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The better reaction conditions are as follows: Reaction temperature is 40°C, Reaction time is 5 hour; the ratio of L - phenylalanine to acetic acid and N - formyl - L- aspartyl anhydrideis 1:10.2:1.1, Its yield is 95.4%.

在查阅文献的基础上,得到较优的α-L-天冬氨酰L-苯丙氨酸甲脂盐酸盐的合成方案,在甲醇一水体系中,N-甲酰-α-L-天冬氨酰-L-苯丙氨酸在浓盐酸的作用下60℃水解90分钟,后冷却到15℃加入浓盐酸在20~30℃保温反应96小时,进行甲脂化,形成甲脂盐酸盐,结晶析出。

Strong acids, such as sulfuric acid, hampered from the occurrence of the phenol hydroxylation.

过强的酸,如硫酸、硝酸和盐酸,对苯酚羟基化反应造成危害,使羟基化反应不能发生。

A new spectrophotometric method for the determination of chromium has been developed. In HCl medium, the chromium oxidizes hydroxylammonium chloride to form nitrite, which produces a pink azo dye when reacting with p-aminobenzene sulfonic acid and α-naphthylamine.

基于铬在稀盐酸介质中氧化盐酸羟胺产生亚硝酸根,而亚硝酸根与对氨基苯磺酸重氮化后可与α-萘胺偶联产生粉红色偶氮染料,提出了分光光度法测定铬的新方法。

In HCl medium, iodate oxidizes hydroxylammonium chloride to form nitrite, which can produce a red azo dye with the reaction of p nitroaniline and α naphthylamine.

基于碘酸根在稀盐酸介质中氧化盐酸羟胺产生亚硝酸根,而亚硝酸根和对硝基苯胺重氮化后可以与α-萘胺偶联产生红色偶氮染料,提出了分光光度法测定碘的新方法。

The synthesis of nalbuphine hydrochloride from thebaine as starting material was through following processes:oxidation,high-pressure hydrogenation,acetylation,removing methyl of 3-methoxy,hydrolysis,condensation,reduction and finial salification.

以蒂巴因为起始原料,经氧化、高压氢化、乙酰化、氰化、脱3-位甲氧基的甲基、水解、缩合、还原、成盐,合成了盐酸纳布啡,总收率达18。

Aminobenzoic acid in procaine hydrochlorid compound injections was determined by differential spectrophotometry and Glenn's method of orthogonal function.

复方盐酸普鲁卜因注射液是盐酸普鲁卡因和对氨基苯甲酸为主要成份的注射剂,一用重氮化法必须分离后进行测定〔'〕。

In the second section, with ketone and hydroxylamine hydrochloride as the starting materials, 3-aminopropanol is prepared via three steps including reaction of ketone and hydroxylamine hydrochloride , condensation of ketoxime and acrylonitrile, and hydrogenation cracking of condensation product.

第二是3-氨基丙醇的制备,由酮肟丙烯睛缩合物催化氢化裂解制得:即先以酮、盐酸羟胺为起始原料在碱性条件下合成酮肟,再与丙烯腈反应生成酮肟丙烯腈缩合物后经催化氢化裂解制得3-氨基丙醇。

The process of the present invention consists in bringing into contact, on the one hand, gaseous phosphorus pentafluoride or a gaseous mixture comprising phosphorus pentafluoride and hydrochloric acid, and, on the other hand, a solution of lithium fluoride in hydrofluoric acid, in a column (10) having a sufficient number of transfer units to carry out the reaction of PF5 with LiF under the chosen conditions of temperature, of pressure and of molar ratio of the two contrasting reactants and with complete or substantially complete absorption of the PF5 in the column.

本发明方法是让气态五氟化磷或五氟化磷与盐酸的气态混合物与氟化锂的氟氢酸溶液在塔(10)中接触,该塔转化单元数足以在选定温度、压力与两种反应剂摩尔比条件下使PF5与LiF反应,塔中五氟化磷完全或基本完全被吸收。

Using hydrotreated gas oil as solvent, under the conditions of a reaction temperature of 400 C, a hydrogen partial pressure of 10 MPa and a reaction time of 1 h, a portion of coke deposits could be removed yet without the function of hydrogenating coke.

采用溶剂萃取法除去工业失活催化剂上沉积的焦炭和金属的研究结果表明,用四氢呋喃、吡啶和喹啉这3种含杂原子的有机强溶剂常温萃取催化剂,其去除焦炭能力很弱,而且会因这些溶剂的强吸附作用污染催化剂;盐酸洗涤能有效去除催化剂表面的钙、铁沉积层,但不能去除焦炭;低芳香性的加氢瓦斯油在400 C、H2压力为10MPa、反应1h的条件下可部分去除催化剂上的焦炭,但不具备强的氢化焦炭作用;1,2,3,4-四氢化萘因具有供给原子氢的能力,可以有效地氢化和去除催化剂上的焦炭。

The synthesis of aniline from benzene and hydroxylamine hydrochloride in acetic acid–water media under mild conditions was also studied. Using NaVO3 as the catalyst, its catalytic performance in the amination was investigated in detail.

本文还采用盐酸羟胺为胺化剂,考察了温和条件下醋酸-水介质中苯与盐酸羟胺合成苯胺的反应。

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According to the clear water experiment, aeration performance of the new equipment is good with high total oxygen transfer coefficient and oxygen utilization ratio.

曝气设备的动力效率在叶轮转速为120rpm~150rpm时取得最大值,此时氧利用率和充氧能力也具有较高值。

The environmental stability of that world - including its crushing pressures and icy darkness - means that some of its most famous inhabitants have survived for eons as evolutionary throwbacks, their bodies undergoing little change.

稳定的海底环境─包括能把人压扁的压力和冰冷的黑暗─意谓海底某些最知名的栖居生物已以演化返祖的样态活了万世,形体几无变化。

When I was in school, the rabbi explained everythingin the Bible two different ways.

当我上学的时候,老师解释《圣经》用两种不同的方法。