甲醛溶液

By means of adjusting the pH value of solution,we eliminated the effect of phosphate on ammonium which is determined by formaldehyde method.

文章通过调节溶液的pH值，消除磷酸盐对甲醛法测定铵根的影响，针对溶液中磷酸盐存在的不同形态，建立了含磷酸盐体系中铵根的快速测定方法。

After sodium bisulfite reacted with methanal at 60-65℃ for 0.5h, aniline was dripped into the system to synthesize phenylaminomethyl-sodium sulfonate subsequently, the diazol solution of p-nitroaniline was dripped into phenylaminomethyl-sodium sulfonate synthesized to form 4'-nitro-4-aminoazobenzene. The compound was then added into diazol solution of p-chloroaniline to obtain the object product, which was identified by IR spectrum and element analysis.

在60~65℃温度下，亚硫酸氢钠与甲醛反应半小时之后滴入苯胺生成苯胺基甲基磺酸钠，另将硝基苯胺重氮化得到重氮盐溶液滴入苯胺基甲基磺酸钠中得到4'-硝基-4-氮基偶氮苯，然后将其滴入氯苯胺重氮化后的重氮盐溶液中，得经红外光谱检验和元素分析证实的目标产物。

The function mechanism among the minerals and floatation drugs had been studied with the way of IR and academic calculation, which pointed out that absorption of G-4 on the surface of phosphorite belonged to physical and chemical types, but the chemical one was in the highest flight. Absorption of amine collector named GE-609 on the surface of quartz belonged to electrostatic and physical type. Distilled water could hardly wash the GE-609 down from the surface of quartz. Leading component of S-721 was the concentrated compound of naphthol sulfonic acid and formaldehyde. The compound had a stronger affinity to the Mg~(2+) on surface of dolomite than the Ca2+ on surface of phosphorite, which is the essential reason in the separation of phosphorite and dolomite. The leading components of soluble glass in function were HSiO3 hydronium and F^SiC^ colloid granule.

通过红外光谱测定以及理论计算的方法研究了选矿药剂与矿物间的作用机理，研究表明：脂肪酸捕收剂G-4对胶磷矿的捕收作用是以化学吸附为主、化学吸附与物理吸附共同作用的结果；胺类阳离子捕收剂GE-609在石英表面的吸附属于静电物理吸附，但很难用水洗的方法使GE-609从石英表面脱附；S-721主要成分为萘酚磺酸与甲醛的缩合物，萘酚磺酸与甲醛的缩合物对白云石表面Mg~(2+)的吸附明显强于对胶磷矿表面Ca~(2+)的吸附，这是胶磷矿与白云石分离的根本原因；水玻璃溶液中对石英起抑制作用的主要组分是HSiO_3~-和H_2SiO_3胶粒，水玻璃除对石英起抑制作用外，对矿浆还具有一定的分散作用。

The following was studied in this paper:(1) The adhesive strength of polyvinyl alcohol with different degree of polymerization and different degree of alcoholysis (2) The adhesive strength of polyvinyl acetals with different acetalization degree (3) Effects of polyvinyl acetate on adhesive strength of white glue when PVA or polyvinyl acetals was used as its protective colloid.

本文主要研究以下内容：(1)不同聚合度、醇解度聚乙烯醇溶液粘接强度；(2)不同缩醛度的聚乙烯醇缩醛溶液的粘接强度；(3)聚乙烯醇或聚乙烯醇缩甲醛为保护胶体时，聚醋酸乙烯酯乳液的粘接强度，以及研究白乳胶改性物，制备高粘度和高粘接强度的白乳胶。

Test of electrochemical methods Benzylidene acetone, formaldehyde, compound additive D, ammonium metavanadate solution of acid sulfate tin polarization curves, test ammonium metavanadate on the open circuit potential acid sulfate solution of tin.

用电化学工作站测试分析苄叉丙酮、甲醛、复合添加剂D、偏钒酸铵对酸性硫酸盐镀锡溶液的极化曲线的影响，测试偏钒酸铵对酸性硫酸盐镀锡溶液开路电位的影响。

Benzylidene acetone desorption potential acid sulfate tin plating solution is very close to the ideal desorption potential; Benzylidene acetone, formaldehyde can regulate the desorption potential role and can increase the current density range; Composite additive D can make acid sulfate tin plating solution in the hydrogen produced during the rapid detachment; Ammonium metavanadate can catalyze Sn4+ and restore to Sn2+, and then make solution stability.

