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This may be taken as a result of electrolysis.

这可以当作是电解的一种结果。

The influence of electrolyte solution pH, electrolysis current and time on the analysis result has been researched respectively.

分别考查了电解液pH值、电解的电流和时间对分析结果的影响。

With the rapid development of the technology of computer and automation, and the demand of the product locale, the computer control system is widely used in the manufacture of aluminum electrolytic and the efficiency is improved and the life-span of the aluminum electrolytic cell is increased.

随着计算机和自动化技术的发展,以及生产现场的需求,以计算机为核心的自动控制系统已经被广泛地应用于铝电解的生产过程控制,提高了铝电解的生产效率、延长了电解槽寿命。

According to the characteristics of high-nickel copper cathode electrolyzation,an analysis is made on the factors of the electrolyte that impacts the surface quality of tough cathode ,and some suggestions are put forward for improving the quality of tough cathode .

针对高镍铜阳极电解的特点,分析研究了电解液对阴极铜质量产生影响的因素,提出了改善阴极铜质量的有关建

The anodic gases composition in neodymium electrolysis in the cases of both normal electrolyzing process and anodic effect happening state was analyzed by means of Orsat analyser and chromatographymass spectrography technique, and the effects of temperature and anodic current density on it were discussed, the final reaction equation was figured out.

摘 要:用Orsat气体分析器和色谱质谱联用仪研究了正常电解和发生阳极效应时钕电解的阳极气体成分,探讨了温度、阳极电流密度等对阳极气体组成的影响,计算了钕电解的总反应方程式。

Preparation of the cathode includes:shaping under the press of 40Mpa, sintering at 550℃for 1 hour and at 900℃for 8 hours and threading with molybdenum bar; Considering the literatures we choose CaCl2 as salt for preparation titanium. Pretreatment of salt is for 1 hour at 100℃and for 2 hours at 300℃. Partial pressure of oxygen which need lower than 5.11×10-7Pa to reduct titanium oxides and hygroscopic property of salt need a sealed equipment to electrolyse. And finally successfully designed a satisfied one and the results show that the equipment can be satisfied the requirment of the experiment. Flow of the inert gas is 1.5L/min, the voltage is 2.8 V, temperature is 850℃and time is 2 hours during pre-electrolysis. Flow of the inert gas is 0.2L/min, the voltage is 3.1 V, temperature is 900℃and time changes with the mass of TiO2 during electrolysis, namely the greater need the longer time; To eliminate influence of salt and other impurities, the products need to wash with distilled water and dilute chlorhydric acid , then wash with dilute hydrochloric acid under supersonic wave assistant. Finally, electrometical properties of the electrolysis of TiO2 is researched by cyclic voltammetry and chronoamperometry, and results show that there are two main reodox steps, namely from TiO2 to TiO and from TiO to Ti.

阴极制备主要包括40MPa压力下模压成型、两段式烧结(1小时内升至550℃保温1小时,再1小时升温至900℃保温8小时)及烧结后TiO2块打孔用钼棒串接三个主要环节;实验中选用CaCl2作为电解熔盐,并对其进行预处理(100℃,保温1小时; 300℃,保温2小时);经热力学计算,还原钛氧化物的氧分压至少要低于5.11×10-7Pa,结合电解过程中所用熔盐CaCl2有极强的吸水性的特点,电解装置应有较高的密封性,自行设计了一套密封性可靠的电解装置,便于实验过程中熔盐预处理和氧分压的控制;通过干燥处理预电解过程中Ar流量大约为1.5L/min、电压为2.8 V、温度为850℃、时间为2小时,电解过程中Ar流量大约为0.2L/min、电压为3.1V、温度为900℃,实验结果表明电解时间与TiO2质量密切相关,质量越大需要电解的时间越长;通过自来水冲洗—稀盐酸浸泡、洗涤—在超声波辅助作用下稀盐酸洗涤,可减少熔盐及其它杂质对电解产物检测结果的影响;最后,通过循环伏安法、计时电流法对电解机理的研究,确定电解还原TiO2制备金属钛主要经历了TiO2-TiO-Ti的过程。

This paper introduces the technical condition of electrorefine high-nickel and high-sulphur copper anode and analyzes the problem and the reason in the practise.

介绍了高镍高硫铜阳极电解的技术条件,分析了电解过程中产生的问题及其原因,提出了解决的对策。

The conclusion is drawn that if the content of fluosilicic acid in wet-process phosphoric acid is less than 0.19% or the content of dialuminium trioxide in wet-process phosphoric acid is less than 1.47%, the elctrolysis would go on wheels.

另外,本文探讨了湿法磷酸中单一杂质对电解的影响,并得出只要氟硅酸含量低于0.19%、Al2O3含量低于1.47%时,电解就能够顺利进行。

From the coupled simulation optimization result analysis, the 10KA drained cathode rare earth electrolysis cell may be used trying to produce in the rare earth electrolysis industry, the new direction for the new rare earth electrolysis cell structure research has been opened.

从仿真优化结果分析,该槽型可以用于稀土电解的工业试生产,这为新型稀土电解结构的研究开辟了新方向。

After the research of anodic oxidation slag, we got the composition of the suspension electrolyte of zinc sulphate solution. 2 The results of electrode kinetic of anodic oxidation showed that the electron transfer during the process of electrochemical oxidation was 1, and the electrochemical mechanism was: ZnS=Zn~(2+)+S~-+e Zn~(2+)+2S~-=ZnS + S~0 3 The flow sheet which can produce zinc according to suspension electrolysis principle in industry was put forward. 4 Elemental sulfur in oxidizing slag was recovered by distillation.

本文的创新点是: 1提出了以硫酸锌溶液为基础的悬浮电解液体系;通过对阳极氧化渣进行系统的分析研究,得出了硫化锌矿物的悬浮电解的电解液组成; 2通过阳极氧化电极过程动力学分析得到,电化学氧化过程中电子转移数为1,电化学机理为: ZnS=Zn~(2+)+S~-+e Zn~(2+)+2S~-=ZnS+S~0 3提出了工业上利用悬浮电解原理生产金属锌的工艺流程; 4对氧化渣中的元素硫采用蒸馏法原理进行回收。

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