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Lead selenide nanocubes were successfully prepared on a large scale via a facile solvothermal route using formamide as both solvent and complexing agent.

用甲酰胺作溶剂和配位剂,通过温和的溶剂热路线成功地大量合成了PbSe纳米立方块。

By synthetically analysizing the physical and chemical properties of all components and particle size, the content of F2641 in the JOB-iC is determined by gravimetric analysis after F2641 is seperated from HMX,TATB and PNP through ? alkali reflux. Determination conditions is set as follows the sample is boilingly refluxed for six hour in a constant temperature bath after adding lOOm! 8.0 ?? 0.1% NaOH. The solvent DMF saturated by TATB is used for extracting HMX,F21 and PNP from the sample and TATB is seperated by crucible filter G4. The mass precent of TATB is determined by extraction fractionation. The mass percent of PNP is measured by multiwavlength linear regression ultraviolet spectrophotometry. The testing conditions are set as follows:multiwavlength constitution: X=267nxn, 275nm, 283nm, 29mm, 299nm,the application scope of the Lambert-Beer law: the concentration of PNP is O.005?0.O25mgIml, the concentration of HMX is 0.060.3Omg/ml,absorption coefficents of PNP and HMX are solved by the slope of linear regression curve of absorbency- concentration of standard solution of PNP and HMIX for measuring wavelengthes,on the basis of the Lanibert-Beer law and absorbancy additivity principle, the slope of linear regression curve of A/E(1) and E1 of PNP and HMX solution is regarded as the concentration of PNP in the solution.

根据传爆药中各组分的物理、化学性质及主体炸药的粒度大小,进行综合分析,确定了采用碱回流重量法测定JOB-1C 中F_(2641)的含量,测定条件:加入100ml浓度为8.0±0.1%的氢氧化钠,在恒温水浴中煮沸回流6h;采用溶剂萃取法测定JOB-1C中TATB的含量,选择TATB饱和的二甲基甲酰胺为萃取溶剂,用G4坩埚式过虑器进行萃取分离;采用多波长线性回归紫外分光光度法测定JOB-1C中PNP的含量,通过实验确定了多波长组合:λ=267nm,275nm,283nm,291nm,299nm;朗波—比耳定律的适用范围为PNP浓度:0.005~0.025mg/ml,HMX浓度:0.06~0.30mg/ml;在测定波长下,对PNP、HMX标准溶液的吸光度—浓度进行线性回归,由回归曲线的斜率得出PNP、HMX的吸收系数;根据朗波—比耳定律和吸光度加和性原理,在测定波长下,对PNP、HMX 两组分混合溶液A_i/E_HMX(i与E_PNP(i/E_HMX(i进行线性回归,回归曲线的斜率即为混合溶液中PNP的浓度。

The same is carried out in the microwave, ethanol, dichloroethane, sodium carbonate, tetrabutylammonium iodide ammonium dissolved in dimethylformamide, then access to carbon dioxide.

同样是在微波炉中进行,把乙醇,氯乙烷,碳酸钠,四丁基碘化铵溶解在二甲基甲酰胺中,再通入二氧化碳。

The results obtained by electron microscopic observation show that the supercoiled pUC18 DNA adopts a doughnut-like solenoidal structure with outside diameter about 43.8 nm and inside diameter about 2.0 nm in ammonium acetate-H2O medium.

观察结果显示:在疏水性的甲酰胺-水展开系统中,DNA采取通常的互缠式结构;在含有1.5 mmol/L醋酸铵的水介质中制备的超螺旋DNA标本,DNA采取线圈型结构,测得pUC18 DNA分子这种结构的外直径约为43.8 nm,内直径约为2 nm。

Methods: Analyses are based on the adolescent a subsample (ages 12-17, N=19430), of a nationally representative community survey.

目的 :评价美国青少年中 Ecstasy ( 3,4-亚甲二氧基甲基苯丙胺, MDMA ,即"摇头丸")使用与心理障碍的共病形式,调查个体、家庭和社区水平的相关危险和预防因素。

The products include two series: Sulfa drugs Industrial Sulfanilamide, Crystel Sulfanilamide, Sulfaguanidine, Sulfadimidine(Sodium, Sulfadiazine, Sulfathiazole Sodium, Sulfaquinoxaline Sodium, Sulfameter Dimethyl Sulfate, Nitromethane, Hydroxylamine Hcl.

本公司专业生产化工、医药中间体,产品主要包括磺胺(工业磺胺、结晶磺胺、磺胺脒、磺胺二甲嘧啶、磺胺嘧啶、磺胺噻唑钠、磺胺喹噁啉钠、磺胺五甲氧嘧啶)及硫酸二甲酯(硫酸二甲酯、硝基甲烷、烟酸羟胺)两大系列。

Ethanol was substituted for N,N-dimethyl sulfoxide as solvent of colouring agent pyrazolone and better results were obtained.

改用无水乙醇代替N,N-二甲基甲酰胺作为显色剂吡唑啉酮的溶剂,效果更好。

Both styrene conversion and epoxide selectivity can be obviously improved when a solution of N,N-dimethylformamide and dimethyl sulfoxide with an appropriate proportion is used.

使用适当比例的N,N-二甲基甲酰胺和二甲亚砜的混合溶剂能够显著提高苯乙烯的转化率和环氧化物的选择性。

In endemic disease preventive medication over the period at risk using 500 to 800g of tetracycline or trimethoprim/sulpha 400g/tonne in-feed may be used but it would be advisable to identify the major bacteria involved and determine their antibiotic sensitivities.

在高风险期需针对地方性疾病采取预防性用药措施,可在每吨饲料中添加500至800克四环素或400克甲氧苄胺嘧啶/磺胺。但建议用药前分离确定主要的病源并进行药敏试验。

In rats treated neonatally with monosodium glutamate the leu-enkephalin and norepinephrine contents in the brain and spinal cord did not change obviously, but the dopamine content of the telencephalon increased significantly, as compared with the control.

本工作分别采用新生期大鼠注射谷氨酸-钠损毁弓状核区及电刺激弓状核区的方法,观察对脑和脊髓内亮-脑啡肽、多巴胺和去甲肾上腺素含量的影响。

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What would he tell Judith and the children?

他将怎样告诉朱迪丝和孩子们呢?

I this is at that time, the opinion with peacockish true girl is full of in a heart.

这就是当时的我,一个心中布满虚荣的女孩子真实的想法。

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哦,我还给我自己买了一个新笔记本"他说。"