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Aroma components of Hexylalcohol,Benzeneethanol,Butylalcohol,Pentylalcohol, ethyl acetate, Lactic acid ethylester, Butanedioic acid,diethylester, isopentylacohol acetate, acetic acid hexylester, acetic acid phenethylester, hexanoic acid ethylester, ethyl caprylate, decanoic acid ethylester, octanoic acid, linalool andα-terpineol were identified in former kiwi wine reports.

本试验首次在猕猴桃酒中发现了油酸乙酯,棕榈酸乙酯,9-癸烯酸,肉豆蔻酸乙酯,月桂酸乙酯,香茅醇,法呢醇,异薄荷酮香气物质,目前国内外资料中报道的猕猴桃酒香气物质—己醇,苯乙醇,丁醇,戊醇,乙酸乙酯,乳酸乙酯,琥珀酸二乙酯,乙酸异戊酯,乙酸己酯,乙酸苯乙酯,己酸乙酯,辛酸乙酯,癸酸乙酯,辛酸,芳樟醇,α-松油醇等均在本试验研究中也检测出,并得到证实。

SM6 and SM7 of uncrystal were analyzed through GC-MS, the results showedthat SM6 main contained unsaturated fatty aldehyde with fragrance, i.e.-2,4-decadienal(58%), tetradecanoic acid (55.78%), 2-decenal(50%), Phthalic acid isobutylundecyl ester(47%), 2, 4-Decadienal(41%), 2-Undecenal (31%), 2-Methyl-Z,Z-3, 13-octadecadi-enol(18.84%), and SM7 contained saturation alkanes, i.e. 1, 2-Benzenedicarboxylic acid, butyl cyclohexyl ester(23.90%), Triacontane(22.63%),Nonacosane(21.04%), Heptadecane(18.84%), Octacosane(13.58%). Toxicological experiments were done to insure the pigment safety.

并对紫红丝膜菌色素非晶体部分的黄色油状物SM6和紫色粉末物SM7作了GC-MS分析,结果显示SM6中主要为具有香气成分的不饱和脂肪醛,其中含量较高的依次为:-2,4-癸二烯醛(58%)、十四烷酸(55.78%)、2-癸烯醛(50%)、邻苯二甲酸异丁基十一烷酯(47%)、2,4-癸二烯(41%)、2-十一碳烯醛(31%)、2-甲基-Z,Z-3,13-十八碳二烯酸(18.45%)等;SM7中主要为饱和直链烷烃,其中含量较高的依次为:1,2-苯二羧酸丁基环己酯(23.90%)、三十烷(22.63%)、二十九烷(21.04%)、十七烷(18.84%)、二十八烷(13.58%)。

The adsorbent is cheap and can be reused after retreacted with steam ,so it is possible to decolorise on the solution of sodium sebacate by this new adsorbent.

同时,在癸二酸生产中排放大量的含酚废水,若不经处理直接排放,不仅会损失大量的原料甲酚,而且会严重污染环境。

The synthetic technologies of three hindered amine light stabilizers were established, the reason for the insoluble side products formed in the production of polymerized hindered amine light stabilizers were studied, and a series of novel hindered amine light stabilizers with antibacterial properties were designed and synthesized in this present paper.1. Based on the investigation of the transesterification between dimethyl sebacate and 1,2,2,6,6-pentamethyl-4-piperinol, the synthetic technologies of Tinuvin292 and Tinuvin 765 were established. The two kinds of hindered amine light stabilizers were obtained in the yield of 93.3% and 92.4% respectively and qualified as the advanced level of the kindred overseas products.2. The synthetic technology of Tinuvin123 was studied and established.

本文研究建立了三个受阻胺类光稳定剂的合成工艺,探索了聚合型受阻胺类光稳定剂生产过程中不溶性副产物产生的原因,并设计、合成了一系列具有抑菌活性的新型受阻胺类光稳定剂。1、在研究癸二酸二甲酯与1,2,2,6,6-五甲基哌啶醇的酯交换反应的基础上,建立了受阻胺类光稳定剂Tinuvin292、Tinuvin765的合成工艺,分别以93.3%和92.4%的收率得到了光稳定剂Tinuvin292、Tinuvin765,所得产品质量达到了国外同类产品的水平。2、研究建立了受阻胺类光稳定剂Tinuvin123的合成工艺。

The components of impurity in sebacic acid from traditional process were analyzed by GC-MS.

采用气相色谱-质谱联用分析确定了传统工艺生产的癸二酸中的主要杂质。

The sebacic acid is a kind of important organic chemical material which can be widely used to produce the polyamide plastics, high temperature lubricant, cold plasticizer, resin and so on.

癸二酸是一种重要的有机化工原料,广泛应用于生产聚酰胺工程塑料、耐高温润滑油、耐寒增塑剂、树脂等方面。

A set of apparatus for determining solid-liquid equilibrium data at atmospheric pressure has been established. The solubility of sebacic acid in water, 20% ethanol aqueous solution, 50% ethanol aqueous solution, 80% ethanol aqueous solution and ethanol were determined. Wilson equation, ideal thermodynamics equation and λh equation were applied to describe solid liquid equilibria data.

建立了一套常压固液平衡测定装置,测定了癸二酸在水、20%乙醇-水溶液、50%乙醇-水溶液、80%乙醇-水溶液、无水乙醇体系中的溶解度,并用Wilson方程、热力学简化方程和λh方程模型对实验数据进行关联。

The results indicated that with this new adsorbent the efficiency of decolourisation was 85.3%and the productivity of sebacic acid was 92.0% under the condition of 2% of adsorbent amount used with 30min of reaction time at 90℃.

本文采用以凹凸棒石粘土为主的新型吸附剂对癸二酸单钠盐溶液脱色。

A thermoplastic biodegradable elastomer was synthesized with propanetriol and sebacic acid by melting cocondensation.

用丙三醇和癸二酸通过熔融共缩聚反应合成了具有一定热塑性、可生物降解的弹性体,并对其结构进行了表征,同时讨论了该弹性体的力学性能、亲水性能和降解性能。

This is a new way for comprehensive utilization of waste fat and oil. The dropping points of lithium grease and lithium-calcium complex grease can be improved through adding the complex additives. Oxalic acid and sebacic acid are effective on lithium grease' and lithium-calcium complex grease' respe...

采用加入复合剂提高锂基润滑脂和锂-钙基润滑脂的滴点,加入草酸复合剂对所制备的锂基润滑脂的滴点的提高最为有效,加入癸二酸复合剂对锂-钙基润滑脂的滴点提高效果最好。

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