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And then we found that ytterbium trifluoromethethanesulfonate is a powerful catalyst for the reaction of amine and ethyl acetate.

然后研究了三氟甲磺酸镱催化的胺和乙酸乙酯的反应,从而合成了乙酰苯胺类化合物。

In this thesis, a convenient and efficient synthesis of highly functionalizeddihydropyrido[2,3-d]pyrimidines via a double [5 + 1] annulation strategy startingfrom easily available α-alkenoyl-α-carbamoyl ketene--acetals 1 and cheapreagents (NH4OAc, DMF, and POCl3) has been developed.

本论文探索了一种简便有效的合成高度官能化的二氢吡啶并[2,3-d]嘧啶的方法,此方法由易得的α-乙酰基-α-氨基乙酰基二硫缩烯酮1和便宜的试剂(醋酸铵,二甲基甲酰胺和三氯氧磷)通过两步[5 + 1]加成而实现。

We perennially deal in PEG, MPEG, Ethyleneamines and the ramification of Ethyleneamines, NP,OP, AEO, specialty surfactants(2A1, CF-10), DOW CORNING antifoam, PE Homopolymer, HEC, latex compounds for the carpet and rug, etc.

我司常年经销产品:聚乙二醇及甲氧基聚乙二醇系列、乙烯胺系列及其衍生物、烷基酚聚氧乙烯醚、脂肪醇聚氧乙烯醚、二苯醚二磺酸盐(2A1)、X-405、CF-10等表面活性剂、道康宁消泡剂、羟乙基纤维素、地毯胶等。

The graft copolymer has an optimum effect of pour point depressing for the Daqing crude oil when it was synthesized under the conditions of that the mole ratio of EVA and octadecyl maleimide was 1:20, mass fraction peroxidation benzoin formyl was 2.5%, polymerization time was 6h, and the polymerization temperature was 90℃.

以目标物的降凝幅度为评价指标,优选出适合的合成条件为:EVA与十八烷基马来酰亚胺的摩尔比为1:20,引发剂过氧化二苯甲酰的量为2.5%,聚合时间6h,聚合温度为90℃。

The title compound (C21H15N5O) was obtained by the reaction of 3-methyl-1-phenyl-1H-pyrazol-5(4H)-one and 4-(2,2-dicyanovinyl)benzonitrile in water in the presence of TEBA and by recrystallization from EtOH(95%) and DMF.

水溶剂中,在三乙基苄基氯化铵存在下,由3-甲基-1-苯基-1H-吡唑-5(4H)-酮和4-(2,2-二氰基)苯基氰合成并经N,N-二甲基甲酰胺与95%乙醇的混合溶剂重结晶得到化合物C21H15N5O的晶体。

Keywords amorphous nickel aluminium alloy catalyst;benzonitrile;benzylamine;catalytic hydrogenation

非晶态镍铝合金催化剂;苯甲腈;苄胺;催化加氢

We provide intermediates of Methylphenidate HCl: 2-Phenyl-2-(2-Piperidyl) Acetamide; 2-Phenyl-2-(2-Piperidyl) Acetic Acid; Series of Benzoic Acid、Benzonitrile; Other pharmaceutical intermediates.

提供盐酸利他林中间体:2-苯基-2-(2-哌啶基)乙酰胺;2-苯基-2-(2-哌啶基)乙酸;苯甲酸、苯甲腈系列及其他医药中间体。

A kinetic study on the photopolymerization of MMA with benzophenone/triethylamine/mer-captan system as initiator has been carried out in the presence of oxygen.

采用二笨甲酮/三乙胺/硫醇体系作为引发剂,在含氧条件下进行了MMA光聚合反应的动力学研究。

METHODS 3-methoxy-7α-methylestra-1,3,5(10)-trien-17β-ol was reducted with lithium and ammonia,then the intermediate was hydrolyzed in oxalic acid and reacted with malonic acid to get 3,3-dimethoxo-7α-methylestra-5(10)-en-17-ol(compound 4),which was oxidated by pyridium bichromate ,reacted with acetylene,and hydrolyzed in oxalic acid again to get the product tibolone.

方法以3-甲氧基-7α-甲基雌甾-1,3,5(10)-三烯-17β-羟基为起始原料经锂胺还原、草酸水解、缩酮化得3,3-二甲氧基-7α-甲基雌甾-5(10)-烯-17β-羟基(化合物4),然后用温和的氧化剂重铬酸吡啶盐氧化、炔化、再水解得目的产物。

Binding constants of ligand-receptor with fours ligands adrenaline hydrochloride,noradrenaline bitartrate,propranolol hydrochloridea and salbutamol sulfate were determined by frontal chromatography.

用前沿色谱法测定了硫酸沙丁胺醇、重酒石酸去甲肾上腺素、盐酸肾上腺素和盐酸普萘洛尔与β_2-AR的结合常数。

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你知道吗,我需要你回来

Yang yinshu、Wang xiangsheng、Li decang,The first discovery of haemaphysalis conicinna.

1〕 杨银书,王祥生,李德昌。安徽省首次发现嗜群血蜱。

Chapter Three: Type classification of DE structure in Sino-Tibetan languages.

第三章汉藏语&的&字结构的类型划分。