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Vapor-liquid equilibrium data for maleic anhydride and its absorption solvents are important for developing and researching the MAN production process. Isothermal VLE data for MAN and di-n-butylsebacate binary system at 413.15, 433.15 and 453.15 K were determined with a modified ebulliometer in this work.

利用改进的沸点仪测定了顺酐-癸二酸二丁酯二元体系在413.15,433.15和453.15 K下的等温气液平衡数据以及纯癸二酸二丁酯和顺酐的饱和蒸气压数据。

By reactions of p-hydroxybenzoic acid with the chlorides of adipic acid, suberic acid, sebacic acid and 1,10-decanedicarboxylic acid respectively four new diacids, and then their dich-lorides, were obtained. The four diacids were found to be thermotropic.

将己二酸、辛二酸、癸二酸、1,10-十二烷基羧酸经酰氯化后,分别与对羟基苯甲酸合成,得到了四种二元羧酸以及与其相应的四种二元酰氯,并发现前者具有热致液晶性。

A small molecule core (TMP-SK3)with three terminal carboxyl groups was synthesized successfully by the reaction of 1,1,1-trihydroxymethylpropane with the excessive sebacic acid diacetic anhydride.

以1,1,1-三羟甲基丙烷与过量癸二酸二乙酸酐反应,制得了端羧基的三官能度小分子核三癸二酸三羟甲基丙烷酯(TMP-SK3)。

Changes of IR group vibrational frequency in the blends of diethyl silicone and se-bacate were studied in this paper. It has been found that there exists an interaction betweendiethyl silicone and sebacate.

研究了乙基硅油与癸二酸酯调和油的IR基团振动频率的变化,发现乙基硅油与癸二酸酯间存在着相互作用。

Firstly, the reactions of glutaric acid, sebacic acid and propargyl alcohol afforded two dipropargylesters:(CH≡CCH_2OCO)_2(CH_2)_3 (compound 1) and (CH≡CCH_2OCO)_2 (CH_2)_8 (compound 2),respectively.

首先,本文分别选用戊二酸,癸二酸与丙炔醇反应得到了两个新的有机二酸二丙炔醇酯:戊二酸二丙炔醇酯(CH≡CCH_2OCO)_2(CH_2)_3(化合物1)和癸二酸二丙炔醇酯(CH≡CCH_2OCO)_2(CH_2)_8(化合物2)。

Liu Yakang Lu Jianmin He Jianyun Jin Guantai College of Materials Science and Engineering, Beijing University of Chemical Technology, Beijing, 100029

引言 环氧基型丙烯酸粉末涂料,通常所采用的固化剂主要有:壬二酸、癸二酸、十二二酸及二十二酸等[1]。

In recent years, the company excellent location advantages, multi-introduction of advanced production equipment and technology to improve old products and develop new products to 12 - hydroxy acid-based rigid and at the same time the production of refined castor oil, hydrogenated castor oil, refined Gan oil, Sebacate methacrylate (annual output 1500 tons), dibutyl sebacate (annual output 1500 tons), octyl sebacate, anhydrous sodium sulfate, castor meal and other products.

近年来,公司以优越的区位优势,多方引进先进的生产设备和技术,改进旧产品,拓展新产品,以 12 -羟基硬质酸为主,又同时生产精炼蓖麻油、氢化蓖麻油,精甘油,癸二酸二甲酯(年产量 1500 吨),癸二酸二丁酯(年产量 1500 吨),癸二酸二辛酯,无水硫酸钠,蓖麻粕等产品。

The inhibition effects of di-(2-ethylhexyl)-sebacate on the corrosion behavior of reinforcing steel bar were investigated by electrochemical polarization curves and electrochemical impedance spectroscopy in simulated pore solution.

采用动电位极化曲线和电化学阻抗谱研究了癸二酸二异辛酯在模拟混凝土孔隙液中对钢筋的保护作用。癸二酸二异辛酯的加入导致混凝土钢筋的腐蚀电位正移,对钢筋的阳极电化学过程有抑制作用。

Abstract— When the solution of sodium sebacate from sebacic acid manufacture is decolorised with activated carbon adsorption,the productivity was low and the cost was high.

由蓖麻油为原料生产癸二酸过程中,传统的脱色工艺是用粉末活性炭吸附,活性炭在脱除溶液中有机色素和混酯的同时,也吸附了部分癸二酸单钠盐,使产品得率较低,生产成本高。

In order to recycle extra caustic soda and increase purity of sebacic acid, the research work in this thesis includes: extra caustic soda recovery, purification of sebacic acid and determination of solubility of sebacic acid in water, ethanol, and ethanol aqueous solution.

但是,它的传统生产工艺中存在过量游离碱浪费,癸二酸产品纯度不高等问题。对此本文做了三方面的研究,包括改进癸二酸生产工艺回收过剩的游离碱;提纯癸二酸;测定癸二酸在乙醇、水、乙醇水溶液中溶解度。

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