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Characterized by a lack of attraction between the colloid medium and the dispersion medium of a colloidal system.

疏液的胶体系统中胶体媒''。'质'。''和分离媒''。'质'。''之间缺乏吸引力特性的

In this paper we combined three chromatographic separation and purification technique such as affinity chromatography, ion exchanger chromatography and hydrophobic interaction chromatography to develope a new technology of stimutaneous extraction of three enzyme from pancreatin. We optimized the technology by studying the methods of purification and assured the technology as: The crude extraction from the dissolution of Pancreatin is directly absorbed on the DEAE gelose fast flow columnEquilibrating buffer is 0.01mol/L NaoAc-HoAc buffer(pH4.5; eluting buffer is 0.2~0.35mol/LNaCl in 0.01mol/LNaoAc-HoAc buffer (pH4.5), and then be eluted by two steps to acquire the peak of kallikrein.The solution which can"t be adsorbed by DEAE gelose fast flow column is adsorbed on affinity chromatographic column Equilibrating buffer is 0.01mol/LTris-HCl buffer(pH7.5, eluting buffer is 0.5mol/LNaCl in 0.01mol/Ltris-HCl buffer(pH7.5)and then be eluted by one step to acquire the peak of trypsin.The solution which can"t be adsorbed by is pretreated with 30%~80%(NH_4)_2SO_4 fractional precipitation, the deposition of the precipitation is dissolved to beabsorbed on phenyl gelose fast flow columnhydrophobic interaction chromatography condition is Equilibrating buffer is lmol/L(NH_4_2SO_4 in 0.01mol/LNaoAc-HoAc buffer(pH4.5), eluting buffer is 0~0.6mol/L(NH_4)_2SO_4 in 0.01mol/LNaoAc-HoAc buffer (pH4.5) and then be eluted by two steps to acquire the peak of chymotrypsin.

本研究考察了各种纯化方法,将离子交换层析、亲和层析和疏水层析三种分离纯化法相结合,建立了激肽释放酶、胰蛋白酶和糜蛋白酶三酶的联产工艺:胰酶用pH4.5醋酸缓冲溶液提取后,粗提液直接上DEAE-琼脂糖快胶柱吸附平衡缓冲液:0.01mol/LNaoAc-HoAc缓冲液(pH4.5,洗脱缓冲液:0.01mol/LNaoAc-HoAc缓冲液(pH4.5)含0.2~0.35mol/LNaCl分两步洗脱,收集激肽释放酶的洗脱峰;DEAE-琼脂糖快胶的未吸附液上亲和层析柱分批吸附平衡缓冲液:0.01mol/LTris-HCl缓冲液(pH7.5,洗脱液:0.5mol/LNaCl溶液,一次洗脱,收集胰蛋白酶洗脱峰;最后,亲和层析未吸附液用30%~80%硫酸铵分级盐析处理,沉淀溶解后用上苯基—琼脂糖快胶吸附平衡缓冲液:0.01mol/LNaAc-HAc缓冲液(pH4.5含1mol/L(NH_4)_2SO_4,洗脱缓冲液:0.01mol/LNaAc-HAc缓冲液(pH4.5)含0~0.6mol/L(NH_4)_2SO_4,分两步洗脱,收集糜蛋白酶的洗脱峰。

In order to resolve the repeatability of contact angle measurement, the factors such as droplet volume, measure time, hydrophilic and hydrophobic targets were studied by using deionized water on glass and paraffin surface.

针对喷雾液滴在靶标上接触角测量的重现性不佳等问题,以玻璃和石蜡模拟靶标表面,研究了去离子水在亲水和疏水靶标表面上液滴体积和测量时间对接触角测量的影响,结果表明:液滴体积越大接触角越小,这种趋势在亲水表面比疏水表面上更突出,测量时体积可分别选择在0.5~1μl和1~5μl;液滴滴下30-50s后与固体表面基本达到平衡,对接触角测量的准确度影响较小。

The fact that spin-label molecules exchange between free water and hydrophobic region was proved by ESR, the arrangement of surfactant chains become loose in the process of hydration and water can penetrate into hydrophobic region of reverse microemulsion.

ESR结果也说明探针分子在反相微乳液的自由水及疏水环境间交换,在水化过程中表面活性剂链的排列较为疏松,且水分子渗透到反相微乳液的疏水区域。

Lever Ball Float Steam Traps biggest advantage is not subject to pressure,temperature,cooling water flow fluctuations,continuous drainage,a water that row,the minimum cooling degree 0℃,能使best efficiency heating equipment;lever float steam trap valve seat total in the following level,forming awater seal,no steam leakage;itsPlug Valves minimum working pressure 0.01Mpa,the maximum back pressure rate of≤85%;interior with exhaust,lever float steam traps use the most advanced components as the automatic emptying of diaphragm valves,can automatically exclude non-condensing gas,very sensitive,high quality work and long service life.

杠杆浮球式蒸汽疏水阀的最大优点是不受压力、温度、冷凝水流量波动的影响,连续排水,有水即排,最小过冷度为0℃,能使加热设备达到最佳工作效率;杠杆浮球式蒸汽疏水阀的阀座总处于液位以下,形成水封,无蒸汽泄漏;它的最低工作压力0.01Mpa,最大背压率≤85%;内部带有排气装置,杠杆浮球式蒸汽疏水阀采用最先进的膜盒元件做为自动排空气阀,能自动排除不凝结气体,非常灵敏,工作质量高,使用寿命长。

A micro-monolithic column was prepared by in-situ free radical polymerization of stearyl methacrylate with ethylene glycol dimethacrylate in the presence of the initiator AIBN and a mixture of porogens including iso-amyl alcohol and 1,4-butanediol.

