盐分析法

In this paper,that a series of sodium tungsten bronze crystals were prepared by electrolysis of molten salts containing sodium tungstic and tungstic oxide was reported.

文中采用熔盐电解法，电解钨酸钠与三氧化钨熔盐制备出系列钠钨青铜晶体，选用离子选择电极分析法快速、简便、可靠地测定了晶体中的钠含量，并通过X－射线粉末衍射确定了晶体的晶型结构及晶格常数a。

The isomerization of resin acid was studied by HCl catalysis method, high temperature catalysis method and microwave-assisted method. Separation of abietic acid was analyzed with recrystallization method and many organic amine salt methods; Using abietic acid separated from resin acid as raw materials, 6 compounds of abietic-type resin acid derivetives were synthesized.

从产率、纯度和成本等方面分析对比了改进的二戊胺盐法、A胺盐法、B胺盐法和文献报道的二戊胺盐法分离提纯枞酸；以得到的枞酸为原料，进行氧化合成，得到6种枞酸的氧化衍生物，通过柱分离得到2种枞酸氧化衍生物纯品，并测试了其抑菌和对家蝇的拒食活性。

Two inducible and extracellular chitosanases secreted by Penicillium sp. D-l were purified by ammonium sulfate precipitation as well as gel filtration. The purified enzymes of ChoA and ChoB had molecular masses of 93 and 21 kDa by SDS-PAGE. Both ChoA and ChoB have an acidic pH optimum, which were 4.0. The enzymes were stable over the pH range 3 to 5 for 1 h.

采用(NH_4)_2SO_4盐析法和凝胶过滤层析对Penicillium sp.D-1的壳聚糖酶进行分离提纯，得到两种壳聚糖酶，酶A经变性聚丙烯酰胺凝胶电泳分析，结果显示该酶的分子量约为93 kD；酶B经非变性聚丙烯酰胺凝胶电泳和SDS-PAGE分析，得出分子量约为21 kD。

Hot corrosion behavior of Na2SO_4 coated B-1900 alloy was studied in air at 827 and 750℃.Corrosion kinetics of the coated alloy was gravimetrically measured,and contents of water soluble ions in the reaction products were chemically analyzed.X-ray diffraction and EMP techniques were employed to determine the components and morphology of the corrosion product scale.

用涂 Na_2SO_4盐膜法研究高温合金 B-1900在827℃和750℃于空气中的热腐蚀行为，测定其腐蚀动力学曲线，用 X -射线衍射和电子探针元素面扫描方法分析腐蚀产物的相组成和成份，还对其中的水溶性离子进行化学定量分析。

By analyzing soil quality of 4 kinds of land use types in Kalamay agriculture development area according to principal component analysis, we draw the conclusions: nature shrub tree land is affected little by mankind, a great deal of organic matter return to soil every year, and root system can improve soil physical quality, can absorb salt from soil, so the soil quality of nature shrub tree land is the best; the soil quality of farmland is better than the soil quality of manpower Tamarix Bulrush land, which may be reasoned that man make for soil quality by irrigation to exclude salt and fertilizing organic muck in the earlier oasis digging up period. Soil physical qualities of tree land get harden and worsen for flooding irrigation, furthermore climate in Kalamay is dry and rainless , the other irrigation is very long time after the former one, so soil get harden severity and result soil physical quality get worse and worse.

利用主成分分析法分析新疆克拉玛依农业开发区四种土地利用方式下的土壤质量，得出：天然灌木林地，受人为影响较小，每年有大量有机物质返还土壤，且天然灌木的根系可以很好的改良土壤的物理性质，同时所选天然灌木林灌木多是耐盐碱并且本身又具有吸收积累来自土壤的盐分，土壤质量最好；农田受到的人为影响最大，但农田综合得分却好于人工柽柳芦苇地综合得分，这可能是由于在开垦初期的绿洲农田，受到了人们灌水压盐及增施各种有机无机肥料等有利于土壤质量提高的措施所致；乔木林地，由于人们用大水漫灌的方式灌溉，致使林地土壤变得板结，土壤物理性质下降，加上克拉玛依地区气候干燥少雨，一次灌溉后较长时间后才有下一次灌溉，致使土壤理化性质恶化，土壤质量不高。

The effects of FLLPS on the immunoactivity of mouse speen lymphocyte were studied in vitro or vivo by means of MTT.

采用四甲基偶氮唑盐比色分析法，对其多糖成分进行了小鼠体内外免疫活性观察。

Experiment was conducted with mature leaves of Zizyphus jujuba Mill. cv. Chuangan (stored at -20℃,-70℃, dried with silica gel) and 3 methods, including CTAB, high salt precipitation and high salt and low pH were used for total DNA extraction for studying their effects on DNA extraction.

