甲胺

Seven Schiff bases of N-(4-hydroxyphenylmethylene)-1-naphthylamine, N-(4-hydroxyphenylmethylene)-p-methoxyaniline, N-(4-hydroxyphenylmethylene)-benzylamine, N-(4-hydroxy-3-methoxyphenylmethylene) furfurylamine, N-(4-hydroxy-3-methoxyphenyl methylene)-p-methylaniline, N-(4-hydroxy-3-methoxyphenylmethylene)-p-methoxyaniline and N-salicylidene-4-aminoantipyrine were first synthesized by the one step solid phase reactions between aromatic aldehydes with phenolic hydroxyl and amines at room temperature without solvent.

分别以带酚羟基的芳醛与胺类反应，首次通过室温固相反应一步合成了N-（4-羟基苯基亚甲基）-1-萘胺、N-（4-羟基苯基亚甲基）-对甲氧基苯胺、N-（4-羟基苯基亚甲基）-苄胺、N-（4-羟基-3-甲氧基苯基亚甲基）糠胺、N-（4-羟基-3-甲氧基苯基亚甲基）-对甲苯胺、N-（4-羟基-3-甲氧基苯基亚甲基）-对甲氧基苯胺和N-亚水杨基-4-氨基安替比林7种Schiff碱，反应15min完成，产率均超过90％。

Three series of segmented polyurethanes were synthesized, which are based on 4,4'-methylene-di, N-methyl diethanolamine and hydroxy terminated poly-butadiene, poly or poly.

本文讨论了以聚环氧乙烷、聚环氧丙烷以及聚丁二烯为软段，以4，4'-二异氰酸二苯甲烷和N，N-二羟乙基甲胺为硬段的链段型聚氨酯的合成。

The research aimed to establish a FIPIX method for the determination of fipronil and acephate in 36% emulsifiable concentrate.

［目的］建立在同一液相色谱条件下测定混刹中氟虫腈和乙酰甲胺磷含量的方法。

Good thermal stability and self-extinguishing behavior was observed with the cured polybenzoxazine resins. Second, furan-containing benzoxazine monomers, P-FBz, BPA-FBz, and 4FP-FBz were prepared using furfurylamine as a raw material. Formation of furfurylamine Mannich bridge networks in the polymerizations of P-FBz and BPA-FBz increased the cross-linking densities and thermal stability of the resulting polybenzoxazines. P-FBz and BPA-FBz- based polymers also exhibited high glass transition temperatures above 300℃, high char yields, and low flammability with a limited oxygen index value of 31. The dielectric (Dk3.21–3.39) and mechanical properties (high storage modulus of 3.0–3.9 GPa and low coefficient of thermal expansion of 37.7– 45.4 ppm) of the P-FBz and BPA-FBz-based polymers were superior or comparable to other polybenzoxazines. 4FP-FBz used for polybenzo- xazine modification by means of formation of benzoxazine hybridation with P-FBz.

第二部份以2-呋喃甲胺为起始物，制备了P-FBz、4FP-FBz与BPA-FBz 三个含呋喃官能基之氧代氮代苯并环己烷的单体；BPA-FBz与P-FBz於开环聚合中形成之Mannich bridge网状结构有效地提升聚氧代氮代苯并环己烷聚合物之交联密度与热安定性；Poly与Poly具有大於300℃之玻璃转移温度、高的焦炭生成率与具有31之极限氧指数(Limited oxygen index， LOI)的难燃性特质，Poly与Poly之介电常数(Dk=3.21~3.39)与机械性质[3.0~3.9 GPa的储存模数与37.7~45.4ppm之低热膨胀系数( Low coefficient of thermal expansion， Low CTE)]均较其他聚氧代氮代苯并环己烷为优；4FP-FBz具有低之介电常数(Dk=2.7)，以其作为降低介电常数之反应型改质剂，与P-FBz混成，证实可有效地降低Poly的介电常数。

Results］ LD50 for acephate by intragastric administration is 823 mg/kg in rats.

结果］乙酰甲胺磷大鼠经口LD50为823 mg/kg。

The catalytic performance of mordenite exchanged by calcium ion is superior to the domestic commercial product. This CaHM was prepared by being roasted with adhesive, and can be directly used in pilot plant.

自制的这种钙离子改性丝光沸石催化剂的催化性能优于目前国内工业化的甲胺生产催化剂，而且CaHM是经添加粘接剂焙烧成型的样品，可直接供产品的中试放大。

With Zn〓 used as an internal standard, the contents of Ni, Co, Cu in real mineral samples were determined successfully in the imidazole or phenylamine systems.

以Zn〓作内标，采用内标标准曲线法分别在咪唑和苯甲胺缓冲液体系中对镍矿样中Ni，Co，Cu的含量进行了测定。

In Chapter 3, the separation of Fe〓, Co〓, Ni〓, Zn〓, Cu〓 by CE in the presence of imidazole or phenylamine as UV-absorbing background electrolyte and α-hydroxybutyric acid as the complexing agent with indirect UV absorbance was investigated.

在第三章，研究了以咪唑或苯甲胺为背景吸收电解质，α-羟基异丁酸为络合剂，采用毛细管离子电泳间接紫外法测定了镍矿石中Ni，Co，Cu的含量。

Kosmotropes are stabilizing solutes which increase the order of water (such as polyhydric alcohols [ 307 ], trehalose, trimethylamine N -oxide, glycine betaine, ectoine, proline and various other zwitterions) whereas chaotropes create weaker hydrogen bonding, decreasing the order of water, increasing its surface tension and destabilizing macromolecular structures (such as guanidinium chloride and urea at high concentrations).

这是稳定增长kosmotropes溶质水秩序(如多元醇〔307〕、海藻糖、甲胺氮氧化物、甜菜碱、ectoine，脯氨酸和其他各种盐)而创造chaotropes氢键较弱，为了减少用水，增加其表面张力和大分子结构不稳定。

Pbo significantly synergizes fenvalerate、cypermethrin and methomyl against Xihua field resistant strain ofHelicoverpe armigera , TPP can somewhat synergize pyrethroids also.

对西华田间棉铃虫抗性种群，Pbo能显著地增加氰戊菊酯、氯氰菊酯、灭多威的毒力，大幅度地降低其致死中量，TPP对两种拟除虫菊酯杀虫剂也表现一定的增效作用；对甲基对硫磷、甲胺磷，无论是Pbo还是TPP其增效作用均十分有限。

The reasons of iron ions content overproof in grade Ⅱ desalting water system,such as variation water quality,contamination of regenerant , operation adjustment of pretreatment system and switching operation of bed were discussed.

对二级脱盐水系统中铁离子含量超标的原因，如来水水质发生波动、再生剂受到污染、预处理系统操作调整、床体运行切换等进行了论述。

You were hired to drum up new business, so go and do it.

公司雇你招徕新业务，你就做你的事好了。