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Based on the investigation of the transesterification between dimethyl sebacate and 1,2,2,6,6-pentamethyl-4-piperinol, the synthetic technologies of Tinuvin292 and Tinuvin 765 were established. The two kinds of hindered amine light stabilizers were obtained in the yield of 93.3% and 92.4% respectively and qualified as the advanced level of the kindred overseas products.2. The synthetic technology of Tinuvin123 was studied and established. Using 2,2,6,6-tetramethyl-4-piperinol as the starting material, the product was synthesized successfully through oxidation, free-radical reaction and transesterification in overall yield of 57.6%.

本文研究建立了三个受阻胺类光稳定剂的合成工艺,探索了聚合型受阻胺类光稳定剂生产过程中不溶性副产物产生的原因,并设计、合成了一系列具有抑菌活性的新型受阻胺类光稳定剂。1、在研究癸二酸二甲酯与1,2,2,6,6-五甲基哌啶醇的酯交换反应的基础上,建立了受阻胺类光稳定剂Tinuvin292、Tinuvin765的合成工艺,分别以93.3%和92.4%的收率得到了光稳定剂Tinuvin292、Tinuvin765,所得产品质量达到了国外同类产品的水平。2、研究建立了受阻胺类光稳定剂Tinuvin123的合成工艺。

The synthetic technologies of three hindered amine light stabilizers were established, the reason for the insoluble side products formed in the production of polymerized hindered amine light stabilizers were studied, and a series of novel hindered amine light stabilizers with antibacterial properties were designed and synthesized in this present paper.1. Based on the investigation of the transesterification between dimethyl sebacate and 1,2,2,6,6-pentamethyl-4-piperinol, the synthetic technologies of Tinuvin292 and Tinuvin 765 were established. The two kinds of hindered amine light stabilizers were obtained in the yield of 93.3% and 92.4% respectively and qualified as the advanced level of the kindred overseas products.2. The synthetic technology of Tinuvin123 was studied and established.

本文研究建立了三个受阻胺类光稳定剂的合成工艺,探索了聚合型受阻胺类光稳定剂生产过程中不溶性副产物产生的原因,并设计、合成了一系列具有抑菌活性的新型受阻胺类光稳定剂。1、在研究癸二酸二甲酯与1,2,2,6,6-五甲基哌啶醇的酯交换反应的基础上,建立了受阻胺类光稳定剂Tinuvin292、Tinuvin765的合成工艺,分别以93.3%和92.4%的收率得到了光稳定剂Tinuvin292、Tinuvin765,所得产品质量达到了国外同类产品的水平。2、研究建立了受阻胺类光稳定剂Tinuvin123的合成工艺。

Keywords Di-(2-ethylhexyl)-sebacate;reinforced concrete;corrosion;polarization curve;electrochemical impedance

癸二酸二异辛酯;钢筋混凝土;腐蚀;极化曲线;交流阻抗法

The compression heating characteristics of three pressure-transmitting fluids such as dioctyl sebacate,water and ethanol in high hydrostatic pressure processing were investigated via the on-line measurement of temperature by inserting the probe into the high-pressure cavity.

通过将温度探头伸入高压腔内在线测定了3种传压介质(癸二酸二辛酯、水、无水乙醇)的温度变化情况,研究它们在不同条件下的压致升温规律。

Several main non-ionic surfactants (AEO、TX、SpanTweem、EL) was used to emulsify liquid paraffin and di octyl sebacate and the anti-coalescence stability of the corresponding emulsion was studied, the impact of the presence of benzene and double bond in lyophobic moiety of surfactant and its length and matching with dispersed phase upon the interfacial viscosity and Gibbs elasticity was analyzed.

本文采用了几种主要的非离子活性剂(AEO、TX、Span-Tween、EL)来乳化白油和癸二酸二辛酯,通过对各乳液体系抗聚并稳定性的考察,分析了活性剂亲油链段的长度、苯环和双键的存在、及亲油链段与被乳化对象分子结构的匹配关系对界面粘度和Gibbs弹性的影响。

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