甲苯

Bis-imidazoline was prepared from triethylene tetraamine and N,N-dimethylformamide dimethyl acetal at 85℃ for 2 h with toluene as solvent, with a yield of 90.4%. The reaction of bis-imidazoline with 1,2-dibromoethane and potassium carbonate in acetonitrile provided with a monobromide salt yield of 78.7%. Hydrolysis of monobromide salt under aqueous causic solution formed 1,4,7,10-tetraazzcyclododecane in a 74.2% yield.

用甲苯作溶剂，使三乙烯四胺和N，N-二甲基甲酰胺二甲基缩醛在85℃反应2 h，得到中间体双咪唑啉，产率90.4%，在乙腈溶剂中，碳酸钾存在下，双咪唑啉和1，2-二溴乙烷进行扩环反应，得到环状中间体一溴盐，产率78.7%，一溴盐经碱性水解2 h，得到1，4，7，10-四氮杂十二烷，产率74.2%。

The optimum conditions of reaction of each reaction:(1) The synthesis condition of PS with monocarboxylic acid terminated is that the mole ratio reatant of FeCl2·4H2O/chloroactic acid was 2.0, the reaction temperature 110℃, the reaction time

各步的最佳聚合反应条件：(1)mPEG与丁二酸酐反应最佳条件：溶剂为甲苯

The process of esterification of propylene glycol monomethyl ether with acetic acid to synthesize propylene glycol monomethyl ether acetate is investigated using 98% sulfuric acid as catalyst.

研究了以浓硫酸为催化剂，丙二醇甲醚和醋酸酯化合成丙二醇甲醚醋酸酯的过程，考察了醚和酸比例、催化剂用量等因素对反应的影响，并选择甲苯为水萃取剂。

Mononitration, dinitration and trinitration of toluene are very important reactions. Products of these reactions are widely used in medicine, dyestuff, explosive, pesticide, etc.

甲苯的多段硝化是重要的化学反应过程，其各段硝化产物在医药、染料、炸药、农药等方面应用广泛。

Results indicate that the severity of a loss of control for mononitration of toluene by mixed acid can be reduced from medium to low by using semi-batch reactor, the reaction is 1.2 kinetic order in toluene, 1.3 order in nitric acid and 2.5 order in all. The MTSR_max under setting operating conditions are all in the range that can be accepted by the industrial nitration, so the reaction has less hazard potential by using those setting conditions.

分析结果表明：在设定的工艺条件下，反应过程中对甲苯的反应级数是1.2级反应，对硝酸是1.3级反应，采用半间歇反应可以使失控反应的严重度等级从中等降低到低等，在设定操作条件下假定反应失控所引发的MTSR_是在工艺条件允许的范围之内，不具有很大的危险性。

Effects of sonic factors, including dosage of catalyst, calcination temperature of catalyst, nitrated reaction time and recovered catalyst, on the selectivity of toluene in mononitration at the presence of silicotungstic acid catalyst were studied by gas chromatography.

通过气相色谱研究了诸如催化剂用量、催化剂焙烧温度、硝化反应时间、硝化反应温度及催化剂的重复使用等因素对甲苯硝酸硝化区域选择性的影响。

The catalyzed isomerization without the presence of hydrogen occurs over M-2 composite mordenite in the self-designed tube reactor, which use 1,2,4-trimethylbenzen as raw materials.

非临氢催化异构化反应试验采用研制的M-2型复合丝光沸石催化剂，以高纯偏三甲苯油为原料，在设计的管式反应器中进行。

The nitration of toluene was carried out in the presence of acetic anhydride with CCl4 as solvent, 95% nitric acid as nitrating reagent, and niobic acid calcinated at 300℃ for 3 h as catalyst for 60 min at 40℃.

实验结果表明，当反应温度为40℃，反应时间为60min时，以CCl4为溶剂，以质量分数为95%的硝酸为硝化剂，在醋酐存在条件下，以经300℃焙烧3h后的铌酸作为催化剂，甲苯硝化产物中异构体的邻对比达1.26，较硝硫混酸的1.67显著降低，产物得率达99.3%。

The effects of all kinds of factors, just like calcination temperature of niobic acid catalysts, nitration reaction time, nitration reaction temperature, recovered catalyst, acetic anhydride and concentration of nitric acid were studied by gas chromatography.

研究了催化剂焙烧温度、硝化反应时间、硝化反应温度、有无醋酸存在、硝酸浓度、催化剂的重复使用等因素对甲苯硝化反应影响。

In this paper,ortho nitrobenzaldehyde is prepared with indirect oxo-process for o nitrotoluene .

以邻硝基甲苯为原料，采用间接氧化法制备邻硝基苯甲醛。

Finally, according to market conditions and market products this article paper analyzes the trends in the development of camera technology, and designs a color night vision camera.

最后根据市场情况和市面上产品的情况分析了摄像机技术的发展趋势，并设计了一款彩色夜视摄像机。

Only person height weeds and the fierce looks stone idles were there.

只有半人深的荒草和龇牙咧嘴的神像。