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Fig. 6 shows that N,N-dimethylformamide is, undoubtedly, the best entrainer.

图 6表明N,N-二甲基甲酰胺毫无疑问是最好的共溶剂。

Therefore, operating the separation sequence at feed ratio optimum requires less entrainer when we use N,N-dimethylformamide.

因此,当我们使用N,N-二甲基甲酰胺作为共溶剂时,在最佳混配比下进行分离操作需要共溶剂的量较少。

The adsorption and desorption behaviors of S-metolachlor in three different soils were investigated using the batch equilibration method.

采用平衡振荡法研究了精异丙甲草胺在粘壤土、粘土及砂壤土中的吸附和解吸附行为。

This article provided a new route to produce 4-dimethoxy phenethylamine. In basic condition, the product could be obtained through etherization, bromation, Grignard reaction, hydroxyethylation, esterification and Gabriel reaction with phenol as raw material, the overall yield is 45.0%.

提出了合成4-甲氧基苯乙胺的新方法,即在碱性条件下,苯酚首先与硫酸二甲酯反应,再选用高选择性的溴化剂溴化后,经格氏反应、羟乙基化反应和酯化反应,最后经Gabriel反应可以制备目标产物,反应总收率为45.0%。

The results show that these derivatives can be obtained in the yield of over 90% in the presence of DMF when using ethyl acetate as a catalyst.

结果表明,以N,N-二甲基甲酰胺为溶剂,以乙酸乙酯为催化剂的合成路线,均可以以90%以上的得率合成出上述化合物。

The calculated IC times of chl-a in ethyl acetate, tetrahydrofuran and dimethyl formamide are 141, 147, and 241 fs, respectively.

计算得到的叶绿素a分子在乙酸乙酯、四氢呋喃和二甲基甲酰胺溶剂中的内转换时间分别是141、147和241 fs。

Effects on the reaction of factors such as reactant ratio, reaction time, and reaction temperature were investigated, and optimum reaction conditions were determined as follows: mole ratio of cyanuric chloride to ethylamine to sodium hydroxide to sodium methyl mercaptide was 1:2.1:2.0:1.7, and the temperature and time of the first, second, and third substitution reactions were -2, 0, and 82℃ and 30, 60, and 180 min, respectively.

讨论了原料配比、反应时间和反应温度等因素对反应的影响,获得了较佳的反应条件。较佳反应条件为三聚氯氰:乙胺:氢氧化钠:甲硫醇钠=l:2.1:2.0:1.7,第一、第二、第三取代反应的反应温度和反应时间分别为-2℃、0℃、82℃和30、60、180min。

Simetryne is synthesized from cyanuric chloride, ethylamine and sodium methyl mercaptide in solution of the trichloroethylene.

以三聚氯氰、乙胺和甲硫醇钠为原料,以三氯乙烯为溶剂制备了西草净。

The appropriate conditions are that the mole ratio of cyanuric chloride to ethylamine, sodium hydroxide, sodium methyl mercaptide is 1:2.1:2.1:4.0, the temperature and time of first, second, third substitution reaction is respectively 0℃, 20℃, 78℃ and 10min, 30min, 480min.

适宜反应条件为三聚氯氰:乙胺:氢氧化钠:甲硫醇钠=1:2.1:2.1:4,第一、第二、第三取代反应的反应温度和反应时间分别为0,20,78℃和10,30,480min。

Simetryne was synthesized from cyanuric chloride, ethylamine, and sodium methyl mercaptide in a 50% isopropanol + water solution.

以三聚氯氰、乙胺和甲硫醇钠为原料,以50%异丙醇+50%水为溶剂制备了西草净。

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