甲醛肟

The 3-chloro-4-trifluoromethoxy benzonitrile was synthesized from 3-chloro-4-trifluorome- thoxy aniline by diazotization, formaldoximation ,hydrolysis and cyanation.

以3-氯-4-三氟甲氧基苯胺为原料，经重氮化、甲醛肟化、水解和腈化反应得到纯度≥99。

This paper presents the synthesis of three kinds of amine such as 2-(methyl- sulonyl)ethylamine,3-propylamine and 2--ethylamine via three different methods.

本文采用三种不同的方法合成了2-乙胺，3-丙胺，2-乙胺等3个含砜基伯胺；还合成了3--x-吲哚甲酸甲酯(x=5，6，7)， E-4-喹啉甲醛肟，E-6-氟-2-吡啶甲醛肟等三类芳环甲醛肟，其中吲哚类和吡啶类化合物未见文献报道。

The reactivities of 1 and other long chain oximes with p nitrophenyl diphenyl phosphate, p nitrophenyl diethyl thiophosphate, and O ethyl ( s β diisopropylaminoethyl) methyl phosphonothiolate were studied.

报道了一种新的高亲核长链咪唑肟N 十四烷基咪唑 2 甲醛肟的设计与合成，并比较了它及其他长链咪唑肟与有机磷酸酯二苯基、对硝基苯基磷酸酯、对硫磷及 Vx 的反应活性。

The reaction mechanism, thermodynamic and kinetic behavior of the dipole cycloaddition reaction of benzaldoxime with propinol have been studied by DFT method at B3LYP/6-31G* level.

用密度泛函理论方法在B3LYP/6-31G*水平上研究了苯甲醛肟与炔丙醇加成反应的微观机制和热力学、动力学行为。

The results show that there are eight reaction channels, corresponding to eight transition states, in the reaction process. The main parts of all transition states are non-planar five-membered ring, in which the geometry of Z -benzaldoxime and E -benzaldoxime is maintained partially, but the bond length, bond angle and charge are all changed.

结果表明，在苯甲醛肟与炔丙醇加成反应过程中， 8个可能反应通道的过渡态中均形成非平面五元环结构，其中苯甲醛肟的 Z 、 E 构型特征得到了部分保留，但主要部分的键长、键角均发生了变化，电荷也进行了重新分布。

The four reaction channels including hydroxyl-type benzaldoxime are endothermic reaction, thermodynamically non-spontaneous process, but the other four reaction channels including ion-type benzaldoxime participation are exothermic reaction and thermodynamically spontaneous process. The latter four reaction channels, which have lower reaction barriers, faster reaction velocities and bigger equilibrium constants than those of the former fours, are the chief reaction channels.

苯甲醛肟以羟基型参与反应的4个反应通道均为吸热反应和热力学非自发过程，它们均具有较高的反应势垒、较慢的反应速率和较小的平衡常数；而以离子型参与反应的四个反应通道均为放热反应和热力学自发过程，它们的反应势垒较低，反应速度较快，平衡常数也较大，故苯甲醛肟应主要以离子型参与反应。

The determination method of trace manganese content in the water was investigated by formaldoxime spectrophotometry.

提出应用甲醛肟分光光度法测定原水中微量金属锰含量的方法，并对可能的干扰进行了讨论，对方法的精密度和准确度进行实验。

Key wordy: Longjiang River; Fe; Mn; Heavy–metal pollution; Countermeasures and Suggestion; Spectrophotometry; Formaldoxime; O-phenanthroline

龙江； Fe； Mn ；重金属污染；对策与建议；分光光度法；甲醛肟；邻菲啰

The intermediate which obtained from oximation of 7a-e reacted withmethyl N-(2-bromomethylphenyl)-N-methoxycarbamate to synthesize oxime ether methyl carbamate 3a-e.

以邻位卤代苯甲醛和3-丁烯-2-醇为原料通过钯催化&一锅法&反应合成了2-乙酰基茚7a-e，7a-e 肟化之后和N-(2-溴甲基苯基)-N-甲氧基氨基甲酸甲酯反应合成了肟醚类氨基甲酸甲酯3a-e，进一步胺解之后得到了肟醚类氨基甲酰甲胺3f-j。

According to the clear water experiment, aeration performance of the new equipment is good with high total oxygen transfer coefficient and oxygen utilization ratio.

曝气设备的动力效率在叶轮转速为120rpm～150rpm时取得最大值，此时氧利用率和充氧能力也具有较高值。

The environmental stability of that world - including its crushing pressures and icy darkness - means that some of its most famous inhabitants have survived for eons as evolutionary throwbacks, their bodies undergoing little change.

稳定的海底环境─包括能把人压扁的压力和冰冷的黑暗─意谓海底某些最知名的栖居生物已以演化返祖的样态活了万世，形体几无变化。