甲醇

The comparison studies on gossypol of different genetic types of pigment gland in the seeds of cotton newly bred, including the special and common glandless and glanded ones, was conducted through highperformance liquid chromatography on a C18 Column with methanol 0.5% acetic acid aqueous solution, 90∶10 as mobile phase at a flow rate of 0.8mL·min-1 and UV detection at 254 nm.

运用高效液相方法对新近育成的特殊和普通的无腺体陆地棉及特殊和普通的有腺体陆地棉及海岛棉等多种遗传类型品种材料的棉酚含量进行了比较研究。实验以一反向C18色谱柱为固定相，甲醇 0.5%的醋酸90∶10为流动相，流速为0.8mL·min-1，建立了分离度好、准确而快速的棉酚HPLC测定方法：其最低检测限量3×10-6g/mL-1，精密度和准确度均小于10%，回收率为100.4%～103.2%。

The glycidol is protected by ethyl vinyl ether first to form 2,3-epoxypropyl-1-ethoxyethyl ether, then polymerized or copolymerized with EO by initiation with the mixture of diphenylmethylpotassium and triethylene glycol to give the well-defined poly.

得到的聚合物用甲酸水解去保护，并在二氧六环和甲醇的混合溶剂中用氢氧化钾溶液皂化后，得到了聚合物链的侧端挂有羟甲基官能团的线形聚醚linear Polyglycidol和poly。

Is located in Yellow River Delta, located in West Liuqiao Guangrao County Economic Development Zone, the brink of East Green high-speed, convenient transportation and strategic location, covers an area of 350,000 square meters, is a professional Companies are now built with an annual output of 3,000 tons glyoxylic acid, Allantoin 300 tons, 5,000 tons of sodium methanol, ethanol production of 5,000 tons of sodium scale.

广饶县弘达精细化工有限责任公司座落于黄河三角洲，位于广饶县西刘桥经济开发区，濒临东青高速，交通便利，地理位置优越，占地面积达350000平方米，是一家专业化公司，现已建成年产乙醛酸3000吨、尿囊素300吨、甲醇钠5000吨、乙醇钠5000吨的生产规模。

Ten batches of Cortex Moutan Carbonisatum were measured by HPLC with Paeonol as a reference substance and the HPLC analysis was performed on a Hedera ODS-3 Chromatographic Column (4.6 mm×150 mm, 5 μm), with methanol to Acetonitrile (1∶1) and 0.5‰ trifluoroacetic acid solution as mobile phase in gradient mode and the detection wavelength was at 258 nm.

采用Hedera ODS-3柱(4.6 mm×150 mm，5 μm)，流动相甲醇-乙腈(1∶1)-0.5‰三氟乙酸水，梯度洗脱，检测波长258 nm。

By adopting the method of stepwise synthesis, this paper synthetizes 1,3 - diaminopropanein 2-Hydroxy-3-methoxybenzaldehyde Zn-Sm heteronuclear bimetallic in Anhydrous methanol solution.

6楼本文采用分步合成的方法，在无水甲醇溶液中合成了1，3-丙二胺缩邻香兰素Zn-Sm异核双金属配合物。

By adopting the method of stepwise synthesis, this paper synthetizes 1,3 - diaminopropanein 2-Hydroxy-3-methoxybenzaldehyde Zn-Sm heteronuclear bimetallic in Anhydrous methanol solution.

本文采用分步合成的方法，在无水甲醇溶液中合成了1，3-丙二胺缩邻香兰素Zn-Sm异核双金属配合物。

In this paper, using Liaoning\'s Ca-bentonite as matrices, modifying with sodium compound at first, organically modifying with Octadecyl/Hexadecyl ammonium chloride as the cover agent, based on hydrothermal process, and dispersing the modified bentonite into the dimethyl benzene-methyl alcohol system fully, we synthesized the high-grade organic bentonite gel with stable quality and excellent characteristics.

本文以辽宁钙基膨润土为原料，首先对其钠化提纯，然后以十八／十六烷基氯化铵为有机复合剂，采用水热合成技术对膨润土进行有机改性，将改性膨润土充分分散于二甲苯-甲醇体系中制备出产品质量稳定、性能国内领先的膨润土高档有机凝胶矿物材料。

In this paper, using Liaonings Ca-bentonite as matrices, modifying with sodium compound at first, organically modifying with Octadecyl/Hexadecyl ammonium chloride as the cover agent, based on hydrothermal process, and dispersing the modified bentonite into the dimethyl benzene-methyl alcohol system fully, we synthesized the high-grade organic bentonite gel with stable quality and excellent characteristics.

