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Nickel sulfate was the most frequent sensitizer, followed by Thimerosal, Potassium dichromate, Fragrance mix and Formaldehyde. Frequencies of contact allergy to Thiuram mix, Mercapto mix, Imidazolidinyl urea, and bronopol were relatively low.

结果: 1 129 例受试者中,阳性反应747例,阳性反应率较高的变应原依次是:硫酸镍、硫柳汞、重铬酸钾、芳香混合物、甲醛,阳性反应率较低的变应原有:秋兰姆混合物、硫氢基混合物、咪唑烷基尿素、溴硝丙二醇。

At 1st、2nd、3rd months after surgery the rats were killed respectively and the implanted tibiae were got , the tissue samples were fixed with 10% Formaldehyde soaked and 8% formic acid was used to dissolve the calcium for 10 days.

于种植术后1个月、2个月、3个月时,取出带种植体的胫骨,取下的标本立即放入10%甲醛缓冲溶液固定、经过8%甲酸溶液脱钙、梯度酒精脱水后,制作HE染色的组织学切片,做光镜及骨组织的形态计量学观察。

From solution polymerization, polymers are tokened using MALDI-TOF-MSand IR spectrum. The structure of polymers are confirmed and obtain 2-28 repeatunits of poly(p-aminobenzaldehyde). The tip of polymer molecule still have one-NH_2 and one -CHO. To a certainty condtion, this polymer can polymerization tocreat even more molecular weight.

对溶液聚合得到的聚合物进行了飞行时间质谱和红外光谱表征,确定了聚合物分子的结构,测得了聚对氨基苯甲醛的2-28个重复单元,且聚合物分子末端还保留有一个-NH_2和一个-CHO,在一定条件下可以进一步缩合生成更高分子量的聚合物。

It has shown that the optimum condition to modify phenol-formaldehyde resin were phenol﹕formaldehyde﹕diethylene triamine 1﹕0.8﹕0.015, reaction temperature 95~105℃and reaction time 2h, when using diethylene triamine as modifying agent.

实验结果表明,以二乙烯三胺为改性剂时,制备改性酚醛树脂的最佳实验条件是:苯酚﹕甲醛﹕二乙烯三胺为1﹕0.8﹕0.015;反应的最高温度为95~105℃;反应时间2h。

According to the Mannich-Reaction, a kind of chelating flocculant grafted with diethylene triamine was prepared from polyacrylamide, formaldehyde and diethylene triarmne.

研究了以聚丙烯酰胺、甲醛、二乙烯三胺为原料,按照Mannich反应机理制备部分胺化接枝型螯合作用絮凝剂及其从水中除铅性能。

Under the optimum conditions (i.e., reaction at 40℃ using hyperthermophilice esterase APE1547, 4-Cl-benzaldehyde substrate, and trichloromethane solvent), this reaction provided optically active secondary alcohol with an enantiomeric excess up to 56% and a yield up to 78%.

在最适条件(嗜热酯酶APE1547为酶源,反应温度40℃,氯仿为溶剂,4-Cl-苯甲醛为底物)下,加成反应生成的光学活性醇产率最高达78%,ee值最高可达56%。

A new production technology of high-quality trimellitic anhydride with the liquid-phase air-oxidation from 1,2,4-trimethylbenzene was developed.

偏苯三酸酐的生产方法主要有偏三甲苯气相空气氧化法、偏三甲苯液相硝酸氧化法、偏三甲苯液相空气氧化法和间二甲苯甲醛液相空气氧化法。

It was shown that the purity of the aim product was higher than 99% and its yield was 60%~70%. The intermediate product p-tertbutoxycarbonyloxybenzaldehyde could be synthesized conveniently and quantitatively. The main byproduct was triphenylphosphine oxide.

结果表明,所得目标产物对特丁氧酰氧基苯乙烯纯度达99%以上,产率为60%~70%,中间产物对特丁氧酰氧基苯甲醛可以定量合成,反应的副产物主要是三苯基氧化膦。

Methods 2-(piperazin-1-yl)-1-(pyrrolidin-1-yl)ethanone (2) was synthesized from pyrrolidine via amidation and substitution, followed by treating with chloroacetyl chloride and triphenylphosphine in a "one pot" manner to give the corresponding phosphonium chloride 3 in a stable and pure form after crystallization from isopropanol.

以四氢吡咯为原料,先与氯乙酰氯成酰胺,再与哌嗪发生取代反应制得中间体[(1-四氢吡咯基)甲基]哌嗪(2);化合物2与氯乙酰氯和三苯基膦反应,经异丙醇重结晶得到稳定的有机鏻盐(3);化合物3与3,4,5-三甲氧基苯甲醛发生Wittig反应,再与马来酸成盐得目标化合物马来酸桂哌齐特(1)。

A new colorimetric chemosensor 1 based on a tripodal benzaldehydic-phenylhydrazone selectively sensing acetate ion has been synthesized.

本文合成了一个新的基于三脚架苯甲醛苯腙的能够选择地检测醋酸根离子的比色化学传感器1。

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I am accused of being overreligious," she said in her quiet, frank manner,"but that does not prevent me thinking the children very cruel who obstinately commit such suicide.""

客人们在卡罗利娜·埃凯家里,举止就文雅一些,因为卡罗利娜的母亲治家很严厉。

Designed by French fashion house Herm è s, this elegant uniform was manufactured in our home, Hong Kong, and was the first without a hat.

由著名品牌 Herm è s 设计,这件高贵的制服是香港本土制造,是我们第一套不配帽子的制服。

Do not 'inflate' your achievements and/or qualifications or skills .

不要 '夸大' 你的业绩或成果,条件或者技能。