盐分析法

Poly/melamine cyanurate composite latex particles are prepared via soapless emulsion polymerization. XPS data and TGA analysis reveal that MC particles are encapsulated by PMMA during polymerization, resulting in the formation of a core-shell structure of PMMA/MC composite latex particles. MC can affect the thermal degradation and promote the charring of PMMA. The application of PMMA/MC in nylon 6 (PA6) indicate that the composite latex particles can improve the mechanical pro...

采用原位乳液聚合法制备了聚甲基丙烯酸甲酯/三聚氰胺氰尿酸盐复合胶粒，对其进行X光电子能谱及热重分析结果显示，在MC阻燃剂颗粒表面覆盖了一层PMMA胶膜，形成了具有核-壳结构的PMMA/MC复合胶粒；MC能影响PMMA的热降解过程并促进其成炭；在尼龙6(PA6)中的应用结果表明，PMMA/MC复合胶粒能改善PA6的力学性能和阻燃性能。

Using pickling liquid wastewater of hydrochloric acid,iron scurf and aluminiferous mine as raw materials,a series of poly-aluminum-ferric-silicate-chloride which has different molar ratio of Si:Al:Fe was prepared.

利用天津某钢厂的工业废料——盐酸酸洗废液、铁屑和含铝矿等为原料，合成了具有不同摩尔比的无机高分子絮凝剂聚硅酸氯化铝铁，采用Zeta电位测定法分析了产品在其水解溶液中的带电情况，并通过絮凝实验对絮凝剂的絮凝机理作了初步分析。

The UV and IR spectroscopic studies of the monomer films showed that the photoreaction ratio of monomer (about 50%) was higher than the corresponding photosensitive polymer (about 10%, PVCi). The polarized IR spectra proved that obvious anisotropic absorption was displayed in the irradiated photosensitive film. With polarizing microscopy method, we found that these kinds of photoalignment films exhibited good alignment ability, and the stability of the photoalignment film could reach about 100℃. 2 A photosensitive self-assembled monolayer was fabricated that contained photo-cycloadditable groups, such as, coumarin and cinnamate. The reaction process were detected by contact angle method because the IR absorption of monolayer was very weak. The photosensitive self-assembled monolayer promote uniform alignment of nematic liquid crystals by LPUV, and it thermal stability could reach about 130℃. 3 A cationic bolaform amphiphiles was synthesized that had two photosensitive double bonds, and can be polymerized by ultraviolet. A layer-by-layer self-assembled deposition film was prepared in aqueous solution by using this material and poly (sodium 4-styrenesulfonate). The UV-Vis. spectra proved that the multilayers film was uniform and layer-by-layer. When LPUV irradiated the film, the photopolymerizable double bond underwent [2+2] cycloaddition, and the production of the reaction distributed along the polarized direction of incident LPUV. Polarized UV-Vis. spectra indicated that the irradiated self-assembled multiplayer film was anisotropic, and the dichromic ration is about 0.09, it is higher than the spin-coating method of photosensitive polymer or monomer. We used this anisotropic film as alignment layer of nematic liquid crystals, and obtained a uniform and stability alignment result, the static contrast ratio is about 100, which is very close to application of liquid crystal device. This thesis is an instance that the photochemical material was used in the physics region of liquid crystals, the route that was from photosensitive monomer, self-assembled monolayer film to self-assembled multiplayer film was undergone, by this logical research method photoailgnment of liquid crystal was extended and consummated.

围绕上述思路开展了如下工作：1合成了三种可进行光二聚反应的光敏小分子单体，LPUV 辐照制作了光控取向膜；用紫外-可见光谱法和红外光谱法分析了薄膜中的光化学反应，发现小分子的光反应程度可达到50%以上，至少比光敏高分子高出5倍；薄膜的偏振红外光谱证实，经过LPUV 辐照后薄膜出现了明显的各向异性；将小分子光控取向膜制成液晶器件，在偏光显微镜下观察看到均匀一致的液晶取向；并且热稳定性达到100℃左右，接近实用化要求。2制备了含肉桂酸、香豆素基团的自组装单层膜；采用接触角的方法监测自组装反应的动力学过程；紫外-可见光谱证实了自组装单层膜在石英基板表面形成；自组装单层膜经LPUV 辐照后能诱导液晶均匀取向，而且热稳定性可达130℃，热稳定性进一步提高。3合成了含有光敏双键的双季铵盐，在水溶液状态下将它和聚乙烯基苯磺酸钠沉积生成layer-by-layer 自组装多层膜，紫外-可见光谱证实这是一个逐层均匀的沉积；在LPUV 照射下，自组装膜中的光敏双键按照偏振方向发生[2+2]环加成反应，形成取向膜，用二向色性值评价的分子取向度高于高分子及小分子光控取向膜的水平；实验证明用自组装多层膜制成的液晶器件亮暗态均匀，静态对比度约为100，达到实用化器件的水平。

METHODS: Whole blood samples (3.000 L) from 10 healthyvolunteers (2 female, 8 male) were acidified by adding 40 Lof hydrochloric acid of increasing molarity to achieve a bloodpH between 7.0 and 7.37, and coagulation was analyzedby rotational thromboelastometry after an incubation periodof 30 min using both intrinsically and extrinsically activated assays.

