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The invasion of drilling fluid is the main cause to the damage of fractured formation. The composite salt free-gel drilling fluid is got after analyzing the influence of different kinds of such soluble adulterant as organic salt and non organic salt on the performance of the solid-free drilling fluid and studying the condition to develop the free gel structure and the method to improve the fluid's high temperature stability and inhibitive property. The experiment shows that the apparent viscosity of this system is as high as 27000 mPas when the share rate is 0.3 r/min and the high temperature reaches at the stable level of 150℃ and the HTHP filtrate loss decreases to 15 ml at 150℃.

钻井液侵入是裂缝性储层损害的主要因素之一,实验分析了无机盐、有机盐等不同类型水溶性加重剂对无固相钻井液性能的影响,研究了无固相钻井液快速弱凝胶特性形成条件以及高温稳定性和抑制能力的提高方法,研制出的无固相复合盐弱凝胶功能性钻井液高温稳定性达到150℃,具有独特的流变性(0.3r/min黏度达到27000 mPas)和优良的抑制能力(150℃HTHP滤失量小于15 mL),成本远低于甲酸盐钻井完井液。

In this paper we combined three chromatographic separation and purification technique such as affinity chromatography, ion exchanger chromatography and hydrophobic interaction chromatography to develope a new technology of stimutaneous extraction of three enzyme from pancreatin. We optimized the technology by studying the methods of purification and assured the technology as: The crude extraction from the dissolution of Pancreatin is directly absorbed on the DEAE gelose fast flow columnEquilibrating buffer is 0.01mol/L NaoAc-HoAc buffer(pH4.5; eluting buffer is 0.2~0.35mol/LNaCl in 0.01mol/LNaoAc-HoAc buffer (pH4.5), and then be eluted by two steps to acquire the peak of kallikrein.The solution which can"t be adsorbed by DEAE gelose fast flow column is adsorbed on affinity chromatographic column Equilibrating buffer is 0.01mol/LTris-HCl buffer(pH7.5, eluting buffer is 0.5mol/LNaCl in 0.01mol/Ltris-HCl buffer(pH7.5)and then be eluted by one step to acquire the peak of trypsin.The solution which can"t be adsorbed by is pretreated with 30%~80%(NH_4)_2SO_4 fractional precipitation, the deposition of the precipitation is dissolved to beabsorbed on phenyl gelose fast flow columnhydrophobic interaction chromatography condition is Equilibrating buffer is lmol/L(NH_4_2SO_4 in 0.01mol/LNaoAc-HoAc buffer(pH4.5), eluting buffer is 0~0.6mol/L(NH_4)_2SO_4 in 0.01mol/LNaoAc-HoAc buffer (pH4.5) and then be eluted by two steps to acquire the peak of chymotrypsin.

本研究考察了各种纯化方法,将离子交换层析、亲和层析和疏水层析三种分离纯化法相结合,建立了激肽释放酶、胰蛋白酶和糜蛋白酶三酶的联产工艺:胰酶用pH4.5醋酸缓冲溶液提取后,粗提液直接上DEAE-琼脂糖快胶柱吸附平衡缓冲液:0.01mol/LNaoAc-HoAc缓冲液(pH4.5,洗脱缓冲液:0.01mol/LNaoAc-HoAc缓冲液(pH4.5)含0.2~0.35mol/LNaCl分两步洗脱,收集激肽释放酶的洗脱峰;DEAE-琼脂糖快胶的未吸附液上亲和层析柱分批吸附平衡缓冲液:0.01mol/LTris-HCl缓冲液(pH7.5,洗脱液:0.5mol/LNaCl溶液,一次洗脱,收集胰蛋白酶洗脱峰;最后,亲和层析未吸附液用30%~80%硫酸铵分级盐析处理,沉淀溶解后用上苯基—琼脂糖快胶吸附平衡缓冲液:0.01mol/LNaAc-HAc缓冲液(pH4.5含1mol/L(NH_4)_2SO_4,洗脱缓冲液:0.01mol/LNaAc-HAc缓冲液(pH4.5)含0~0.6mol/L(NH_4)_2SO_4,分两步洗脱,收集糜蛋白酶的洗脱峰。

The results show that a MgSnO3·H2O conversion film is formed by treatment in the stannate solution at 90℃, and the immersion test and potentiodynamic polarization show that the corrosion resistance of the AZ91D alloy is improved to some extent.

结果表明:锡酸盐转化处理后合金表面形成了以MgSnO3·H2O为主要成分的转化膜,可对合金起到一定的防护作用;转化膜由细小的球形颗粒密积而成,颗粒之间存在间隙,它可以为化学镀镍的前处理过程提供良好的吸附条件;转化膜上的化学镀镍层组织致密、无缺陷, MgSnO3·H2O转化膜在镀镍层与基体之间起到过渡作用,镀层的磷含量达到9%,与基体结合良好;在3.5% NaCl (pH=7)溶液中的动电位极化测试表明,镀镍以后的合金在阳极极化过程中发生了明显的钝化,耐腐蚀性能进一步提高,对基体起到了较好的防护作用。

The problem that noxious chrome of sexavalence and trivalence is present in the galvanizing coat and passivating solution of the prior art is solved substantially by the passivating solution of the present invention.

