电子衍射

The filled skutterudite compound possesses bcc structure as evidenced by electron diffraction analysis. Powder X-ray diffraction data of filled skutterudite samples were characterized by Rietveld method for some crystallographic parameters such as lattice constant, atomic occupation, atomic position, etc.

另外，通过对化合物电子衍射的分析证实了〓化合物是一种具有bcc结构的化合物；运用Rietveld方法对填充skutterudite化合物X衍射谱线进行了分析，对化合物的晶格常数、原子位置的占有率以及原子位置坐标等晶体学参数进行了表征。

The structure and chemical compositions of the surface oxide film were investigated by XRD and Auger electron spectrometry.

利用X射线衍射和俄歇电子衍射观察了表面膜的化学成分及结构。

The crystalline phase of the nanocrystalss is the cubic zine blende, consistent with the results of X-ray diffraction and selected area electron diffraction.

电子衍射、高分辨电镜晶格像和X-射线衍射对纳米晶的晶体结构进行了表征，结果都证实ZnSe纳米晶的结构为闪锌矿结构。

We can say that neutron scattering is an important and necessary complement for X-ray diffraction and electronic diffraction.

中子散射可以说是对X射线衍射和电子衍射的一个重要的和不可缺少的补充。

The results of XRD and ED show that the crystal structure of CdSquantum dots synthesized in water solution is wurtzite structure.

通过X射线衍射谱、电子衍射花样的研究表明：水溶液法制备的CdS量子点纳米晶体具有纤锌矿的晶体结构。

The crystallitic carbon was prepared from anthracite by demineralization and carbonization,then the magnesium/carbon nanocomposites for hydrogen storage were manufactured through reaction milling of the mixture of magnesium,crystallitic carbon and aluminium under hydrogen atmosphere.

将无烟煤进行脱灰和碳化，制备微晶碳，再将微晶碳和铝添加到镁中，用氢气反应球磨法制取镁/碳纳米复合储氢材料。用透射电子显微镜、选区电子衍射、X射线衍射和差示扫描量热分析对储氢材料的粒度、晶体结构和放氢温度进行了测定。

In the Secondone,we presented a simple and expedient electrolytical reductionmethod to grow molybdenum blue bronze crystals from salts melts.The structure and composition were verified by single-crystal X-raydiffraction and XPS electron-probe analysis.

通过XPS和四园单晶X-射线衍射方法对单晶成份和结构，利用汇聚束电子衍射和STM方法对单晶的群对称性及表面电子结构进行分析研究，结果表明：生长的单晶具有高质量，且与国外制备的单晶一致，给进一步深入的研究工作提供了可靠的依据。

Provided are carbide derived carbon materials prepared by thermochemically reacting carbide compounds and a halogen containing gas and extracting all atoms of the carbide compounds except carbon atoms, wherein the intensity ratios of the graphite G band at 1590 cm -1 to the disordered-induced D band at 1350 cm-1 are in the range of 0.3 through 5 when the carbide derived carbon is analyzed using Raman peak analysis, wherein the BET surface area of the carbide derived carbon is 1000 m 2 /g or more, wherein a weak peak or wide single peak of the graphite (002) surface is seen at 2 = 25 DEG when the carbide derived carbon is analyzed using X-ray diffractometry, and wherein the electron diffraction pattern of the carbide derived carbon is the halo pattern typical of amorphous carbon when the carbide derived carbon is analyzed using electron microscopy.

提供了得自碳化物的碳，其通过热化学反应碳化物化合物和含卤族元素的气体并提取除了碳原子之外的碳化物化合物的全部原子制备，其中当使用拉曼峰分析法分析该得自碳化物的碳时，在1590cm -1 的石墨G波段与在1350cm -1 的无序引发的D波段的强度比为0.3至5，其中该得自碳化物的碳的BET表面积是1000m 2 /g或更大，其中当使用X射线衍射法分析该得自碳化物的碳时，在2θ＝25°观察到石墨(002)面的弱峰或宽单峰，以及其中当使用电子显微法分析该得自碳化物的碳时，得自碳化物的碳的电子衍射图是代表无定形碳的晕图案。该发射体具有良好的均匀性和长寿命。可以使用比用于生产常规碳纳米管的方法更廉价的方法制备发射体。

In this dissertation,Co-Cr2O3 and Fe-Cr2O3 granular films with superiorproperties have been successfully fabricated by RF co-sputtering technique underroom and 77K substrate temperatures for the first time.The microstructure,electrical transport and magnetic properties as well as their relation to TMR effectare systematically investigated by various techniques such as X-Ray diffraction,transmission electron microscopy,electrical diffraction,X-Rayphotoelectron spectroscopyand VSM,etc.,the change of electrical transportand magnetic properties in these films with their microstructure is also shown.Someinteresting and valuable results have been obtained after the theoretical fitting ofexperimental data with the existed theory.The temperature dependence of TMReffects in these films and the way to get larger TMR effect is also studied.Our mainprincipal results obtained are as follows:(1)Microstructure and Magnetism

在本论文中，我们采用射频共溅射方法，在室温及77K的衬底温度下首次成功地制备了性能优异的Co-Cr2O3及Fe-Cr2O3系列颗粒薄膜，并利用X-Ray衍射、透射电镜、电子衍射、X-Ray光电子谱及宏观电性及磁性测量等手段详细地研究了Co-Cr2O3颗粒膜的微结构、电性、磁性及它们与TMR效应之间的关系，系统地研究了薄膜的电性和磁性随薄膜微结构的变化，通过实验数据点的理论拟合，得出了一些有价值的物理信息，探讨了磁电阻效应的温度依赖性及获得较大TMR效应的途径，主要内容可概括如下

The resolution index of electron diffraction in TEM is analyzed. The exactly experimental method is given for demarcating electron diffraction camera length by Gold-monocrystal in TEM.

同时对TEM中的电子衍射分辨率指数进行了分析和讨论，并给出了实际应用金单晶标样精确标定TEM电子衍射相机长度的实验方法。

With Death guitarist Schuldiner adopting vocal duties, the band made a major impact on the scene.

随着死亡的吉他手Schuldiner接受主唱的职务，乐队在现实中树立了重要的影响。

But he could still end up breakfasting on Swiss-government issue muesli because all six are accused of nicking around 45 million pounds they should have paid to FIFA.

不过他最后仍有可能沦为瑞士政府&议事餐桌&上的一道早餐，因为这所有六个人都被指控把本应支付给国际足联的大约4500万英镑骗了个精光。