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This article provided a new route to produce 4-dimethoxy phenethylamine. In basic condition, the product could be obtained through etherization, bromation, Grignard reaction, hydroxyethylation, esterification and Gabriel reaction with phenol as raw material, the overall yield is 45.0%.

提出了合成4-甲氧基苯乙胺的新方法,即在碱性条件下,苯酚首先与硫酸二甲酯反应,再选用高选择性的溴化剂溴化后,经格氏反应、羟乙基化反应和酯化反应,最后经Gabriel反应可以制备目标产物,反应总收率为45.0%。

Poly with sulfonic acid groups were readily synthesized with biphenol and 1,3-bis(4-fluorobenzoyl)benzene in the presence of excess potassium carbonate followed by sulfonation with chlorosulfonic acid.

以二氯二苯甲烷和2,6-二甲基苯酚为原料合成了含有阻碍基团的双酚单体,用此双酚单体和1,3-二(4-氟苯甲酰基苯)在无水碳酸钾存在的条件下反应制得聚芳醚酮,然后用氯磺酸磺化,控制反应条件,使磺酸基团恰好进入苯环对位,制得新型结构的磺化聚芳醚酮。

Phenylenediamines, aminophenols, methoxyanil ines, and 1,4- hydroquinone, 1-naphthylamine were polymerized via the catalysis of horseradish peroxidase in mixed solvents of l,4-dioxane and water at amibient conditions by using hydrogen peroxide as the oxidant. Several factors influencing the polymer yield, such as the concentration of the substrate, pH value and oxidant amount were examined using a- phenylenediamine as substrate.

本文选择了苯二胺、氨基苯酚、甲氧基苯胺三个系列,以及对苯二酚、1-萘胺等单体,在二氧六环-水混合介质中以辣根过氧化物酶为催化剂,以双氧水为氧化剂进行了不同底物的室温酶促聚合,并以邻苯二胺为底物考察了溶剂用量、pH值、作为氧化剂的双氧水用量等条件对聚合物收率的影响。

In this paper,pyromellitic dianhydride,1,2,3,4-cyclobutanetetracarboxylic dianhydride,4[(4-aminophenyl)-bis(4-methoxyphenyl)methyl]benzeneamine,4-hexyloxy-biphenyl-3′,5′-diaminobenzoate,and additive ADD-34 were used to synthesize four PIs.

文章用均苯四甲酸二酐,4[(4-氨基苯基)-二(4-甲氧基苯基)甲基]苯胺,1,2,3,4-环丁烷四羧酸二酐,4-己烷氧基联苯酚-3′,5′-二胺基苯甲酸酯和不同含量的添加剂制备了聚酰亚胺液晶取向剂。

A diazo coupled spectrophotometry for the determination of nitrite was reported in this work. Some experimental conditions were studied.

建立了邻甲氧基苯酚重氮偶联分光光度法测定水基切削液及机械加工废水中亚硝酸盐的方法。

DATA SYNTHESIS: From the synthesis materials we found that there was little progress on the drug treatment of muscular spasm of cerebral palsy in recent years. The main drugs for treatment still were valium, baclofen, tizanidine, anhydrous alcohol, phenol, A-type borulinus toxin etc. common used drugs.

资料综合:综合资料发现近几年脑性瘫痪肌痉挛的药物治疗进展不多,治疗的主要药物仍然是苯甲二氮草、巴氯芬、替扎尼定、无水乙醇、苯酚、A型肉毒毒素等常用药物,给药的途径主要有口服、鞘内注射或肌肉注射。

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Yang yinshu、Wang xiangsheng、Li decang,The first discovery of haemaphysalis conicinna.

1〕 杨银书,王祥生,李德昌。安徽省首次发现嗜群血蜱。

Chapter Three: Type classification of DE structure in Sino-Tibetan languages.

第三章汉藏语&的&字结构的类型划分。