本发明提供的无铬钝化液可以从根本上解决了现有的产品镀锌层及钝化液中含有有毒有害的六价铬和三价铬元素的问题,并可真正替代现有的含有六价铬和三价铬的铬酸盐钝化液,实现对电镀锌层和热镀锌层的钝化。

The second layer (10) comprises: 100 parts by weight of an acrylonitrile-butadiene rubber, said acrylonitrile rubber comprising from 20 to 65 percent by weight of bound acrylonitrile; from 3 to 20 parts by weight, per 100 parts by weight of the NBR, of at least one acid acceptor; from 1 to 10 parts by weight, per 100 parts by weight of the NBR, of at least one organophosphonium salt; and from 0.25 to 10 parts by weight, per 100 parts by weight of the NBR, of at least one amidine.

公开的是一种包含直接相互接触的第一层与第二层的软管;第一层包含从四氟乙烯、六氟丙烯、偏二氟乙烯、和全氟乙烯醚衍生的一种热塑性四元共聚物;第二层包含100重量份丙烯腈丁二烯橡胶,所述丙烯腈橡胶包含约20~约65wt%结合丙烯腈;每100重量份NBR约3~约20重量份至少一种酸受体;每100重量份NBR约1~约10重量份至少一种有机盐;和每100重量份NBR约0.25~约10重量份至少一种脒。

By a method using fraction precipitation of ammonium sulphate, ion exchange, modified hydrorylapatite and gel filtration chromatography, we separated and purified two kinds of phycoerythrin(R-PE and r-PE) from Corallina officinalis . The purity standard(ratio of ODs65/OD2go) of R-PE reaches to 11, which is the highest purity comparing with the reported purity of phycoerythrin.

经盐析、离子交换层析、羟基磷灰石吸附层析和凝胶过滤层析等分离纯化方法,从珊瑚藻中分离纯化出两种藻红蛋白,其中R-PE纯度OD_(565/OD_(280)高达11左右,是目前国内外报道的藻红蛋白中纯度最高。

FT-IR spectra shows that the polyaniline is present primarily in the emeraldine salt form, and the polymeric chains interact with inorganic framework, most likely via V=O…HN hydrogen bonding. XRD,TG and DSC indicate that the lamellar structure of the V_2O_5 is preserved, PAn chains eliminate water form the interlamellar region and are partially inserted between the layers, and exist with extended-chain conformation owing to the confined environment.Electrochemical investigation in the range of 1.8~3.8V vs.

红外光谱表明复合物中PAn主要以导电聚苯胺盐的形式存在,PAn链与V_2O_5晶格之间可能形成了V=O…HN氢键。X射线衍射、热重和差示扫描量热证实了PAn/V_2O_5复合物保持了较规整的层间排列结构,PAn取代了V_2O_5干凝胶中的层间水而部分嵌入其片层间,由于受空间的限制,PAn分子链以比较伸展的链构象存在。

The salty gland of Messerschmidia sibirica is developed from epidermic cell of stem and leaf.

利用石蜡切片法研究了砂引草茎叶的解剖结构,尤其是对泌盐腺的位置、泌盐腺的形态结构及泌盐腺的发生发育过程进行了系统的研究,结果表明:砂引草茎的初生结构维管束是外韧的,且其有10-12束,大小不等,髓和髓射线发达;叶的上下表皮细胞各一层,栅栏组织与海绵组织分化明显。

The results of observation on the microstructure of Karelinia caspica, Tamarix stromongolica, Salsola collina. Cheno Dodium glaucum, stipa bangenana show that the nutritional organs of these halophytes present some adaptability structures as follows:(1) sunken stomas, thick cuticle and orderly arrangement of epidermal cell;(2) equilateral leaves with developed palisade tissue, or squama-shaped leaf;(3) well-developed water-storing tissue in stems and leaves;(4) crystal cells, salt glands in most of the leaves and assimilating branches.

通过对花花柴、甘蒙怪柳、猪毛菜、灰绿藜、长芒草五种盐生植物显微结构观察,这五种盐生植物营养器官的形态结构均呈现一定的适应性特征:(1)气孔器下陷,角质层加厚,表皮细胞排列紧密而整齐;(2)多为等面叶,叶片栅栏组织发达,或退化为鳞片状,而具同化枝;(3)茎、叶多为肉质化,贮水组织发达;(4)具有含晶细胞,枝叶具盐腺。

Study and application on reservoir sensitivity of Baimiao gas condensate field ;2. Yangtake gas condensate field exists a suit of composite salt bed in Eogene system,in which interspersing soft mudstones.

羊塔克凝析气田位于塔北隆起羊塔克构造带1号构造东端,下第三系普遍存在一套复合盐岩层,特别是夹在复合盐岩层中的软泥岩、复合盐膏层缩径与井漏并存,造成井眼极不稳定,给钻井施工带来很多复杂和事故,其钻井风险很大,尤其是216mm井眼的电测和下套管作业更是异常困难。

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