电子衍射

In this paper,acetanilide,adipic acid and potassium hydrogen phthalate were chosen as additives to advance polyvinyl chloride to crystallize. The effects of compress mold,annealing temperature and time,additive property and loading on the crystallization,microscopicmorphology and mechanical properties of PVC were studied by means of wide angle X-ray diffraction,differential scanning calorimetry,fourier transform infrared spectrophotometer,scanning electron microscopeand tensile test.

本文利用乙酰苯胺、己二酸和邻苯二甲酸氢钾作为聚氯乙烯结晶改性的添加剂，通过广角X-射线衍射法、差示扫描量热法、傅立叶转换红外光谱、扫瞄电镜和万能电子实验机研究了热压、热处理温度和时间、添加剂结构和质量分数对PVC结晶、微观形态和宏观机械性能的影响。

Through electron probe\'s analysis to the albite jade, union grinding sample thin slice under polarizing microscope observation as well as X powder crystal diffraction data analysis. Discovery like Chen zhenqiang and "System Gemology" said that secondary mineral for actinolite, green mudstone, epidote and quart.

通过对钠长石玉进行电子探针的分析，结合磨制的样品薄片在偏光显微镜下的观察以及X粉晶衍射数据分析，可知钠长石玉中的主要成分为钠长石，次要矿物为硬玉、角闪石、绿辉石、钠铬辉石；并未发现如陈振强等人以及《系统宝石学》中所说的次要矿物为阳起石、绿泥石、绿帘石、石英。

In current study, the laser shock processing technique of high energy and short pulse duration is adopted. The substructural transformation characteristics and mechanisms of 2Cr17Mn15Ni2N austenitic stainless steel, subjected to ultra-high strain-rate and impact stress in excess of dynamic yield strength of the target, are investigated by scanning electron microscope, X-ray diffraction and transmission electron microscope technology.

采用高能短脉宽激光冲击加载技术，利用扫描电子显微镜，X射线衍射和透射电子显微镜等手段，研究了在激光诱导的超高应变率和高于材料动态屈服强度冲击加载条件下，2Cr17Mn15Ni2N奥氏体不锈钢表面亚结构的转变特征和机制。

The fretting wear experiments were made on nitrogen imp-larted samples and unimplanted samples of 9Crl8Mo steel respectively in this in vestigation. SEM was used to observe the topography of the fretted surfaces. AES and micro-region X-ray diffraction were also used to deter mine the elements distribution and phase construction of the implanted surface tilm and wear track surface.

作者对9Cr18Mo钢的氮离子注入试样及未注入试样进行了微动磨损的对比试验，利用扫描电子显微镜对磨损表面的形貌进行了观察，利用俄歇电子能谱仪和微区X-射线衍射仪对氮离子注入试样表面与磨损表面的元素分布及相组成进行了分析。

The morphology, structure and composition of the final nano-products were characterized by scanning electron microscope, energy-dispersive spectroscope and x-radial diffraction analysis.

采用扫描电子显微镜、X射线衍射、EDS能谱仪和透射电子显微镜对其表面形貌、结构和成分进行分析，结果表明所得纳米线为In2O3。

To study high temperature corrosion behavior on materials during solid waste incineration, laboratory corrosion tests were performed to iron, cast iron, 20# carbon steel, stainless steel in oxidizing gaseous environments which included O〓, SO〓, H〓O, HCl, Cl〓and some ashes coming from self-designed incinerator, the Xunde's one and synthetic ashes. The synthetic ashes are used as corrodents composed of chlorides , sulfates and oxides.

