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Results By using two-phase solvent systems composed of petroleum ether-ethylacetate-methanol-water (22:25:23:17) at the flow rate of 2.0 mL/min, with rotating speed of 800 r/min, and at temperature of 25℃, the yield of d1-tetrahydropalmatine and of protopine purified from the total alkaloids being 16.9% and 14.7%, with purity of 99.3% and 98.8% respectively can be reached.

结果 石油醚-乙酸乙酯-甲醇-水(22:25:23:17)为溶剂体系,流速为2.0 mL/min,仪器转速800 r/min,温度25℃,从延胡索总碱中可一步纯化得到原阿片碱和延胡索乙素,得率分别为16.9%和14.7%,纯度分别为99.3%和98.8%。

Pseudoephedrine hydrochloride is the main content used in the Cold Medicine and plays the most important role in the treatment.

盐酸伪麻黄碱(S--a-1[1-乙基]-苯甲醇盐酸盐)是感冒药中的常用成分,并且是发挥主要药效的成分。

We find that methanol will effectually pyrolyze and generate large amounts of hydrogen when it is heated above 400℃. The ratio of pyrogenation and amount of hydrogen generated increase rapidly with the temperature rise.

实验发现,甲醇在被加热至400℃后会开始热分解产生氢气,并且随着温度的升高,热分解率及产氢量快速增大。

Methanol can pyrolyze and generate hydrogen when it is heated by the exhaust of diesel engine(temperature range between 400℃and 600℃). Then let the hydrogen generated from methanol go into cylinder with the air directly. By this means, we hopefully increase the rate of economizing oil of emulsified fuel in diesel engine.

利用柴油机排烟(温度一般在400~600℃)余热加热甲醇热分解制氢,并在线通入到柴油机进气道入口,有望实现柴油机燃用乳化油时节油率的提高。

The determination of quercitin was performed on Century SIL C18 BDS (250 mm×4.6 mm, 5μm) column, using methanol-water-phosphoric acid (V:V:V=60.00:40.00:0.02) as mobile phase at a flow rate of 0.8mLmin^(-1) and UV detection at 360 nm. The determination of gallic acid was performed on Century SIL C18 BDS (250 mm×4.6 mm, 5μm) column, using acetonitrile-water-phosphoric acid (V:V:V=5.00:95.00:0.02) as mobile phase at a flow rate of 0.8mLmin^(-1) and UV detection at 272 nm.

槲皮素的测定条件为:Century SIL C18, BDS(250.0mm×4.6mm, 5μm)色谱柱,流动相为甲醇-水-磷酸(体积比为60.00:40.00:0.02),流速为0.8mLmin^(-1),检测波长为360nm;没食子酸的测定条件为:Century SIL C18 BDS (250.0mm×4.6mm, 5μm)色谱柱,流动相为乙腈-水-磷酸(体积比为5.00:95.00:0.02),流速为0.80mLmin^(-1),检测波长为272nm。

Then recrystallize the thick product with the petroleum ether, the end product obtains its melting point after infrared lamp drying with the melting point detector and compares with the pure Diphenyl carbinol.

粗产物用石油醚重结晶,终产品经红外灯烘干后用熔点测定仪得到其熔点,并与纯品二苯甲醇比较。

In addition, dichloromethane-methanol-acetic acid (60: 30: 10, V/V) is selected as regenerant and the appropriate regeneration condition is also established by evaluation of the regeneration effciency.

此外,通过对再生效率的考察,寻找到二氯甲烷—甲醇—乙酸(60:30:10,V/V)为再生剂及合适的再生条件。

To express chicken osteoprotegerin in Pichia pastoris and determine its inhibitive effects on mature osteoclastic bone resorptive function in vitro. The chOPG cDNA encoding for 382 amino acid without signal peptice was subcloned into Pichia pastoris expression vector pPICZα-A. The constructed plasmid was transformed into yeast X-33 by electroporation. The recombinant transformants were selected by Zeocin. Induced by the addition of methanol every 24 hours, the product analyzed by SDS-PAGE was sized about 43kDa and 53kDa at a yield of 200mg per litter of culture. The result of Western blotting indicated that the recombinant protein had specific antigenicity mainly owing to heterogeneous glycosylation.

为了在毕赤酵母中分泌表达鸡骨保护素(osteoprotegerin,OPG),采用DNA重组技术将chOPG成熟肽cDNA片段插入毕赤酵母表达载体pPICZα-A中,以电穿孔法转化酵母X-33,用Zeocin 平板筛选重组子,经甲醇诱导表达后, SDS-PAGE 和免疫印迹分析表达产物,由于糖基化不同,表达产物有两种,其相对分子量分别为43kDa和53kDa,表达量约为200mg/L,经Western印迹验证,有较好的抗原性。

Evaluation of the detergency on hair, the detergency ability of methanol extracts was similar with sodium dodecyl sulfate and were better than Sapindus mukorossi water extracts.

头发评估与应用方面,比较无患子甲、乙、丙、丁醇萃取物、无患子水萃取物及Sodium dodecyl sulfate之清洁力,结果显示以甲醇萃取物之清洁力与SDS相当,且优於无患子水萃物。

Results The results showed that the material with the antibacterial activity in sapium root bark primarily was in the part of large polarity, but there was antibacterial activity in the material of the methanol elution with larger polarity; and the inhibitory components of the soluble material of ethyl acetate was complex and the different parts had the variable inhibition to different bacteria and in general these materials had a certain inhibition to Staphylococcus aureus and Escherichia coli.

结果]乌桕根抑菌活性物质主要存在极性较大的部分,但极性很大的甲醇洗脱部分也没有抑菌活性;乙酸乙酯可溶部抑菌成分较复杂,不同部分时不同细菌的抑制作用不同,总体来说对金黄色葡萄球菌和大肠杆菌有一定的抑制作用。

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According to the clear water experiment, aeration performance of the new equipment is good with high total oxygen transfer coefficient and oxygen utilization ratio.

曝气设备的动力效率在叶轮转速为120rpm~150rpm时取得最大值,此时氧利用率和充氧能力也具有较高值。

The environmental stability of that world - including its crushing pressures and icy darkness - means that some of its most famous inhabitants have survived for eons as evolutionary throwbacks, their bodies undergoing little change.

稳定的海底环境─包括能把人压扁的压力和冰冷的黑暗─意谓海底某些最知名的栖居生物已以演化返祖的样态活了万世,形体几无变化。

When I was in school, the rabbi explained everythingin the Bible two different ways.

当我上学的时候,老师解释《圣经》用两种不同的方法。