本文以辽宁钙基膨润土为原料，首先对其钠化提纯，然后以十八／十六烷基氯化铵为有机复合剂，采用水热合成技术对膨润土进行有机改性，将改性膨润土充分分散于二甲苯-甲醇体系中制备出产品质量稳定、性能国内领先的膨润土高档有机凝胶矿物材料。

When 45% methanol solution containing 0.5 mmol/L hexamethylene tetraamine was used as the pump carrier, the pump flow rate and output pressure achieved 0.58 mL/min and 0.79 MPa at 4950 V, respectively. By using the pump carrier as the mobile phase, benzene and naphthanlene were separated on baseline by the EFA system.

在4950 V的外加电压下，以含0.5 mmol/L六亚甲基四胺的45%甲醇溶液为泵载流，电渗泵的流量和输出压强分别为0.58 mL/min和0.79 MPa，以泵载流为流动相，该系统对苯和萘进行了反相色谱分离。

Six experimental stages were designed in our procedure, those are:(1) metabolite recovery and tested sample preparation: the metabolites were recovered by Amberlite XAD-2 absorption, followed by MeOH elution and solvent concentration;(2) antioxidant detection and strain selection: samples were quantitatively analyzed by the inhibition effects on formation of lipid peroxides and TBARS to screen the strains able to produce antioxidants. According to the established screening methods, we chose out a strain of actinomycetes, designed as AMBL-029C;(3) antioxidant purification: the fermentation broth was recovered by a series of separation techniques including centrifugation, Amberlite XAD-2 absorption, followed by MeOH elution and a successive TLC purification. The resulting primary purified compound [temperately designed as AMBL-029C-TS] was further analyzed by HPLC to monitor its purity;(4) physical-chemical characteristics: judging from the acid-base fractionation experiments, and the pH and temperature stability tests, the compound was deduced to be a acidic compound with the properties of low polarity and highly pH and temperature stable;(5) mechanism of the antioxidant: in comparison with some other known antioxidants, TS was subjected to investigate its antioxidant mechanism, together with BHT,-tocopherol, as well as two streptomyces metabolites, homogentisic acid and -phenylpyruvic acid, which were previously isolated as the natural antioxidants in our laboratory.

针对本实验目的，我们设计了以下的实验步骤﹔（1）二次代谢物回收及检测样本处理：我们将发酵所得的培养上清液，利用疏水吸附性树酯Amberlite XAD-2吸附回收，并以甲醇溶离及真空减压浓缩脱水等方式处理，以取得提供抗氧化活性筛选之检测样本；（2）抗氧化活性检测及菌种筛选：以「过氧化脂质」和「硫丙二醯尿」的生成量进行定性定量分析以作为抗氧化物质生产菌筛选之用；经此筛选程序，我们选获了具有抗氧化物质高生产力的菌株，命名为AMBL-029C；（3）抗氧化物质的分离纯化：针对生产菌株的发酵回收处理液，以矽胶薄层色层分离法经物质层析纯化后，并以高效能液相层析法(High performance liquid chromatography；HPLC)分析物质可得一初级纯化物质，命名为AMBL-029C-TS；（4）抗氧化物质的物理化学性质分析：由酸碱转溶（acid-base fractionation）实验得知，此抗氧化物质属於中低极性的强酸性物质，对温度（37℃-100℃）及酸碱度（pH3.0-13.0）均表现出高稳定性；（5）在抗氧化机制探讨方面，我们针对数种不同的抗氧化机制进行探讨，即： 1。

According to the clear water experiment, aeration performance of the new equipment is good with high total oxygen transfer coefficient and oxygen utilization ratio.

曝气设备的动力效率在叶轮转速为120rpm～150rpm时取得最大值，此时氧利用率和充氧能力也具有较高值。

The environmental stability of that world - including its crushing pressures and icy darkness - means that some of its most famous inhabitants have survived for eons as evolutionary throwbacks, their bodies undergoing little change.

稳定的海底环境─包括能把人压扁的压力和冰冷的黑暗─意谓海底某些最知名的栖居生物已以演化返祖的样态活了万世，形体几无变化。