最后，本论文为揭示材料垃圾焚烧过程中的高温腐蚀行为，借助于腐蚀重量实验，X-射线衍射仪，扫描电子显微镜，电子能谱等分析测试手段，研究了铁、铸铁、20#碳钢和不锈钢在垃圾焚烧环境中的高温腐蚀行为及腐蚀动力学。

In this work, nanostructure samples of La1-xCaxMnO3（x=0.2、0.3、0.4、0.5）were prepared by hydrothermal-precipitation method . The structural characterization of the powder samples were done by X-ray diffraction. XRD patterns showed that all the samples ate single perovskite-type phase withoutother impurity or secondary phase. The shape and size of samples were performed on Scanning Electron Microscopy. SEM photographs investigated that temperature of hydrothermal effects the phase of samples and alkalinity of the reaction mixture by ΔTad-T curve measurement device at low magnetic fielded

本论文采用水热共沉淀退火法制备了La1-xCaxMnO3（x=0.2、0.3、0.4、0.5）系纳米结构，用X射线衍射仪确定产物为单相钙钛矿结构，无任何杂峰及第二相；用扫描电子显微镜与透射电子显微镜分析了产物的大小和形貌，发现水热温度对产物的形成起决定作用，随着温度的升高，产物由薄膜状向丝状转变，而溶液的碱度可控制产物的形貌和大小，当碱度为6.35mol/L，水热温度为240 C时，La0.6Ca0.4MnO3的主要形貌为纳米丝并有少量纳米颗粒，纳米丝平均直径为40nm；最后测量了粉末样品在低磁场（1.4T）下的磁热效应，发现水热共沉淀退火法制备样品的最大绝热温度明显高于球磨法制备样品的最大绝热温变。

Electron microscope of the scheme of chart of X ray diffraction that analyses composite material, transmission and photograph of scanning electron microscope make clear: OMMT basically is with coming off condition disperses in PLA matrix, form in order to come off model give priority to, the accept rice that at the same time existence inserts a structure composite material, the affiliation of OMMT makes the drawing section of composite material ruptures to tenacity by brittleness change.

分析复合材料的X射线衍射谱图、透射电子显微镜和扫描电子显微镜照片表明：OMMT主要以剥离状态分散在PLA基体中，形成以剥离型为主、同时存在插层结构的纳米复合材料，OMMT的加入使复合材料的拉伸断面由脆性断裂向韧性断裂转变。

In order to disclosure the reason why the electrocatalysis activeness and selectivity droped after being used several hundred hours continuously, the x-ray diffraction, scanning electron microscopy and energy dispersive spectroscope have been used to characterize the surface condition variations of Monel metal. The results indicated: Monel metal belongs to the Cu-Ni alloy around the electrolysis experiment.And after being used for 600hr, the surface layer element composition and geometry distribution of the alloy changed, namely in the alloy the Cu element /which superficial free enthalpy was smaller,"concentrated" to the alloy surface,and formed one kind of marble structure microcrystallite.Thus the electrode surface becamed rough a

为了揭示蒙乃尔合金阴极在连续使用数百个小时后电催化活性剂选择性下降的原因，采用X射线衍射仪、电子扫描电镜和电子能谱分析仪对电解实验所用的蒙乃尔阴极材料在电解实验前后的表面状态进行了表征，结果表明：所使用的蒙乃尔合金阴极材料在电解实验前后均属于Cu-Ni合金，使用600hr后，由于表面层元素组成和几何排布发生了变化，即合金中表面自由焓较小的Cu元素向合金表面&富集&，形成一种大理石结构的微晶，表面粗糙、不均一，这是造成其对硝基苯电还原的催化活性及选择性随着使用时间延长而逐渐下降的主要原因，同时也为此类电极的修饰改进提供了方向。

The article introduced the measuring technique of the grain size of ceramic alpha alumina, including electronic microscope, Laue X-ray diffraction, nitrogen absorption specific surface area, infrared spectra and grinding method.

本文介绍了电子显微镜、X射线衍射、氮吸附小比表面法、红外光谱结构分析、研磨法等用于陶瓷氧化铝晶粒度测定的情况，通过对比，指出了电子显微镜能够真实地反映微观世界，是多种分析方法的基

With Death guitarist Schuldiner adopting vocal duties, the band made a major impact on the scene.

随着死亡的吉他手Schuldiner接受主唱的职务，乐队在现实中树立了重要的影响。

But he could still end up breakfasting on Swiss-government issue muesli because all six are accused of nicking around 45 million pounds they should have paid to FIFA.

不过他最后仍有可能沦为瑞士政府&议事餐桌&上的一道早餐，因为这所有六个人都被指控把本应支付给国际足联的大约4500万英镑骗了个精光。