盐分析法

In this paper, high citric acid content was analyzed by precipitation in the system of treating SO2 in flue gas by citrate solution.

本文采用重量法对柠檬酸盐法治理低浓度二氧化硫体系中柠檬酸根进行了分析测定。

Based on the previous literatures, the following major innovation works were carried out in this dissertation:(1) The derivatization reaction conditions of ephedrine and pseudoephedrine with sensitive derivation reagent in aqueous system were studied and two new methods were developed for the assay of them by microemulsion electrokinetic chromatography and micellar electrokinetic chromatography with LIF detection. The sensitivity and analysis times were greatly improved compared with the previous reports;(2) A new method of CZE with indirect LIF detection was developed for the simultaneous determination of six coumarin compounds (esculin, esculetin, isofraxidin, genistein, naringin and sophoricoside) with fluorescein as the probe. The proposed method enlarges the application range of LIF detector, and provides new approach for the analysis of certain compounds difficult to derivatize;(3) Based on the above research, an MEKC with indirect LIF detection method for the simultaneous determination of adenine and guanine in DNA extracts from fungus, maize and soybean was established;(4) A new method for the investigation of the complexes formed between human serum albumin and ampicillin sodium under the simulated physiology conditions using laser light scattering technique was developed.

该论文在综述前人工作的基础上，开展了如下未见文献报道的创新性的研究工作：(1)使用灵敏的衍生试剂对麻黄碱和伪麻黄碱在水体系中的衍生反应条件进行了系统研究，建立了微乳电动色谱-激光诱导荧光检测法和胶束电动色谱—激光诱导荧光检测法测定麻黄碱和伪麻黄碱的灵敏分析新方法，与以前的报道相比，灵敏度和分析时间均有很大改善；(2)使用荧光素钠作为背景荧光试剂，建立了同时分析测定六种黄酮类化合物(秦皮甲素、秦皮乙素、异秦皮定、染料木素、柚皮苷和槐角苷)的毛细管区带电泳—间接激光诱导荧光检测新方法，扩大了激光诱导荧光检测的应用范围，对难衍生化合物的分离分析提供了一种新思路和新途径；(3)以荧光素钠作为背景荧光试剂，建立了一种用于同时测定食品提取DNA中的腺嘌呤和鸟嘌呤含量的胶束电动色谱—间接激光诱导荧光检测新方法；(4)用动态和静态激光散射法研究了模拟生理条件下人血清白蛋白与氨比西林钠盐相互作用所形成的复合物，为药物分子与蛋白质的相互作用、药代动力学等的研究提供了一种新思路。

By analyzing the result of these experiments, we realizing that the solvent is very essential in the controlling of the crystallizing and the melting salt works as solvent is possible, and we proposed the idea of operating chemical metathesis synthesizing in melting salt.

通过对实验结果的分析，根据溶剂对于纳米晶粒生长的重要性和熔盐作为溶剂的可能性，我们提出了熔盐中的化学交换法的思路。

The property of no film, micro-arc oxidation film and chromate film influenced the corrosion of joint samples which was analyzed in same corrosive conditions by calculate the corrosion effects and observe macro-photograph micro-photograph. The corrosive regularity influenced by corrosive condition factors and the corrosion resistance of different thickness of micro-arc oxidation film also be compared.

采用减重法计算连接腐蚀效应并观察试样表面的腐蚀宏观及微观形貌，对比分析了无表面处理、铬化处理及微弧氧化处理在相同盐雾腐蚀条件下对减小镁合金-钢连接腐蚀作用的差异性以及盐雾腐蚀条件参数对镁合金-钢连接腐蚀的影响规律。

Proliferation of cells was analyzed by mitochondrial reduction of tetrazolium salt MTT to formazan and actual cell count.

用四甲基偶氮唑盐法和细胞计数法分析细胞增殖情况。

The technological process in preparation of the delafossite structure p-TCO thin films by sol-gel method is discussed systematically. The relative advantages and disadvantages of the systems of sol about organic alkoxide and inorganic salt are analyzed, and further development are discussed. It is pointed out that sol-gel method is an effective and feasible means to prepare p-TCO thin films.

本文介绍了铜铁矿结构p-TCO的结构特性以及溶胶凝胶法的基本原理和特点；系统地介绍了溶胶凝胶法制备铜铁矿结构p-TCO薄膜的工艺；分析比较了有机醇盐、无机盐溶胶体系的优缺点；最后讨论了进一步的发展方向，指出溶胶凝胶法是一种高效可行的制备p-TCO薄膜的方法。

In this paper, we analyzed the larch extract tannin, aminom ethylation of larch extract tannin, quaternization of cationic larch extract tannin and amphoteric larch extract tannin (sulfonation of the larch extract tannin quaternary ammonium) by infrared spectral analysis, confirmed the quarternization and sulfonate groups, and measured its water treatment properties such as flocculation, scale inhibition, results showed that quaternization of larch extract tannin and amphoteric larch extract tannin have better water treatment ability, can realize the multifunction.

本论文采用红外光谱法对落叶松单宁、胺甲基化落叶松单宁、阳离子落叶松单宁季胺盐、两性落叶松单宁进行了化学结构分析，并对其水处理剂性能如絮凝、阻垢进行了检测。实验结果表明：落叶松单宁季胺盐和两性落叶松单宁均具有较佳的水处理能力，是性能良好的一剂多效工业水处理剂。

The density of potassium fluotantalate and its mixed melt salt system with sodium chloride, potassium chloride, sodium fluoride and potassium fluoride are measured by Archimedes principle .

用阿基米德法测定了氟钽酸钾及其与氯化钠、氯化钾、氟化钠、氟化钾等混合熔盐体系在熔融状态下的密度，用线性回归分析方法导出了各熔盐体系的密度与温度的关系。

We also introduced spectrophotometer into the analysis of sulfamate type electrolete to measure the content of nickel sulfamate for the first time. This method is much easier than the conventional chemistry titration, it can be accomplished within one minute. Furthermore, it enhances significantly the precision of the measurement.

在电铸液分析中，我们首次将分光光度法应用于氨基磺酸盐型镍电铸液中氨基磺酸镍的测定，该方法较传统的化学滴定法操作更简单，它可以在1分钟内完成氨基磺酸镍浓度的测定，且大幅提高了分析结果的精确度，样品的消耗量仅为原来的千分之一。

The paper analyzes the advantages and disadvantages of desalting technology by membrane process adopted in iron and steel enterprises at home and puts forward the reform program.

钢铁企业综合污水处理厂的出水脱盐处理回用具有重要意义，本文对国内一些钢铁企业采用的膜法脱盐技术的优缺点进行了分析，并提出了改进方案。

Do you know, i need you to come back

你知道吗，我需要你回来

Yang yinshu、Wang xiangsheng、Li decang,The first discovery of haemaphysalis conicinna.

1〕 杨银书，王祥生，李德昌。安徽省首次发现嗜群血蜱。