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甲醇

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The whole analysis was completed on a C〓 column in 18min at a flow rate of 0.5 ml/min, with the mobile phase of methanol-water (93: 7, v: v) containing 75 mmol/L TEOLA and 200 mmol/L HAc, or with the mobile phase of ethanol-water (90: 10, v: v) containing 25 mmol/L TEOLA and 200mmol/L HAc pumped at 0.25ml/min. Compared with the methanol system, the ethanol system was a better candidate for the separation of thulium porphyrin complexes in view of selectivity.

在C〓分析柱(5μm,2.5×150mm)上,流动相为:甲醇:水=93:7(v/v内含75mmol/L三乙醇胺和200mmol/LHAc),流速为0.5ml/min和流动相为:乙醇:水=90:10(v/v,内含25mmol/L三乙醇胺和200mmol/L HAc),流速为0.25ml/min,均能使六个铥卟啉配合物在18min内得到有效的分离,相比之下,乙醇体系对铥卟啉配合物更具有分离选择性。

Repeat the procedure with a second portion of methanol, or other suitable solvent, accurately measured, add this washing to the titration vessel, and immediately titrate.

用第二部分的甲醇或其他合适的溶剂重复上述操作,准确测量,将这一部分洗涤物加至滴定容器中,立即滴定。

In this way, we can get the optimum parameters which are ip = 100mA/cm2, ton/toff = 0.1s/0.5s, and loading capacity 6C/cm2. This result is suitable for both the hydrogen adsorption and the methanol oxidation.

发现脉冲参数控制在ip=100mA/cm2、ton/toff=0.1s/0.5s、通电量6C/cm2时,不论是氢的脱附或甲醇的氧化,该电极触媒活性表现均最佳。

Methods: Glipizide gliclazide glyburide glimepiride gliquidone repaglinide nateglinide pioglitazone rosiglitazone metformin phenformin and tolbutamide added in the blank ground samples were extracted with 80% methanol and were separated from an ACQUITY UPLC DBH C18 column with a gradient mobile phase of acetonitrile - 0.2 % formic acid water solution. A tandem quadrupole mass spectrometer equipped with electrospray ionization source was used in positive ion mode multiple reaction monitoring was performed to quantify above mentioned compounds.

被添加在中成药制剂及其包装物中的二甲双胍、苯乙双胍、罗格列酮、吡格列酮、格列吡嗫娶瑞格列奈、甲苯磺丁脲、格列齐特、格列苯脲、那格列奈、格列美脲、格列喹酮等西药成分用80%甲醇提取,以乙腈- 0.2%甲酸水溶液为流动相梯度洗脱,在ACQUITY UPLC DBH C18色谱柱上分离,串联四级杆质谱检测,MRM方式采集并定量。

This method can be used to determine the residue level of methanol, ethanol and toluene in aniracetam.

本方法可用于茴拉西坦中甲醇、乙醇和甲苯的残留量测定。

The influence of shapes of current loading cycles including rectangle,triangle and trapezium and magnitude and slope of increasing current on the cell voltage response were studied.

结果表明电池电压对各种电流变化的响应很快。动态负载时电池的开路电压要比稳态运行时的高,主要原因是因甲醇窜流造成的过电势的减少。

About 100% yield of cyclohexanemethanol could be obtained in the presence of triethylamine if adding more catalyst and prolonging the reaction time.

在三乙胺存在下,增大催化剂用量并延长反应时间,苯甲醛可以100%的收率转化为环己基甲醇,没有出现任何副产物。

Influences of derivatization condition are analyzed,such as concentration of boron trifluoride in the solution of methanol,reaction temperature and the reaction time.

阐明三氟化硼在甲醇中的浓度、反应温度和反应时间对衍生化效果的影响。

Treat each flask as follows. Add 5.0 mL of a solution prepared by dissolving 14 g of boron trifluoride in methanol to make 100 mL, swirl to mix, and reflux for 15 minutes or until the solid is dissolved.

在每一个锥形瓶中,加5.0mL三氟化硼溶液(取14g三氟化硼,用甲醇溶解并稀释至100ml),搅拌使混合,回流15分钟或直至固体物溶解。

When the ratio of methanol to oil is higher than 6, the tung oil transformation ratio improved slightly.

结果表明,当甲醇和油脂的物质的量之比超过6:1后,桐油转化率提高范围很小。

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