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In addition, molecular orientation behaviors induced by shearing, electric field and magnetic field were investigated. The space group of the monomers A3EO7 and A9EO7 were determined as P2〓2〓2 and P112/m by means of electron diffraction and X-ray diffraction. Liquid crystalline properties of the monomer and the polymer were studied using DSC, variable X-ray diffraction, TEM and polarized optical microscope. Both monomers exhibit monotropic liquid crystalline behavior, and they also give a metastable phase on the cooling process. The polymer PA9EO7 shows enantiotropic liquid crystalline properties. Thus the rigid polymer backbone is not a fatal defect that completely distorts the packing arrangement of the mesogenic moiety in the side chain liquid crystalline polyacetylene.

结合电子衍射倾转方法和粉末X射线衍射技术,确定了两个液晶小分子A3EO7和A9EO7的晶胞参数和空间群,采用Cerius〓模拟软件,运用分子模拟的方法给出了小分子在晶胞中的排列方式;利用DSC、变温X射线衍射技术和透射电子显微镜研究了小分子和聚合物的液晶态,单体A3EO7和A9EO7表现出单向液晶性质,并且在降温过程中都表现出一个亚稳液晶相或亚稳结晶相,聚合物PA9EO7具有双向液晶性;采用偏光显微镜和X射线平板照相技术,研究了剪切和电场对聚合物分子取向的影响,在不同的液晶态,剪切作用对聚合物PA9EO7具有不同的诱导取向结果,直流电场可以诱导聚合物联苯液晶基元沿施加电场方向取向。

The article simply intrduces the working principle of Scanning Electron Microscope,and dis-cusses the application of Scanning Electron Microscope with EDS in gemmology to the identify gems , synthetic gems and optimizing gems and so on.

本文简要介绍了扫描电子显微镜的工作原理,并结合能谱仪,探讨了扫描电子显微镜在宝石学中鉴定天然宝石与合成宝石及优化宝石等方面的应用。

The products were characterized by X-ray diffraction, scanning electron microscopy, transmission electron microscopy and thermal gravimetric analysis.

采用X射线衍射仪、傅里叶变换红外光谱仪、扫描电子显微镜、透射电子显微镜和热失重分析仪等对产物的组成、形貌以及热失重情况进行了表征。

A suspension of carbon nanotubes as a nanofluids was prepared by dispersing carbon nanotubes into deionized water. The effects of several typical kinds of surfactants such as sodium dodecyl benzene sulfonate, hexadecyl trimethyl ammonium bromide and emulsifying agent OP on the stability of the nanofluid were studied by stationary and centrifugal tests with sample morphologies characterized by SEM and TEM.

在水中加入碳纳米管制备了含碳纳米管悬浮液,研究了几种典型类型的表面活性剂:十二烷基苯磺酸钠、十六烷基三甲基溴化铵及乳化剂OP对纳米流体稳定性的影响,通过静置和离心分离等手段研究了其稳定性,并采用扫描电子显微镜和透射电子显微镜对样品的形貌进行了表征。

Electroplating with ultrasonic agitation was used to deposit these composite coatings. The composite coatings were observed with SEM and TEM. It was observed that carbon nanotubes and carbon nanofibers were distributed homogen eously and embedded tightly in the Ag matrix, in additio...

通过扫描电子显微镜和透射电子显微镜进行观察,证明碳纳米管及碳纳米纤维能够均匀分散到Ag基体中并实现良好结合,其中,Ag更在碳纳米管表面外延生长,形成了有效的界面结合。

The ultrastructure of spermatozoa of Takifugu xanthopterus was observed by means of scanning electron microscopy and transmission electron microscopy.

在透射电子显微镜及环境扫描电子显微镜下观察黄鳍东方鲀精子的超微结构。

Carbon nanocoils were in situ synthesized by the flame combustion of ethanol using stannic chloride as catalyst precursor. The morphology and structure of CNCs were characterized by means of scanning electron microscope, transmission electron microscope, X-ray diffraction and Raman spectrum.

采用乙醇火焰燃烧,借助于基板材料上涂敷锡盐作为催化剂前驱体,制备了螺旋结构碳纳米纤维;借助于扫描电子显微镜、透射电子显微镜、XRD和拉曼光谱等分析了螺旋碳纤维的形貌和结构。

In current study, the laser shock processing technique of high energy and short pulse duration is adopted. The substructural transformation characteristics and mechanisms of 2Cr17Mn15Ni2N austenitic stainless steel, subjected to ultra-high strain-rate and impact stress in excess of dynamic yield strength of the target, are investigated by scanning electron microscope, X-ray diffraction and transmission electron microscope technology.

采用高能短脉宽激光冲击加载技术,利用扫描电子显微镜,X射线衍射和透射电子显微镜等手段,研究了在激光诱导的超高应变率和高于材料动态屈服强度冲击加载条件下,2Cr17Mn15Ni2N奥氏体不锈钢表面亚结构的转变特征和机制。

Pristine Li-Al LDHs are synthesized by hydrothermal process in different reaction conditions by varying the aging time for 1 and 24 hours. Both the Li-Al layered double hydroxides (abbreviated as Li-Al LDH1 and Li-Al LDH24 for aging time 1 hour and 24 hours, respectively) were modified by using sulphanilic acid sodium salt hydrate, modified agent to form modified Li-Al LDH1-SAS and Li-Al LDH24-SAS. The morphology of the pristine layered double hydroxides are investigated by using wide angle X-rays diffraction, scanning electron microscopy and particle size analyzer which indicates that the crystallinity and aspect ratio is increased with increasing the aging time from 1 hour to 24 hours. The particle size of Li-Al LDH24 and Li-Al LDH1 are found to be ~1000 nm and ~250 nm, respectively. Both the pristine and modified LDHs are characterized by XRD, FTIR spectra and thermogravimetric analysis.

本研究目的在於改变长晶时间的长短,合成出同径大小的Li-Al LDHs,再经由改质剂sulphanilic acid sodium salt hydrate将Li-Al LDHs无机层材表面有机官能化制备出改质型Li-Al LDHs-SAS,於是进一步藉由扫描式电子显微镜、射径仪和穿透式电子显微镜等仪器分别观察LDHs改质前和改质后其主层结构型态上的变化;从中可以发现Li-Al LDHs随著长晶时间的增加其径有随之增大的趋势,但经有机化改质后其径会由於改质环境的影响明显低许多,针对此现象本实验将未改质和改质后之Li-Al人工无机层材制备成复材进一步探讨其在热性质和难燃特性上的为表现。

The morphology, structure and composition of the final nano-products were characterized by scanning electron microscope, energy-dispersive spectroscope and x-radial diffraction analysis.

采用扫描电子显微镜、X射线衍射、EDS能谱仪和透射电子显微镜对其表面形貌、结构和成分进行分析,结果表明所得纳米线为In2O3。

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Yang yinshu、Wang xiangsheng、Li decang,The first discovery of haemaphysalis conicinna.

1〕 杨银书,王祥生,李德昌。安徽省首次发现嗜群血蜱。

Chapter Three: Type classification of DE structure in Sino-Tibetan languages.

第三章汉藏语&的&字结构的类型划分。