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甲醛

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Rats in the experimental group received conventional fixation, and then decalcified with modified decalcifying fluid [10 mL of methanoic acid, 8 mL of concentrated hydrochloric acid (1.19 relative density, 3 g of aluminum chloride, 20 mL of formaldehyde (0.4 volume fraction), 3 mL of glacial acetic acid, adding to 200 mL with saline solution], dehydrated, transparentized with chloroform, and then embedded for a long time, dyed, mounted and made into tissue sections.

实验组经过常规固定,而后应用改良脱钙液(甲酸10 mL、浓盐酸(相对密度1.19)8 mL、氯化铝3 g、体积分数为0.4的甲醛20 mL、冰乙酸3 mL,加生理盐水至总体积200 mL)脱钙、脱水、氯仿透明、包埋时间延长、染色、封固和切片;对照组进行常规固定、脱钙、脱水、透明、包埋、染色、封固和切片。

The Mannich-type addition of O , O'-dialky phosphite to 2-fluorobenzaldehyde and 4-trifluoro- methylaniline was carried out in one pot by means of adopting three kinds of green synthetic methods, microwave irradiation, ionic liquid and free solvent-catalyst condition. According to the results, the synthetic method was optimized without catalyst and solvent at 100 ℃ and 15 min, and it was economic, convenient, high yields, timesaving and environment friendly.

采用微波辐射﹑离子液体和无溶剂无催化剂三种绿色合成方法,分别进行了以亚磷酸酯、邻氟苯甲醛和对三氟甲基苯胺为原料的类Mannich一锅法合成反应研究,经合成筛选,优选出控制反应温度100 ℃、无溶剂和无催化剂加热反应15 min的合成方法,实验结果表明该方法经济、简便、产率高、反应时间短及对环境友好。

The ozonolysis of isoprene has a significant contribution to atmospheric carbonyls, especially to formaldehyde and methylglyoxal.

异戊二烯臭氧氧化反应对大气羰基化合物特别是甲醛和丙酮醛具有重要贡献。

Secondly, the silver based catalysts modified by phosphorus, zirconium, zinc, potassium and so on using molecular sieve as carrier, which were produced by ion-exchange method, had also good catalytic performance for 1,2-propane glycol oxidation to methylglyoxal. The conversion of 1,2-propane glycol and the selectivity of methylglyoxal were both high, and the impurity such as formaldehyde and acetaldehyde in the product is little. At the condition of the temperature 300 ℃, the molar ratio of oxygen to 1,2-propane glycol 1.7:1, the space velocity 6000h~(-1), and the concentration of 1,2-propane glycol 70wt%, the conversion of 1,2-propane glycol is 90% and the selectivity of methylglyoxal is 45% on the Ag-P catalyst.

其次对采用离子交换法制备的负载在分子筛上的银系催化剂进行了研究,发现此催化剂在助催化剂磷、锆、锌、钾等的作用下对丙二醇的低温氧化脱氢具有很高的活性,可以得到较好的丙酮醛的收率,并且产物中的甲醛、乙醛副产物的量比较低;经过对Ag-P催化剂上反应条件的考察,发现当温度为300℃、氧醇比1.7:1、空速6000h~(-1)、丙二醇浓度为70wt%时,丙二醇的转化率为90%,丙酮醛的选择性为45%。

The results indicated isoprene was soon consumed under the condition of excess ozone. During the reaction, the major carbonyl products formed were methyl vinyl ketone, methacrolein, methylglyoxal, and formaldehyde. Formic acid, CO and CO2 were also among the products.

在反应温度(294±2)K,压力为1.01×10^5Pa空气,O3过量的条件下,异戊二烯很快反应完全,反应中生成的羰基产物主要包括甲基丙烯醛、甲基乙烯基酮、丙酮醛和甲醛;产物中还包括甲酸、一氧化碳和二氧化碳。

Methylol was led into the surface of carbon black and then graft esterificated with maleic anhydride using the feature that the hydrogen atoms onto the layer surface of carbon black were easily substituted.

为了改善导电炭黑与聚合物间的互容性,利用炭黑表面氢原子易被取代的特点,用甲醛在炭黑表面引入羟甲基,再与马来酸酐进行酯化接枝。

Methylol was led into the surface of carbon black and then graft esterificated with maleic anhydride using the feature that the hydrogen atoms onto the layer surface of carbon black were easily substituted.

摘 要:为了改善导电炭黑与聚合物间的互容性,利用炭黑表面氢原子易被取代的特点,用甲醛在炭黑表面引入羟甲基,再与马来酸酐进行酯化接枝。

In addition, the optical microphotography showed that the dispersion of methylolated MWCNTs in water was improved significantly. And then, the dispersion of the grafted MWCNTs in xylene was enhanced remarkably.

光学图像分析表明,经甲醛处理后的MWCNTs在水溶液中的分散性明显提高,而马来酸酐酯化接枝后的MWCNTs在二甲苯中的分散性明显增强。

The results showed that the optimum preparation conditions of moulding materials were as follows: moler ratio of melamine to formaldehyde 1:2.5, water turbidity of the reaction end point 1:3, content of cellulose 42%~48%, fineness of moulding powder 100~120 mesh.

结果表明,三聚氰胺与甲醛物质的量比为1:2.5、终点控制在水浊度1:3,纤维素用量42%~48%,干燥温度70℃,球磨至100~120目时,制得的模塑料性能良好,符合国家日用级产品相关标准。

Urea and its monomeric species were as scavenger of formaldehyde in the resin.

尿素及其衍生物对于该类树脂而言,仅仅起到的是甲醛捕捉剂的作用。

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They weren't aggressive, but I yelled and threw a rock in their direction to get them off the trail and away from me, just in case.

他们没有侵略性,但我大喊,并在他们的方向扔石头让他们过的线索,远离我,以防万一。

In slot 2 in your bag put wrapping paper, quantity does not matter in this case.

在你的书包里槽2把包装纸、数量无关紧要。

Store this product in a sealed, lightproof, dry and cool place.

密封,遮光,置阴凉干燥处。