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电子显微镜

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The Scanning electron microscopy is used to study the morphological features of porcelaneous layer s on surface of freshwater cultured pearls from Zhuji, Zhejiang Province, and the calcium carbonate polymorph of porcelaneous layer s is identified by X-ray powder diffraction.

采用扫描电子显微镜对中国浙江诸暨三角帆蚌养殖珍珠表面特别是无珍珠光泽的瓷质层的微形貌进行了研究,并采用X射线粉晶衍射对瓷质层进行了物相鉴定。

The dissolubility of PPLA in water was (2.16~4.32)×10-2 mg·mL-1 according to eye judgment. The critical micelle concentration was 2.16×10-2 mg·mL-1 obtained from a fluorospectrophotometer. The self-assembled aggregates of PPLA in water were nanoscale spheres observed by a transmission electron microscope. The particle size and zeta potential tests by dynamic light scattering revealed that during preparation, the ratio of hydrophilicity/hydrophobicity, the aqueous medium and the pH had great influences; while dilution, freezing and pH change to basic condition had no effect after preparation, but pH change to acidic condition made the nanoparticles precipitate.

目测法得到其溶解度为(2.16~4.32)×10-2 mg·mL-1;荧光法得到聚合物的临界胶束浓度为1.12×10-3 mg·mL-1;透射电子显微镜观察显示该聚合物在水中的自组装聚集体为纳米级球形;动态激光光散射测试微球的粒径和Zeta电位发现,在微球的制备过程中,聚合物的亲/疏水性比例、水相介质及水溶液的pH值对它影响显著;而制备后,稀释和冷冻对它无显著影响,改变微球的环境pH值至酸性,出现聚集,至碱性无影响。

In this study, Chitosan-Poly complex nanoparticles were prepared by template polymerization of acrylic acid in the chitosan solution. The preparation and characterization of CS-PAA nanoparticles including the yields of the nanoparticles, FT-IR spectrum analysis, dynamic light scattering, zeta potential, and morphology of nanoparticles were concentrated in this study. The effects of temperature, weight ratio of CS and PAA, and pH value on the physicochemical properties of nanoparticles were studied.

本研究中,我们以模板聚合法在几丁聚醣(Chitosan, CS)溶液中聚合丙烯酸(Acrylicacid, AA)以制备几丁聚醣-聚丙烯酸复合奈米颗粒并计算其产率,再以傅利叶红外线光谱仪、动态光散射粒径分析仪(Dynamic light scattering, DLS)、表面电位测定仪及穿透式电子显微镜等仪器分析CS-PAA 复合奈米颗粒之性质,以探讨聚合时温度、聚合反应时间、CS 与AA 之重量比,以及介质pH 值对CS-PAA 复合奈米颗粒结构的影响。

Results showed that the paint can achieve good adhesion, better heat resistance and excellent protectiveness for magnesium alloy.

用扫描电子显微镜等分析手段研究了涂层的片状层叠组织结构,并探讨了涂层的成膜机理与防护作用。

Pd film was deposited on the surface of pure titanium using welding complex Pd target by arc ion plating.

利用电子显微镜、X射线衍射仪、显微硬度试验机等分析手段,对采用焊接复合式靶材,在钛表面沉积出的钯膜层进行分析研究。

Electron beam brazing parameters of stainless steel quadrate tube were decided.

确定了不锈钢方管电子束钎焊的工艺参数,并利用扫描电子显微镜和能谱分析仪,对电子束钎焊试样的显微组织进行了分析。

The electron microscope and scanning electron microscope are used to observe the dot feature of Ni stamper and injection part, and via backlight module afterward assembles with six axes radiometry to measure radiance value and uniform.

4以电子显微镜与SEM观测镍模仁及射出品上的Dot特徵,并经由背光模组组装之后,以六轴辉度计量测其辉度值与均匀性。

1 Steel plant,and profound analysis was carried out for the capability of reducing impurity of blowing-argon,ladle reefing,middle-vessel,crystallizer,and the infection of variant deoxidation ability on the content,composition and shape of the impurity in carting blank,through gas-analysis,image-analysis and electron microscope scan.

为了解济钢一炼钢钢水纯净度的实际状况,选择两个典型钢种BC和AH32为分析对象,通过气体分析、图像分析和电子显微镜扫描分析分别对吹氩处理和LF炉精炼处理、中间包和结晶器去除夹杂物的能力及采用不同的脱氧工艺对铸坯夹杂物含量、组成及形态的影响进行了深入分析,找出了全氧和氮的变化规律、夹杂物粒度分布及主要组成,为研究如何降低夹杂物含量和改变夹杂物形态提供了技术基础。

According to the proposed "autocatalytism"for γ→ε transformation, both regular and irregular overlapping of stacking faults were possible for the formation of the lamellar ε martensite.

用透射电子显微镜研究了Fe28Mn6Si5Cr合金ε马氏体生长前端的"矛状"形态特征、层片状结构(1amella structure)以及ε马氏体在γ/ε界面处的交滑移现象。

The surface morphologies of flax fiber during retting of nature fermentation and enzyme-retting period were studied by scanning electron microscopy.

利用扫描电子显微镜研究温水浸渍法脱胶和酶法脱胶过程中亚麻纤维表面形态的变化情况。

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This one mode pays close attention to network credence foundation of the businessman very much.

这一模式非常关注商人的网络信用基础。

Cell morphology of bacterial ghost of Pasteurella multocida was observed by scanning electron microscopy and inactivation ratio was estimated by CFU analysi.

扫描电镜观察多杀性巴氏杆菌细菌幽灵和菌落形成单位评价遗传灭活率。

There is no differences of cell proliferation vitality between labeled and unlabeled NSCs.

双标记神经干细胞的增殖、分化活力与未标记神经干细胞相比无改变。