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甲醇

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Methods: The analytical column was SHIMADZU VP-ODS C18 column(4.6 mm×150 mm, 5 μm) with a mobile phase consisted of 0.05 mol/L disodium hydrogen phosphate solution(85% phosphoric acid solution with pH adjustment to 2.5)-acetonitrile-methanol(42.5∶47.5∶10) at the flow rate of 1.0 ml/min, the detection wavelength was set at 254 nm.

色谱柱为SHIMADZU VP-ODS C18柱(4.6 mm×150 mm,5 μm),流动相为0.05 mol/L磷酸氢二钠溶液(用85%磷酸溶液调节pH值至2.5)-乙腈-甲醇(42.5∶47.5∶10),流速为1.0 ml/min,检测波长为254 nm。

Methods: The analytical column was SHIMADZU VP-ODS C18 column(4.6 mm×150 mm 5 μm) with a mobile phase consisted of 0.05 mol/L disodium hydrogen phosphate solution(85% phosphoric acid solution with pH adjustment to 2.5)-acetonitrile-methanol(42.5∶47.5∶10) at the flow rate of 1.0 ml/min the detection wavelength was set at 254 nm.

目的:建立丙酸氯倍他索尿素乳膏中丙酸氯倍他索含量的HPLC测定方法。方法:色谱柱为SHIMADZU VP-ODS C18柱(4.6 mm×150 mm5 μm)流动相为0.05 mol/L磷酸氢二钠溶液(用85%磷酸溶液调节pH值至2.5)-乙腈-甲醇(42.5∶47.5∶10)流速为1.0 ml/min 检测波长为254 nm。

Methods 7 kinds of antibiotics, dexamethasone phosphate disodium salt and salicylic acid were separated on a C18 column using methanol: acetonitrile-aqueous solutions:0.01mol/L oxalic acid=l1:22:67 as the mobile phase at a flow rate of 0.8ml/min, with the column temperature 25℃ and detection wave 240nm and 268nm.

采用C18色谱柱(4.6mm×250mm, 5μm),以甲醇:乙腈:0.01mol/L草酸=11:22:67为流动相,流速为0.8ml/min,检测波长为240和268nm,柱温为25℃,在此色谱条件下进行检测。

MTBE can be formed by addition of methanol to the double bond of isobutene.

MTBE可由异丁烯和甲醇经加成反应而合成。

Positive high yield expression recombinant was characterized by its drug-fast phenotype and methanol induction.

用抗药性表型和甲醇诱导筛选出重组蛋白表达阳性的转化X-33。

Direct methanol fuel cell is the most promising power generator for electric powered vehicles.

直接甲醇燃料电池是电动汽车最有保障的电源。

Uranium solution is obtained electrolytically by reducing uranyl ion on mercury cathode. The effect of the addition of various aminopolycarboxylic acids (such as EDTA, DTPA, CyDTA and TTHA) and organic water-miscible solvents (such as CH3OH, C2H5OH and CH3COCH3) on the stability of ura-nium in air has been investigated. The absorption spectra of uraniumand uraniumin 1 mol/l and 9mol/l hydrochloric acid solutions are examined.

本文采用汞阴极电解还原法制备了铀溶液,研究了在盐酸介质中各种氨羧络合剂乙二胺四乙酸二钠、二乙三胺五乙酸、1,2-环已烷二胺四乙酸、三乙基四胺六乙酸和水溶性有机溶剂甲醇、乙醇和丙酮的存在对铀稳定性影响,测定了在不同盐酸浓度中铀和铀的吸收光谱。

The technique and economic comparison between it and the technique of preparing hydrogen gas by water electrolyzation was carried out.

张玫概要阐述了甲醇裂解制氢的原理及其在山梨醇生产中的应用,并与水电解制氢进行了技术经济比较。

Procedure— Where the individual monograph specifies that the water content is to be determined by Method Ib, transfer 35 to 40 mL of methanol or other suitable solvent to the titration vessel, and titrate with the Reagent to the electrometric or visual endpoint.

规程---当各论规定使用方法Ib测定水的含量时,转移35~40ml的甲醇或者其他合适的溶剂至滴定容器中,用卡尔试剂滴定,以永停法或视觉观察终点。

Procedure— Unless otherwise specified, transfer 35 to 40 mL of methanol or other suitable solvent to the titration vessel, and titrate with the Reagent to the electrometric or visual endpoint to consume any moisture that may be present.

操作---除另有规定外,转移35~40ml的甲醇或其他合适的溶剂至滴定容器中,以永停法或视觉指示终点,用卡尔试剂滴定可能存在的水汽(所消耗体积忽略不计,因为不会代入到公式计算),快速加入测试样本,混匀,然后再次用卡尔试剂滴定到终点。

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