来自10名健康志愿者（2女，8男）的全血样本(3.000L)，加入40L 摩尔浓度增加的盐酸酸化以达到血 pH介於7.0和7.37之间。用本质和非本质活化测定法孵化30分钟后，再用旋转血栓弹性测定法分析凝血功能。

Lithium metaborate melting technology was used to make the quick analysis flow sheets of rock samples by Inductively Coupled Plasma Atoms Emission Spectrometry.

应用偏硼酸锂熔融技术建立岩石样品电感耦合等离子体原子发射光谱法的快速分析流程，并针对含锂硼酸盐熔融物较难溶解的特点，通过熔剂与样品混匀方式实验、熔融体形成龟裂条件实验和浸取液条件实验，研究三者与熔融物浸取时间的关系，从而选择一个适合ICP-AES分析技术的最佳熔融和浸取条件。

The purpose of this study is to screen microorganisms with growth inhibition against plant fungal pathogens. The plate-dilution method was used to isolate the bacteria from salt marshes at Dafeng, Jiangsu. The antifungal activity of the bacterial broth filtrates against 5 phytopathogens was determined using mycelial disk method. The antifungal compositions of four active bacteria were analyzed primarily with chromatography techniques. Two hundred and thirty-five aerobic (92) and anaerobic (143) bacterial strains have been isolated from the coast salt marsh and sixty-five strains, of which 39 are aerobic and 26 are anaerobic showed greater than 30% of inhibition rate against the growth of at least one of the phytopathogenic fungi on petri dish.

为了开发对植物病原真菌生长有抑制作用的药源微生物，本实验采用平板稀释法从江苏大丰盐沼湿地土壤中分离微生物，并通过菌丝块法检测这些微生物代谢产物对5种植物病原真菌生长的抑制活性，进而利用柱层析分析其活性成分；结果共分离得到235株细菌，其中好氧细菌92株，厌氧细菌143株；体外活性测试结果显示有65株至少对1种测试植物病原真菌的抑制率在30%以上，其中好氧菌39株，厌氧菌26株。

Methods The cultured 3T3 -L1 cells were pretreated with naringin, and then MTT method was used to detect the proliferation of the cells, oil red O staining method and spectrophotography were applied to analyze the degree of differentiation.

培养3T3-L1细胞，并用不同浓度的柚皮苷进行干预，以四甲基偶氮唑盐法检测细胞增殖，用油红O染色和染色比色法分析脂肪细胞的分化程度。

Comparative tests of black color passivation of zinc coating based on reference formulas published in literature including copper salt method, silver salt method and method of mixture of copper salt and silver salt were conducted.

根据已发表的镀锌层黑色钝化的铜盐法、银盐法及铜银结合法等类型的黑色钝化的参考配方进行了对比试验，并就其中较为理想的钝化配方的成分含量及其作用、操作条件的影响做了细致的分析，并对钝化液配制时的注意事项予以说明。

This thesis has chosen the H_2SO_4 anode oxidation. From degreasing, alkaline cleaning, neutralization, the effect of surface before hand treatment on the quality of surface anodizing treatment is discussed. From electrolyte concentration, electrolyte temperature, voltage, timing, additive, the effect of anodizing oxidation on the quality of surface treatment are discussed, From hole sealing liquid composition pH, value, timing, the effect of hole sealing on the quality of surface oxidation treatment are examined.

对氧化的各个工序进行了较详细的分析，通过脱脂、碱蚀、中和等表面预处理进行了详细的研究讨论，确定了三个预处理工序的最佳工艺控制参数；从阳极氧化机理着手，对阳极氧化电解液浓度，氧化电解液温度，氧化时间、电流密度，氧化电压，添加剂等对氧化质量的影响因素进行了分析；对化学氧化工艺进行了传统的铬酸盐-磷酸盐氧化法正交实验研究，讨论了各个氧化液成分对氧化膜性能的影响。

This study focused on the absorption of vapor into aqueous LiBr and the absorption of ammonia gas into aqueous ammonia.

本项目以溴化锂溶液和氨水溶液作为研究重点，主要内容包括：对添加剂作用下的溴化锂溶液和氨水溶液表面张力进行了实验研究，发现添加剂对两种溶液表面张力的影响呈现出不同的性质；利用表面吸附动力学原理，对溶液的表面张力及动态表面张力进行了理论分析；利用激光阴影法对溴化锂溶液静池吸收过程中马拉戈尼对流的形成进行了可视化研究，并进而发现蒸汽添加剂比液体添加剂对吸收具有更好的强化效果；利用实验方法对溴化锂溶液垂直降膜吸收进行了研究，并从其基本方程出发得出了影响添加剂强化效果的主要因素；同时，也对添加剂对氨水鼓泡吸收的影响进行了实验研究；最后，对添加剂的强化机理进行了分析，即对于溴化锂溶液来说，添加剂对溶液吸收的影响主要体现在对吸收界面吸附特性的影响上，无论是气体添加剂还是液体添加剂，都有可能对溴化锂溶液吸收起到强化作用；对于氨水溶液而言，添加剂的影响主要还是体现在&盐析&作用上，当氨水浓度较低时，添加剂有可能对吸收起到强化作用。

Do you know, i need you to come back

你知道吗，我需要你回来

Yang yinshu、Wang xiangsheng、Li decang,The first discovery of haemaphysalis conicinna.

1〕 杨银书，王祥生，李德昌。安徽省首次发现嗜群血蜱。