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A huge gap between reality and expectations, so that Del Nido Spanish league title for attribution without concern, he said at a news conference, he did not care who won the Spanish title: I do not care who won the Spanish Primera Liga ...

现实和期望的巨大差距，让德尔尼多对于西甲联赛的冠军归属毫不关心，他在一次新闻发布会上表示，他根本不在乎谁会夺得西甲冠军：我一点都不关心谁赢得西甲联赛。。。。

The study employed fenpropathrin to jeopardize pregnant rats modeling as the experimental object to observe and analyze the effective of fenpropathrin to the pregnant SD rat itself, the filial generation and the reproductive capability.

以甲氰菊酯染毒妊娠大鼠模型为实验对象，观察、分析甲氰菊酯对母体、妊娠及子代生长发育和生殖能力的影响，评估甲氰菊酯对免疫系统、神经系统及生殖系统的可能损害，并初步揭示其机理。

Patient of data of 1 case of illness, male, 46 years old, colonitis of sex of liver cirrhosis, ulcer, inputting armour yellow acid in process of fluid of inject of sodium chloride of handkerchief bead sanded star, the patient appeals to abdominal distension, follow the doctor's advice give drop of 20mg of rice of Fu a place of strategic importance to fight crock, into the discovery after crock the liquid becomes white instantly muddy, shut instantly adjust clip changes infusion implement, the patient did not appear harmful response. Sodium chloride of bead sand star applies to handkerchief of yellow acid of 2 discussion armour the infection that sensitive bacterium causes, apply to cholecystitis, bile duct abscess of phlogistic, liver, have the better effect that fight bacterium, in clinical in use very extensive.

我们在临床治疗过程中发现甲黄酸帕珠沙星氯化钠注射液和呋塞米注射液存在配伍禁忌，不能配伍使用。1病例资料患者，男，46岁，肝硬化、溃疡性结肠炎，在输入甲黄酸帕珠沙星氯化钠注射液过程中，患者诉腹胀，遵医嘱给予呋塞米20mg滴斗入壶，入壶后发现液体立即变成白色混浊，立即关闭调节夹更换输液器，患者未出现不良反应。2讨论甲黄酸帕珠沙星氯化钠适用于敏感细菌引起的感染，适用于胆囊炎、胆管炎、肝脓肿，具有较好的抗菌功能，在临床中使用非常广泛。

Results show that, by using thionyl chloride and N,N-dimethyl formamide as chlorinating reagent and dichloromethane as solvent and taking -15℃ as reaction temperature, Z-iomer crystals with pale white color and stable to temperature can be obtained with an overall yield of 70%.

以2-（2-氨基噻唑－4-基）－2-甲氧亚氨基乙酸为原料，经盐酸化、氯代等反应合成了Z-2-（2-氨基噻唑－4-基）－2-甲氧亚氨基乙酰氯盐酸盐；氯代时以用亚硫酰氯和N，N-二甲基甲酰胺的混合物代替五氯化磷作氯化剂，并考察了温度和溶剂对氯代产物中Z-异构体和E-异构体收率的影响。

A three-dimensional large pore zeolite Hβ is used in the benzoylation of anisole instead of the classical Lewis acid catalysts to synthesize the important fine chemical intermediate 4-methoxybenzophenone.

采用高硅铝比、热稳定性好的三维大孔Hβ沸石替代传统Lewis酸催化剂催化苯甲醚的苯甲酰化反应，合成了重要精细化工中间体4-甲氧基二苯甲酮，收率可达92%。

In order to explore the feature of Diarrhetic shellfish poisoningproduction and elucidate the complicate mechanism of DSP biosynthesis, production of DSP in different growth phases in Prorocentrum lima and under different nutrients conditions was investigated by ELISA.

为了解海洋底栖甲藻——利玛原甲藻的产毒特征，阐明腹泻性贝毒（Diarrhetic shellfish poisoning， DSP）复杂的生物合成机制，采用酶联免疫试剂盒，对利玛原甲藻不同生长期、不同营养盐条件下毒素生成情况进行了研究。

Serotonin (5-HT), its precursors tryptophan and 5-hydroxytryptophan (5-HTP), major metabolites 5-hydroxyindoleacetic acid (5-HIAA); and 3-methoxy-4- hydroxyphenylethylene glycol , homovanillic acid , the respective major metabolites of noradrenaline and dopamine were measured by a method of HPLC.

应用高效液相色谱法测定其中5—羟色胺（5-HT）系列代谢物：色氨酸、5-羟色胺酸（5-HTP）、5-HT、5-羟吲哚乙酸（5-HIAA）；多巴胺的主要代谢产物3-甲氧基-4-羟基苯乙酸；去甲肾上腺素的主要代谢产物3-甲氧基-4-羟基苯乙二醇等。

Amino-monomethoxypoly(ethy1ene glycol)(mPEG-NH2) was synthesized based on the principle of Gabriel synthesis.Monomethoxypoly(ethy1ene glycol) tosylate was prepared at first,and then reaction with potassium salt of phthalimide as nucleophile to produce the monomethoxypoly(ethy1ene glycol)phthalimide derivative.

摘 要：首先合成了单甲氧基聚乙二醇对甲苯磺酸酯，然后根据盖布瑞尔合成法原理，以邻苯二甲酰亚胺钾盐为亲核试剂与mPEG-OTs反应，生成单甲氧基聚乙二醇的邻苯二甲酰亚胺衍生物，mPEG-PI与水合肼反应肼解生成伯胺，合成了一端为氨基的单甲氧基聚乙二醇(mPEG-NH2)。

Methyl phenyl glyoxylate was prepared firstly by reaction of 2-methyl benzoyl chloride with NaCN. The reaction of 2-methyl phenyl glyoxylate with methanol gave the target product methyl 2-methyl phenyl glyoxylate. An improved 3 step synthetic method of methyl 2-methyl phenyl glyoxylate was studied. The optimization conditions were presented.

以2-甲基苯甲酸为原料，酰化后与氰化钠反应生成2-甲基苯甲酰腈，经甲酯化生成2-甲基苯甲酰甲酸甲酯，改进了三步合成2-甲基苯甲酰甲酸甲酯的方法，并对反应时间、反应温度等影响因素进行了优化，确定了合成反应中的最优化条件。

Synthesis and structural characterization of novel cycioplatinated complexes with 2-aryl imidazolines 2-arylimidazoline ligands 2a-2d were synthesized from benzoyl chloride or p-methoxybenzoyl chloride with aminoethanol or valinol and 2e was synthesized from 2-phenylimidazoline.

新型2-芳基咪唑啉环铂化合物的合成与结构表征以苯甲酰氯或4-甲氧基苯甲酰氯和氨基醇(2-氨基乙醇或外消旋的缬氨基醇)为原料，合成了四种2-芳基咪唑啉配体2a-2d，以2-苯基咪唑啉为原料合成了配体2e，其中2d为新化合物。

The split between the two groups can hardly be papered over.

这两个团体间的分歧难以掩饰。

This approach not only encourages a greater number of responses, but minimizes the likelihood of stale groupthink.

这种做法不仅鼓励了更多的反应，而且减少跟风的可能性。