甲醇

LaCr_(1-x)M_xO_3(M=Co, Fe, Ni, Sn, Ti)and LaNi_(1-x)Ti_xO_3 compounds were synthesized by sol-gel technique in this paper. The thick film based sensors were fabricated and their gas-sensing properties were tested in the acetone, ethanol, normal propyl alcohol, carbinol, formaldehyde gases etc.

本文采用柠檬酸盐溶胶-凝胶法合成了LaCr_(1-x)M_xO_3(M=Co，Fe，Ni，Sn，Ti)和LaNi_(1-x)Ti_xO_3系列化合物的纳米粉体，并制备了厚膜型气敏元件，在丙酮、乙醇、正丙醇、甲醇、甲醛等有机气体中测试了它们的气敏性能。

Following are summary of our works:(1)The powders of LaCr_(0.9)Co_(0.1)O_3, LaCr_(0.9)Fe_(0.1)O_3, LaCr_(0.9)Ni_(0.1)O_3, LaCr_(0.95)Sn_(0.05)O_3 and LaCr_(1-x)Ti_xO_3(x=0.0-0.3) were single perovskite phase with orthorhombic structure. The gas-sensing properties of their thick film sensors were tested in the acetone, ethanol, normal propyl alcohol, carbinol and formaldehyde organic gases. The sensitivity of the sensors can not be enhanced effectively by doping Co、Fe、Ni、Sn elements in B-site of LaCrO_3. Ti dopant with proper concentration can greatly improve the gas-sensing properties, which make the sensor display higher sensitivity and quicker response-recovery characteristics.

所得结果摘要如下：(1)LaCr_(0.9)Co_(0.1)O_3、LaCr_(0.9)Fe_(0.1)O_3、LaCr_(0.9)Ni_(0.1)O_3、LaCr_(0.95)Sn_(0.05)O_3和LaCr_(1-x)Ti_xO(来源：ABfd1dC论文网www.abclunwen.com)_3(x=0.0-0.3)粉体为正交单相钙钛矿结构，其厚膜型气敏元件在350℃时对丙酮、乙醇、正丙醇、甲醇、甲醛等有机气体的气敏性能测试表明：0.1mol Co、Fe、Ni和0.05mol Sn元素在LaCrO_3的B位进行掺杂后，不能有效提高材料对以上测试气体的气敏性能；而Ti元素的适量掺杂可以极大地改善LaCrO_3的气敏性能，使之显示出对丙酮气体的高灵敏度和快速响应恢复能力。

The reaction rate of propylene oxide with water is much lower than that with methanol.

PO的水解反应比PO与甲醇的反应慢的多。

We had determined the reducing power of the three Boletes,in addition,the antioxidant effect on peroxidation of unsaturated fatty acid in lipoprotein,Fenton system and the self oxidation method of pyrogallol were measured in vitro,we also detected the compounds of antioxidant.

实验测定了三种牛肝菌甲醇提取物的还原力，以及在卵黄脂蛋白不饱和脂肪酸过氧化体系、Fenton体系和邻苯三酚自氧化体系中的体外抗氧化活性及其起抗氧化作用的物质。

On a ZORBAX Stable Bound (2.150 mm, 1.8 m), the rutin、quercitrin、quercitrin-3-O-giucoside and quercitrin-3-O-galactose could be separated completely with 0.05 mol/L potassium dihydrogen phosphate and methanol as mobile phase (40:60,V/V) at a flow rate of 0.3 ml/min and detected with a photodiode array detector .

在色谱柱为ZORBAX Stable Bound (2.150 mm， 1.8 m)，流动相为0.05 mol/L的磷酸二氢钾缓冲溶液-甲醇(40：60，V/V)，流速为0.3 ml/min，在检测波长为360 nm的色谱条件下，芦丁、槲皮素、槲皮素-3-O-葡萄糖苷和槲皮素-3-O-半乳糖苷分离效果好，方法灵敏度高，重现性好，用于测定雪莲果叶中的上述几种黄酮芦丁型黄酮，效果满意。

Synthesis of target compounds namely: to vanillic acid as the starting material with methanol under reflux conditions for 4 - hydroxy -3 - p-methyl, then ether, and nitration, reduction, cyclization reaction 6 - methoxy -7 - benzyloxy-quinazoline -4 - one, and then by the chloride in place of aniline, benzyloxy-off, such as etherification reaction of the target compounds; target compounds with the second and third occurrence of substitution reactions of amines by the TM1, that is, 4 - amino-benzene -6 - methoxy -7 - [2 - hydroxy -3 -(N, N-diethyl amino) oxy c] quinazoline; with ether occurred Ornidazole reaction of TM2, namely, 4 - amino-benzene -6 - methoxy -7 - [2 - hydroxy -3 -(2 - methyl -5 - nitroimidazole) C oxy] quinazoline.

本论文以嘌呤类似物喹唑啉为母核，分别在其4位和7位引入结构多样的取代苯氨基和柔性侧链，设计了一系列4-取代苯胺基-6-甲氧基-7-(2-羟基取代丙氧基)喹唑啉类化合物。目标化合物的合成即：以香草酸为起始原料，与甲醇回流条件下得到4-羟基-3-甲氧基苯甲酸甲酯，然后经过醚化、硝化、还原、环合反应得到6-甲氧基-7-苄氧基喹唑啉-4-酮，然后再经氯化、取代苯胺、脱苄氧基、醚化等反应得到目标化合物；目标化合物与二乙胺发生胺取代反应得到了TM1，即4-苯氨基-6-甲氧基-7-[2-羟基-3-丙氧基]喹唑啉；通过与奥硝唑发生醚化反应得到TM2，即4-苯氨基-6-甲氧基-7-[2-羟基-3-(2-甲基-5-硝基咪唑)丙氧基]喹唑啉。

In the case of racemate 2, better resolution was obtained when using 2-propanol as modifier in the place of methanol and ethanol, while for racemate 1, methanol provided the best performance. Both retention and resolution decreased with increase in pressure.

结果表明对映体的保留因子均随着改性剂含量的增加而显著下降，当改性剂含量大于10%时，保留因子的下降趋势变缓；分离帕罗酮酯时，异丙醇作改性剂的分离度和分离因子均最大，分离帕罗醇对映体时，甲醇是最佳的改性剂。

Objective To analyze the components of organic acids in the Radix Ranunculi Ternati from different methods. Methods With using 10%H2SO4-CH3OH as methyl esterification solvent, the analysis for organic acids were carried by using GC-MS . Results 46 components were determined.

目的 分析不同提取法提取的猫爪草有机酸部位的成分方法采用离子交换法提取分离水提液和醇提液中的有机酸，以10%硫酸甲醇溶液甲酯化试剂进行甲酯化，用气相色谱-质谱联用技术分析。

When the fuel runs out, you could instantly "recharge" by refilling the cell with methanol,.

霍克蒂说，当燃料用完的时候，你可以立刻给电池填充甲醇来充电。

Two sugars, rhamnose and sucrose, were found in the methanol extracts from yams and bulbils.

山药及零余子甲醇萃取物，可检测出醣组成含有鼠李糖与蔗。

This one mode pays close attention to network credence foundation of the businessman very much.

这一模式非常关注商人的网络信用基础。

Cell morphology of bacterial ghost of Pasteurella multocida was observed by scanning electron microscopy and inactivation ratio was estimated by CFU analysi.

扫描电镜观察多杀性巴氏杆菌细菌幽灵和菌落形成单位评价遗传灭活率。