以串杆枣的成熟鲜叶为试材，分别采用-20℃、-70℃和硅胶脱水干燥3种方法保存样品，采用简易CTAB法、高盐沉淀法与高盐低pH值法分别对3种方法保存的样品及对照样进行了基因组DNA提取效果的比较分析。

By this method, the productivity of 3. 18g/l extracellular polysaccharides was obtained. The optimum extraction method was obtained by RSA. It was determined as follows: 91. 4 ℃, 2. 9h, the weight ratio between mycelia and water was 1 to 3. The productivity was 12. 38% of dry mycelia. Set the purifying methods of Grifola frondosa: Precipitated polysaccharides part by 60% ethanol→removed protein by Sevag method→removed coloring matter by H〓O〓→removed salts by dialyse→DEAE-cellulose column chromatogram→ purified polysaccharides groups.

对于胞内多糖的提取，采用湿菌体经捣碎再高压破壁的方式破碎菌体细胞，采用响应面分析法得出优化后的提取条件为：提取温度91.4℃，提取时间2.9h，料水比1：3，此提取条件下胞内粗多糖的率为干菌体重的12.38％建立了灰树花多糖分离纯化的技术路线 60％乙醇沉淀的粗多糖→Sevag法脱蛋白→H〓O〓脱色→透析脱盐→DEAE-纤维素层析分离→多糖组分。

Dorsalis by salting out, ion exchange chromatography, and gel filtration chromatography. By salting out the egg homogenate, SDS-PAGE analysis revealed that the Vns were mainly precipitated in a 50~70% ammonium sulfate solution. The salted-out proteins were further purified by ion exchange chromatography, and the result showed that Vns were mainly eluted with a 0.3~0.5 M sodium chloride gradient. Finally, the elutes of ion exchange chromatography were refined by running them through gel filtration chromatography to obtain purified Vns. SDS-PAGE separated the 48- and 51-kDa purified Vns, and used them as antigens to raise polyclonal antibodies.

利用硫酸铵盐析法初步分离果实蝇卵中的蛋白质，以SDS-PAGE蛋白质电泳分析得知，卵黄蛋白主要在硫酸铵溶液浓度为50~70%时被沉淀出；盐析沉淀所得之卵黄蛋白，再以离子交换层析法进一步纯化显示，卵黄蛋白主要会在0.3~0.5 M氯化钠的浓度范围间被析出来；再将析出液浓缩后，经凝胶过滤层析法做最后的纯化，即获得纯化之卵黄蛋白。

The seed purity of more than one hundred and thirty samples of six maizevarieties was assayed by using the three testing methods: storage proteins electrophoresis,isozyme isoelectric focusing in acrylamide and examination at field plots. Some importantpoints can be concluded from analyses as spearman order rank correlation on the seedpurity data as follows:First, there were deviations of the real performances to those purities obtained from out or in laboratory testing, even from the examination at field plot that is a routine way. Second, the seed globulin and isozyme electrophoresis, both with characteristics of rapid, cost-effective, devoid of environmental effect and speed, showed consistent purity; while the field-testing gave a higher degree of purity on the high side of cost than that in-lab approaches. Third, a good consistent purity was observed in the field plot and seed globulin testing, whereas inconsistency between field-testing and isozyme process. The last point is that seed globulin electrophoresis be a practical method apt to seed purity testing for maize.

并对130多份样品用三种检验方法(盐溶蛋白电泳、同功酶等电聚焦电泳和田间小区)检测的种子纯度数据作排序相关等统计分析，得到如下结果：室内外检测方法都会与种子真实状况有一定差异，田间种植鉴定与真实情况符合性并不一定最好；盐溶蛋白与同功酶等电聚焦这两种方法检测种子纯度所需时间短，成本低，不受外界环境限制，出结果快，二者的结果没有太大差异；田间种植鉴定成本较高，检测的结果普遍偏高；等电聚焦电泳与田间鉴定的一致性年度间存在差异，而盐溶蛋白凝胶电泳法与田间鉴定的一致性较高；种子盐溶蛋白凝胶电泳法较适于鉴定玉米种子纯度。

The absorption and distribution of chromium were studied in ryeusing nutrient culture technique and pot experiment.

采用不同浓度K2CrO4(0，0.4，0.8和1.2 mmol/L)的Hoagland营养液处理黑麦幼苗，测定铬在黑麦体内的亚细胞分布、铬化学形态及不同部位的积累。

By analyzing theory foundation of mathematical morphology in the digital image processing, researching morphology arithmetic of the binary Image, discussing two basic forms for the least structure element: dilation and erosion.

通过分析数学形态学在图像中的理论基础，研究二值图像的形态分析算法，探讨最小结构元素的两种基本形态：膨胀和腐蚀；分析了数学形态学复杂算法的基本原理，把数学形态学的部分并行处理理念引入到家实际应用中。