以甲基丙烯酸碳酰十八酯为单体,乙叉二甲基丙烯酸酯为交联剂,异戊醇和1,4-丁二醇为二元致孔剂,偶氮二异丁腈为引发剂,原位制备了具有强疏水性的SMA整体微柱,并利用此整体微柱在普通高效液相色谱仪上测定滴眼液中氧氟沙星的含量。

The sizes of the self-assembly micelles of the amphiphilic block copolymers and the effects werestudied by dynamic light scattering and UV-visible spectrophotometer. The micelle sizes werelargely influenced bythe hydrophobic chain content in the copolymer, the properties of the solvent and the copolymer concentration in the organic phase. The morphology of the micelles was investigated by transmission electron microscopy. Theresults showed that the micelles appeared spheres with inner core and outer shell. The critical association concentrations were determined by pyrene monomer fluorescence probe technology. The degradability of copolymer was studied by the loss of the intrinsic viscosity in the degradation process. The results indicated that the degradation rate of PECL was slower thanthat of PELLA and PEDLLA. The stability of the copolymer micelle dispersion was examined by measuring the critical flocculation concentration, which gradually decreased with increasing the content of thehydrophobic chain in the copolymer. The rheological results showed thatthe viscosity ofthe micelle dispersion with higher content of PEG segments was firstly decreased and then increased with the increasingthe temperature. Otherwise, the variation of viscosity was irregular. The viscosity of the micelle dispersion increased with the increase of the electrolyte (Na 2SO 4) concentrations. Polymer micelles paclitaxel was prepared by self-emulsification/solvent evaporation method and solid dispersion technique with amphiphilic block polymers as the carrier material.

运用动态光散射和紫外分光光度计研究了两亲性嵌段共聚物自组装胶束的粒径及其影响因素,结果表明,自组装胶束的形成机理受制备方式的控制,胶束的粒径随着共聚物相对分子质量或疏水嵌段相对分子质量和有机相中共聚物浓度的增大而增大,随着有机溶剂的水溶性的增强而减小;采用透射电镜观察胶束的形态结构,发现胶束呈具有核壳结构的均匀球形;采用芘荧光探针法测两亲性嵌段共聚物的临界聚集浓度;通过降解过程中共聚物特性粘度的变化研究两亲性共聚物的降解性能,发现与PELLA和PEDLLA的相比,PECL 降解速率较慢;随着共聚物中疏水嵌段含量的增大,纳米分散液的稳定性逐渐下降;PEG含量高的PEDLLA纳米分散液随着温度的升高,纳米分散液的粘度先下降然后增大,反之,没有规律性,且随着电解质Na 2SO 4浓度的增大,体系粘度增大。

The effect of the special monomers on the properties of the emulsion was studied. The results showed that when the amount of GMA was 4.4% and the amount of actyflon was 1.0% of the monomers, salt spray resistance of the emulsion, could be up to 240 h without rust spots and babbles.

结果表明,当环氧单体甲基丙烯酸缩水甘油醋用量为总单体用量的4.4%,含氟单体用量为总单体用量的1.0%时,能够显著提高乳液的交联度和疏水性,乳液成膜后进行中性盐雾实验,中性盐雾时间可达到240h,板面无锈点,主体无起泡。

Lever Ball Float Steam Traps are not subject to the greatest advantage of pressure, temperature, condensate water flow fluctuations, continuous drainage, water that is exclusive, the Butterfly Valves minimum undercooling of 0 ℃, heating equipment can achieve the best efficiency; Lever Ball Float Steam Traps seat total in the level below, the formation of water seal, no steam leakage; its minimum working pressure 0.01Mpa, the biggest back-pressure rate of ≤ 85%; house with an exhaust device, lever float steam trap uses the most advanced components as the automatic emptying of diaphragm valves, can automatically rule out non-condensing gas, very sensitive, high-quality work and long service life.

杠杆浮球式蒸汽疏水阀的最大优点是不受压力、温度、冷凝水流量波动的影响,连续排水,有水即排,最小过冷度为0℃,能使加热设备达到最佳工作效率;杠杆浮球式蒸汽疏水阀的阀座总处于液位以下,形成水封,无蒸汽泄漏;它的最低工作压力0.01Mpa,最大背压率≤85%;内部带有排气装置,杠杆浮球式蒸汽疏水阀采用最先进的膜盒元件做为自动排空气阀,能自动排除不凝结气体,非常灵敏,工作质量高,使用寿命长。

A printing plate fountain solution dasage is too large, oleophilic hydrophobic organic polymer film would have been destroyed, so that the pictures and texts not fully been adsorption ink, fountain solution encroachon, gradually build superhydrophilic and necleophilic of inorganic salt layer, hydrocolloid layer become superhydrophilic acattered guease basis, resulting in a printing plate version.

印版润版液用度功不小,干油疏火的无机矮不不合子膜层不离会被爱护,使图文局部不克不及充不不合吸附油不朱,而被润版液霸占,忽然天生干火的无机盐层和干火胶体层,成为干火疏油的本原,变成印版&花版&。

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