甲胺

N-（3-Amino-4-methoxyphenyl）acetamide is an important intermediate for the production of azo disperse dyes,while it is still produced by reduction with iron powder in industry currently.

摘 要： N-（3-氨基-4-甲氧基苯基）乙酰胺是生产偶氮型分散染料的一类重要中间体。现有的工业生产方法仍全部采用铁粉还原。

Electron-withdrawing groups (F, CF 3 ) decreased the efficiency of the transformation, which has as byproducts benzonitrile and phenethyl N -acetamide.

电子集团撤回(六，比照3)转换效率降低，而作为副产品和苯氮苯甲-乙酰胺。

A novel Pd／C catalyst with high activity,high selectivity and good stability developed by our group was used for the hydrogenation of N-（3-nitro-4-methoxyphenyl）acetamide into N-（3-amino-4-methoxyphenyl）acetamide in methanol and water,respectively.

笔者开发了一种高效的Pd／C催化剂，分别选用甲醇和水作为反应溶剂，实现了高活性、高选择性和高稳定性地催化加氢制备N-（3-氨基-4-甲氧基苯基）乙酰胺。

Two compounds were isolated from ethyl acetate extract of the fermentation of fungus 07-11,which obtained from the soil of Yunnan Province. They were identified as N-(4-hydroxy-2-methoxyphenyl)acetamide (1) and ergosta-7,22-diene-3,6-dione (2) respectively on the basis of spectral analyses and physical and chemical identifications.

从云南土壤真菌07-11号菌株的发酵液乙酸乙酯萃取物中分离得到2个化合物，通过理化鉴别和光谱测定，鉴定两化合物分别为N-(4-羟基-2-甲氧苯基)乙酰胺(1)和麦角甾7，22-二烯-3，6-二酮(2)。

The effect of content of water on the yield of 2-phenylbenzamide by using sodium amide to cleave fluorenone was studied.

研究了水分含量对氨基化钠裂解芴酮制备2-苯基苯甲酰胺收率的影响。

When the effect ofNTP was examined after depletion of monoamines in the spinalcord by intrathecal neurotoxins, the antiallodynic and antihyperalgesiceffects were still observed after serotonergic denervation,but not after noradrenergic denervation.

鞘内给予神经毒素耗竭脊髓单胺递质后检查 NTP 的作用时，去除5羟色胺能神经支配后 NTP 的抗触觉性痛感和抗痛觉过敏作用仍然存在，但是去除去甲肾上腺素能神经支配后则消失。

In this research, liposoluble chlorogenic laurate was synthesized by the acylation with lauroy chloride in the existence of alkali catalyst in non-water phase, and yellowish CGL powders with a yield of 81.24% were obtained under the optimal synthesis conditions determined via single-factor tests and orthogonal experiments, that is, carrying out the acylation at 35℃ for 8h with a n:n: n ratio of 1:1:1.5 and with dimethylformamide as the solvating agent and the thinner.

文中对绿原酸进行了改性，即在碱性催化剂催化的条件下使其与月桂酰氯进行非水相的酯化反应，得到了脂溶性的绿原酸月桂酸酯。经过单因素及正交试验，确定了最佳合成条件为：以N，N-二甲基甲酰胺作为溶解、稀释剂，绿原酸／月桂酰氯／三乙胺的摩尔比为1：1：1.5，温度控制在35℃，反应时间8h。

A method is described for simultaneous analysis of simazine, atrazine, acetochlor, alachlor, prometryne, pyridaben, quizalofop-ethyl residue in strawberry using gas chromatography-mass spectrometry.

建立了气相色谱-质谱法，选择离子技术对草莓中乙草胺、西玛津、哒螨酮、禾草克、阿特拉津、扑草净、甲草胺多残留进行同时检测的方法。

Moreover, the protein-free spreading-free spreading technique, involvingbenzyldimethyl-alkyammonium bromide and the denaturing agent formamide, wasestablished. With very low DNA concentration, the fully extended DNA samples for linearDNA can be prepared.

采用Sephadex色谱柱分离，保温稀释的DNA溶液，不仅可除去DNA链上吸附的盐，而且可使盘绕一起的DNA链部分展开；在此基础上，通过采用苯二甲基辛基溴化胺－甲酰胺微量展层技术，可使纳克级DNA完全展开到云母基底上。

Results: The level of homocysteine was progressively increased in control group, and decreased after treatment with cyanocobalamin and methylcobalamin.

结果：对照组血清tHcy治疗后继续升高；氰钴胺组和甲钴胺组血清tHcy治疗后均下降。

Do you know, i need you to come back

你知道吗，我需要你回来

Yang yinshu、Wang xiangsheng、Li decang,The first discovery of haemaphysalis conicinna.

1〕 杨银书，王祥生，李德昌。安徽省首次发现嗜群血蜱。