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电子衍射

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The phase compositions and the microstructures of the samples were investigated by an X-ray diffractometer and a scanning electron microscope, respectively.

利用X射线衍射仪和扫描电子显微镜分别对试样的相组成和显微结构进行分析。

MAIN OUTCOME MEASURES: At 1, 3, 5, 7, 14 days following immersion, microstructure of the sample surface was observed using scanning electron microscope. The structure of composite was analyzed utilizing X-ray diffractometer.

主要观察指标:于浸泡1,3,5,7,14 d后采用扫描电子显微镜观察样品表面形貌的显微结构,复合材料的结构采用X射线衍射仪进行表征。

Molecular model of the amino acid tyrosine with experimental electron density in front of an X-ray diffractometer at MIT.

根据实验数据绘制出电子密度分布的酪氨酸分子模型,它后面的仪器就是麻省理工学院的一台X射线衍射仪。

The resultant particles were characterized by X-ray diffractometer and scanning electron microscope.

用X射线衍射仪测定出产物的相结构,用扫描电子显微镜观察产物的微观结构。

Microstructure,change of phase, distribution and morphology of oxide were analysed by X ray diffractometer,scanning electron microscope and optical microscope.

用 X射线衍射仪、电子探针和金相观察分析了粉末氧化前后相的转变、氧化物的分布、形貌。

The structural evolution of Mo33Si66 element powders in the process of mechanical alloying and subsequent heat treatment was studied by X-ray diffractometer and transmission electron microscope.

用X射线衍射和透射电子显微镜研究了Mo33Si66混合粉在机械合金化以及热处理过程中的结构演变,并讨论机械合金化过程中的相形成机理。

The distribution of temperature stress was calculated by finite element analysis. The results showed when the surface temperature of concrete was higher than 110℃, the temperature stress was more than 4 MPa without regard to the creep. This might be lead to the damage of the surface of concrete. At the same time, a lot of microstructure analysiss such as XRD, SEM, IR, HSA etc. were done to analysis the difference of the component and microstructre of concrete before and after corrosion. The results indicated that the decomposion of CSH gel and calcium hydroxide and the creation of dilatability calcium oxide were the internal reason of the deterioration of concrete in the corrosion form of high heat.

该文通过有限元方法计算了由于温度而产生的结构应力分布,计算结果表明当混凝土表面温度超过110℃时,如不考虑徐变时表层混凝土受到的温度应力将超过4MPa,这使得表层混凝土很容易因温度应力而破坏;同时通过X射线衍射分析、扫描电子显微分析和混凝土孔结构分析等多种微观结构测试手段,分析了混凝土受热前后的宏观性能以及微观组成和结构的变化,指出混凝土原水化产物如水化硅酸钙凝胶和氢氧化钙的分解以及膨胀性产物氧化钙的产生是高热腐蚀形式下混凝土破坏的内在原因。

The products are characterized by scanning electron microscopy, X-ray diffraction and energy dispersive spectroscopy.

用X-射线衍射、扫描电子显微镜和能谱对产物进行表征。

We used XRD, EDS and other methods to study different samples.

并采用X射线衍射仪、场发射扫描电子显微镜等方法对不同烧结温度的羟基磷灰石靶材进行检测研究。

Through the study of metallographic specimen and the inclusions through electrolyzation under SEM, it is indicated that the Ti-deoxidized products are globular compound inclusions with the size of 1~3μm in this experiment condition. With the technical of ion beam thinner the inner structure of these inclusions can be observed, whose core is Ti-O and outer is Mn-S. Based on EBSD the phase composition has been analyzed and it indicated that these globular compound inclusions are Ti2O3 and MnS with nucleating center Ti2O3, which can prompt to nucleate IGF.

在扫描电镜下通过对金相试样和电解提取的夹杂物研究表明,本实验条件下钢液凝固过程中析出的夹杂物是Ti-O-Mn-S形成的尺寸为1~3μm的球形复合夹杂物;通过离子减薄后观察了夹杂物的内部结构,中心是Ti-O化合物,外围是Mn-S化合物;通过电子背散射衍射对夹杂物的物相组成的分析表明了该复合夹杂物是有利于针状铁素体形核的Ti2O3和在凝固过程中以Ti2O3为核心形核的MnS。

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