甲胺

Starting from the hydroxylamine (dimethyl amino ethanol, triethanolamine) and 1, 3-propane sultone, a series of hydroxyl and sulfonyl dual-functionalized zwitterionic salts were synthesized. Then dual-functionalized ionic liquids containing both hydroxyl and sulfonyl functional groups were produced successfully by zwitterionic salts and three kinds of strong acids (p-toluene sulfonic acid, trifluoromethanesulfonic acid, methanesulfonic acid) respectively. The structure of zwitterionic salts and dual-functional ionic liquids were confirmed by the 1H NMR and IR.

以羟基有机胺(N，N-二甲基乙醇胺，三乙醇胺)为原料与1，3-磺酸内酯反应合成了一系列含有羟基和磺酸基双官能团的内盐，并将所得到的内盐分别与三种强酸(对甲苯磺酸，三氟磺酸，甲磺酸)反应，成功地合成了双功能化室温离子液体，并通过红外光谱、核磁氢谱测定，证实了内盐和双功能化离子液体的结构。

And 5-hydroxytryptamine (5-HT) in rat nucleus accumbens and ventral tegmental area.

高效液相色谱-电化学法测定大鼠伏隔核及腹侧被盖区内去甲肾上腺素、多巴胺和5羟色胺(5HT)的含量。

A new tripodal aryl amide type ligand,1,1,1-tris{[(2′-benzylaminoformyl)phenoxyl]methyl}-p-toluene sulfonyl aminomethane,and its Eu(NO_3)_3,Tb(NO_3)_3 complexes have been synthesized.

合成了一个新的三足芳香酰胺型有机配体1，1，1-三[(2′-甲酰苄胺苯氧)甲基]对甲苯磺酰氨基甲烷，及其Eu(NO3)3和Tb(NO3)3的配合物，并通过元素分析、红外光谱、核磁共振氢谱和摩尔电导率进行了表征。

The clenbuterol and ractopamine of specimen was extracted by 0.5% tungstenic acid: methanol (80:20). It was then purified by Oasis MCX. The mobile phase was 4 mmol/L ammonium acetate: acetonitrile (80:20). PDA detector was used for separation and detection.

采用0.5%钨酸：甲醉(80：20)提取试样中的盐酸克伦特罗和莱克多巴胺，用Oasis MCX小柱净化，4mmol/L乙酸胺溶液：乙腈(80：20)为流动相，用PDA检测器分离测定。

Results:The rats occurred rotational behavior to ipsilateral side of intranigral FeCl3 injection; the DA level of FeCl3 and FeCl2 injection side reduced significantly (P＜0.01), the A, NA and 5-HT were uneffected.

结果： 注射FeCl3的大鼠出现向损毁同侧的旋转行为；注射FeCl3和FeCl2侧黑质内多巴胺水平显著降低，去甲肾上腺素、肾上腺素和5-羟色胺水平不受影响。

They are insoluble in water, ethanol, methanol, acetone, chloroform and benzene, but soluble in DMA, DMF and DMSO.

它们溶于N，N-二甲基甲酰胺、N，N-二甲基乙酰胺和二甲基亚矾等溶剂，但不溶于水、乙醇、甲醇、丙酮、氯仿和苯。

Model compounds were synthesized from benzoyl chloride and diamine Ⅰ or diamine Ⅱ in NMP with anhydrous lithium chloride. Structures of model compounds were measured by melting point, FT-IR, element analysis and 〓H NMR. Reaction mechanism was from model reaction.

二胺Ⅰ和二胺Ⅱ分别与苯甲酰氯在含有LiCl的NMP溶液中合成模型化合物，采用熔点，FT-IR，元素分析，〓H NMR等方法对模型化合物的结构进行了表征，根据模型反应确定反应机理。

Seven biogenic amines were extracted from a sample with 6% perchloric acid, then derivatized with benzoyl chloride. 0.02 mol/L borate buffer (pH 9.2) containing 0.06 mol/L sodium deoxycholate-methanol （95∶5, v/v）was used as a running buffer. The detection wavelength was set at 214 nm. The separation was achieved within 12 min. Good linearities were observed from the calibration plots in the concentration ranges.

样品经6%过氯酸萃取后，由苯甲酰氯衍生化，以含0.06 mol/L脱氧胆酸钠的0.02 mol/L硼酸(pH 9.2)-甲醇(体积比为95∶5)混合液为电泳介质，电泳电压25 kV，温度25 ℃，检测波长214 nm，在12 min内实现了7种生物胺的完全分离。7种生物胺的浓度与其峰面积在一定的范围呈良好的线性关系，检出限除组胺为15 μg/g外，其余均为5 μg/g。

Thus if we control the reaction temperature at somesolvent we can obtain the products either by the reaction of phosphoryl-stabilizedcarbonanion with N-tosyl imines or by the reaction of methoxycarbonyl-stabilizedcarbanion with N-tosyl imines.

在一定溶剂中，如果控制反应的温度可以控制得到由膦酰基稳定的碳负离子和亚胺反应或由甲氧羰基稳定的碳负离子和亚胺反应。

Compared the homogeneous enthalpic interaction coefficients of glycine in aqueous potassium chloride solutions with that in aqueous sodium chloride solutions and discussed different cations influence on the interaction of glycine in aqueous solutions. The dilution enthalpies of DMF in aqueous ethylene glycol, glycerol, glucose and sucrose solutions of various molalities have been determined using CSC4400 flow microcalorimetry at

本文选择N，N—二甲基甲酰胺为模型化合物，用流动量热法测定了298.15K下DMF在不同浓度的乙二醇、甘油、蔗糖和葡萄糖水溶液中的稀释焓，根据McMillan-Mayer理论，计算了其在不同溶剂组成下的同系焓相互作用系数，得到水溶液中多羟基化合物与酰胺的相互作用规律。

Do you know, i need you to come back

你知道吗，我需要你回来

Yang yinshu、Wang xiangsheng、Li decang,The first discovery of haemaphysalis conicinna.

1〕 杨银书，王祥生，李德昌。安徽省首次发现嗜群血蜱。