苄叉丙酮的脱附电位很接近酸性硫酸盐镀锡溶液的理想脱附电位；甲醛具有调节苄叉丙酮脱附电位的作用，并且能够增大电流密度范围；复合添加剂D能够使酸性硫酸盐镀锡溶液在电镀过程中产生的氢气迅速脱离；偏钒酸铵能够催化Sn4+还原为Sn2+，从而使镀液稳定。

A clean production technology of sodium sulfoxylate formaldehyde by one-step process with sodium pyrosulfite ,zinc powder and formaldehyde as raw materials was studied in detail.

详细研究了以焦亚硫酸钠、锌粉和甲醛为原料，一步法合成甲醛合次硫酸氢钠的清洁生产工艺，其最佳操作条件为：焦亚硫酸钠与锌粉物质的量比约1∶2.5，焦亚硫酸钠与甲醛物质的量比约1∶2.1，亚硫酸氢钠溶液的pH 3.3~3.6，活化温度≤45℃，最高温度97~102℃，高温反应时间

The effects of solution\'s pH value, mol ratio between phenyl aldehyde and L-Arginine, concentrations of sodium chloride, ammonia chloride andL-Lystine, initial concentration of L-Arginine on precipitation rate of a -tolylene arginine were investigated, the results indicated that phenyl aldehyde precipitation method\'s appropriate pH value was higher than 11, suitable mol ratio between phenyl aldehyde and L-Arginine was 1.25, initial concentration of L-Arginine was must higher than 15g/L, sodium chloride had little effect on precipitation rate, on the contrary, ammonia chloride and L-Lystine had great effect on it, both of them must be eliminated; At the same time, adsorption isotherm at 25 C of L-Lystine on anion exchange resin A was measured, the result showed that the maximal equilibrium adsorbance was 30mg/g, the influences of solution\'s pH value, temperature, concentration of chloride ion on adsorption of L-Lystine by anion exchange resin A were also studied, the results indicated that appropriate operational pH value was 0.5 0.2, the effect of temperature on adsorption ratio was little, process could be operated at room temperature, the concentration of chloride ion must be eliminated.

考察了溶液pH值、苯甲醛与L-精氨酸摩尔比、氯化钠与氯化铵浓度、L-赖氨酸浓度、L-精氨酸初始浓度对苯甲醛沉淀L-精氨酸的影响，结果表明，沉淀反应的适宜pH值大于11，苯甲醛与L-精氨酸的适宜摩尔比为1.25，(来源：Aa6BC论文网www.abclunwen.com)L-精氨酸适宜的初始浓度在15g/L以上，氯化钠的存在对沉淀率基本上没有影响，而氯化铵和L-赖氨酸的存在使沉淀率下降；同时测定了25℃时阴离子交换树脂A吸附L-赖氨酸的吸附等温线，表明其最大平衡吸附量为30mg/g，考察了溶液pH值、温度、氯离子浓度对阴离子交换树脂A吸附脱除L-赖氨酸的影响，结果显示从L-精氨酸和L-赖氨酸混合液中吸附分离出L-赖氨酸的适宜pH值为10.5±0.2，温度对L-赖氨酸吸附率影响不大，吸附过程可在室温下进行，氯离子的存在使L-赖氨酸的吸附率降低。

The optimun technological conditions were studied on the synthesis of 9-flourenylmethanal by the reaction of flouren and ethyl formate , and the synthesis of 9-flourenylmethanol by the reaction of 9-flourenylmethanal and methanal with sodium ethylate as catalyst.

研究了乙醇钠为催化剂，由芴与甲酸乙酯合成芴甲醛，再由芴甲醛与甲醛合成苯甲醇的工艺条件，结果表明：合成芴甲醛时，当芴为 16g时，催化剂乙醇钠 4 。5g ，甲酸乙酯 66ml，反应时间为 36h ，收率 75 %：合成芴甲醇时，当芴甲醛为 19g时，甲醛 7.0ml，10 %NaOH溶液 70ml，反应时间 2 。0h ，收率：63

The inflammatory infiltrate in the cutaneous lesions of secondary syphilis was investigated using immunohistochemical technique. Results: The TP-specific DNA was found in 10 of 24 (45.8％) lesions of secondary syphilis.

用巢式PCR方法对24例10％甲醛溶液固定、石蜡包埋的二期梅毒疹标本进行了梅毒螺旋体DNA检测；用免疫组化方法对二期梅毒皮损中的浸润细胞进行检测。

The split between the two groups can hardly be papered over.

这两个团体间的分歧难以掩饰。

This approach not only encourages a greater number of responses, but minimizes the likelihood of stale groupthink.

这种做法不仅鼓励了更多的反应，而且减少跟风的可能性。