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And then we found that ytterbium trifluoromethethanesulfonate is a powerful catalyst for the reaction of amine and ethyl acetate.

然后研究了三氟甲磺酸镱催化的胺和乙酸乙酯的反应,从而合成了乙酰苯胺类化合物。

It was found that,under comparable conditions,the rate of formation of N-carbobenzoxy-L-serine anilide is the...

在最适pH,酶浓度自1.31毫克蛋白N/毫升反应液提高到2.27毫克蛋白N/毫升反应液时,N-苯甲氧羰酰-L-丝氨酸酰苯胺的产率,在24小时自76.43%提高到100%。

The 3-chloro-4-trifluoromethoxy benzonitrile was synthesized from 3-chloro-4-trifluorome- thoxy aniline by diazotization, formaldoximation ,hydrolysis and cyanation.

以3-氯-4-三氟甲氧基苯胺为原料,经重氮化、甲醛肟化、水解和腈化反应得到纯度≥99。

Methodological furan and reaction of Diels-Alder of course of Ma Lai anhydride are generated go armour goes element of hydrogenous Chinese blister beetle, reductive below palladium charcoal catalysis into go element of armour Chinese blister beetle, with replace aniline condensation to become nitrogen - phenyl goes acyl of armour Chinese blister beetle inferior the ramification of amine.

方法呋喃和马来酐经过Diels-Alder反应生成去甲去氢斑蝥素,在钯炭催化下还原成去甲斑蝥素,和取代苯胺缩合成氮-苯基去甲斑蝥酰亚胺的衍生物。

Teflubenzuron was synthesized from 2,4-difluoronitrobenzene and 2,6-dichlobenil as starting reagent through six-step reaction with the yield of 75.3%.3,5-Dichloro-2,4-difluoroaniline was synthesized by chlorination,reduction reaction from 2,4-difluoronitrobenzene,the yield was 84.5%;2,6-difluorobenzamide with the yield of 87.7% was synthesized by fluoridation and hydrolysis from 2,6-dichlobenil.

以2,4-二氟硝基苯和2,6-二氯苯腈为起始原料,经过6步反应合成伏虫隆,总收率为75.3%。以2,4-二氟硝基苯为原料,经过氯化、还原反应合成3,5-二氯-2,4-二氟苯胺,产率为84.5%;以2,6-二氯苯腈为原料,经过氟化和水解,制得2,6-二氟苯甲酰胺,产率为87.7%;将Ⅱ与二碳酸酯酰化,合成2,6-二氟苯甲酰异氰酸酯,产率为91.3%;Ⅲ与Ⅰ加成,得到杀虫剂伏虫隆,产率为95%。

Commercially available 2 nitro 4 methoxyaniline was used as starting material and converted via reduction with zinc dust and cyclization with potassium ethyl xanthate into the title compound,suggesting that this procedure is suitable for industrial production.

以4 甲氧基 2 硝基苯胺为原料,经锌粉还原后,再与乙基黄原酸钾环缩合制得2 巯基 5 甲氧基 1H 苯并咪唑。结果收率80%。结论该方法简单易行,适合工业化生产。

Off-line HPLC coupled with MS gives the result that 4-chlorophenyl urea and 2-chloro-N-(4-chlorophenyl) benzamide are two photoproducts. In comparison with their retention times and UV specta with those of standards, some other photoproducts identified are 2-chloro benzamide, 4-chlorophenyl urea and 4-chloro aniline.

收集光解产物各级分,采用直接进样法在MS上测得其中的二种光解产物为对氯苯基脲和N-邻氯苯甲酰胺:通过与标样在同样HPLC条件下的保留时间和UV吸收光谱相对照,证明产物中存在有邻氯苯甲酰胺、对氯苯基脲和对氯苯胺等。

Huapai products:pchlorophenol,ochlorophenol,2,4dichlorophenol,2,6dichlorophenol,2,4,5trichlorophenol,2,4,6trichlorophenol,4chloro2benzyl phenol,pbromophenol,2,4,6tribromophenol,1chloro4(1,1dimethyl ethyl) benzene ether,3bromoanisole,mbromofluorobenzene,2tetra hydrofuran,αbromo4chloro acetophenone,αbromo4methoxy acetophenone,4chloro benzophenone,4chloro2methylaniline,n(2hydroxyethyl)ethane diamine; n(2aminoethyl)ethanolamine,2,3dibromopropionyl chloride,4bromo benzene sulphonyl chloride,terephthaloyl chloride,isophthaloyl chloride,nchlorosuccinimide,nbromosuccinimide,pchloranil;tetrachloro1,4benzoquinone,5chloroisatin.

华派公司产品:对氯苯酚,邻氯苯酚,2,4二氯苯酚,2,6二氯苯酚,2,4,5三氯苯酚,2,4,6三氯苯酚,4氯2苄基苯酚,对溴苯酚,2,4,6三溴苯酚,对氯苯基叔丁基醚,间溴苯甲醚,间溴氟苯,α溴甲基四氢呋喃,α溴代4氯苯乙酮,α溴4甲氧基苯乙酮,4氯二苯甲酮,4氯2甲基苯胺,N(2羟乙基)乙二胺, 2,3二溴丙酰氯,对溴苯磺酰氯,对苯二甲酰氯,间苯二甲酰氯,N氯代丁二酰亚胺,N溴代丁二酰亚胺,四氯苯醌,5氯靛红。

PANSA nanoparticles were synthesized by oxidative copolymerization of aniline and 2-methoxyaniline-5-sulfonic acid in 1.0 mol/L HCl aqueous solution with ammonium peroxydisulfate as oxid...

PANSA纳米颗粒通过化学氧化聚合法,在无乳化剂或稳定剂存在下,以过硫酸铵为氧化剂,在1.0m ol/L盐酸水溶液中由苯胺与2-甲氧基苯胺-5-磺酸合成得到。

Nine sugars and five sugar alcohols were analysed by HPLC with a differenctial refractometerdetector. p-Methoxyaniline and benzoyl chloride were used to the pre-column derivatization of sugar and sugar alcohol, in which a ultraviolet absorption organic group was added, Then the derivatives were detected sensitively by an UV monitor sensitively.

采用高效液相色谱示差折光检测器,对9种糖和五种糖醇进行了分离检测;另以对甲氧基苯胺和苯甲酰氯为衍生试剂,分别对糖和糖醇进行柱前衍生,使其接上紫外吸收基团,然后用紫外检测器进行检测。

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This one mode pays close attention to network credence foundation of the businessman very much.

这一模式非常关注商人的网络信用基础。

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