，然后以盐酸羟胺为试剂，通过偕胺肟化转变，将接枝的PAN转变为聚偕胺肟，制得了接枝有聚偕胺肟的功能微球CPVA-g-PAO，采用红外光谱法、扫描电子显微镜及Zeta电位测定等法，对功能微球CPVA-g-PAO的化学结构及物理化学特性进行了表征，重点考察了各主要因素对接枝PAN的偕胺肟化转变反应的影响，也以脲酸为模型分子，初探了功能微球CPVA-g-PAO对生物分子的吸附性能。

Treatment of the diacetoxy-calix [4] arene with a series of ditosylates in dry MeCN in the presence of NaOH resulted in formation of electron-rich calix [4] areneocrowns, which reacted with 4, 4'-bipyrindinium and p-bis -benzene at room temperature in dry MeCN to afford self-assembling [2] catenanes by π-π stacking interaction.

以杯[4]芳烃为原料，通过三氟乙酸铊将其氧化成醌，醌类化合物在Zn粉、冰醋酸、少量盐酸和过量的乙酸酐中反应得到双乙酰化产物，利用氢氧化钠使其水解，然后再与各种对甲苯磺酸二酯进行环化反应，得到一系列具有富电子空腔的杯[4]芳烃并冠醚。

Melting point 3410 ℃, boiling point 560 ℃, relative density of 1935, F the external electronic structure of 5d46s2, in the chemical reaction time is very easy to lose 1-6 electronic, but also can get 1-2 electronic, so oxidation number of 0,± 1,± 2, 3, 4 , 5 and 6, with 6 price of the most stable compounds, such as WO3 does not dissolve in water, the air will form in the tungsten trioxide thin protective layer of tungsten, tungsten with fluorine at room temperature, chemical combination, red hot when there is no moisture and Bromine iodide together, red hot when you can and water reaction WO3, at room temperature reaction of tungsten with aqua regia, but the hot concentrated hydrochloric acid and sulfuric acid can only be played with its weak response, but molten nitrate, nitrite, too Hydrogen peroxide, sulfur steam, steam and other phosphorus can play intense reaction, high temperature can not be carbon, boron and silicon reaction of binary compounds, widely used in industrial tungsten steel and tungsten carbide, pure tungsten filament is used to the system, and X-ray tube Tube heating components, semiconductor components can be prepared tungsten silicide, tungsten industrial production is white or black tungsten ore tungsten ore refining.

熔点3410℃，沸点560℃，相对密度1935，F外围电子结构为5d46s2，在化学反应时很容易丢掉1—6个电子，也能得到1—2个电子，所以氧化数为0、±1、±2、＋3、＋4、＋5和＋6，以＋6价化合物最稳定，如WO3不溶于水，空气中的钨会形成薄层三氧化钨保护层，钨能与氟在室温下化合，红热并无潮气时能与溴、碘化合，红热时还能和水反应生成WO3，室温下钨可与王水反应，但热的浓盐酸和硫酸只能与其起微弱反应，但对熔融的硝酸盐、亚硝酸盐、过氧化氢、硫蒸汽、磷蒸汽等能起激烈反应，高温下不能与碳、硼和硅反应生成二元化合物，工业上广泛使用钨钢和碳化钨，纯钨用来制灯丝、电子管和X射线管的发热元件，硅化钨可制半导体元件，钨工业生产是将白钨矿石或黑钨矿石精炼。

According to the clear water experiment, aeration performance of the new equipment is good with high total oxygen transfer coefficient and oxygen utilization ratio.

曝气设备的动力效率在叶轮转速为120rpm～150rpm时取得最大值，此时氧利用率和充氧能力也具有较高值。

The environmental stability of that world - including its crushing pressures and icy darkness - means that some of its most famous inhabitants have survived for eons as evolutionary throwbacks, their bodies undergoing little change.

稳定的海底环境─包括能把人压扁的压力和冰冷的黑暗─意谓海底某些最知名的栖居生物已以演化返祖的样态活了万世，形体几无变化。