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Three ways leads to the synthesis of fenclorin, one way discussed here has 3 steps. Stepl :benzonitrile using as raw material goes though dry hydrogen chloride and becomes a-imino phenylmethyl ether after meet carbinol.

解草啶的合成主要有三条路线,本文选取合成路线是以苯甲腈为原料,经三步反应而成:1、苯甲腈在干燥的氯化氢通入,与甲醇形成亚氨基苯甲醚,通入氨气后置换甲氧基得到苯基脒盐酸盐(收率76.18%)。2、苯基脒盐酸盐在碱性条件下与丙二酸二乙酯环合而得嘧啶醇(收率84.39%)。3、嘧啶醇在三氯氧磷中羟基被氯化得到产品解草啶(收率87.29%)。

It is that:(1) the related compounds in Metronidazole Buccal Tablets prepared by Chongqing Medical College can be tested by determining (321nm) the total peak area of the impurities;(2) The related compounds in Metronidazole Disodium Phosphate for Injection prepared by Chongqing Medical College can be test by determining (254nm) the total peak area of the impurities and the peak area of the largest impurity;(3) Ceftriaxone polymer in Ceftriaxone Sodium for Injection prepared by Chongqing Keru Pharmacy Co.

结果如下:①用HPLC一UV法,在321nm处检测,用归一化法计算,控制各杂质峰面积的和,可检查重庆医科大学的注射用甲硝吟磷酸二钠中的有关物质:②用HPLC一UV法,在254nm处检测,控制杂质峰面积的和及控制最大杂质峰面积,可对重庆科瑞制药股份有限公司的注射用头饱曲松钠中的有关物质实施控制;③用HPLC一Uv法,在254nm处检测,按外标法计算,可检查注射用头抱曲松钠中的聚合物;④用紫外分光光度法,在277nm波长处测定吸收度,按C6H9N303的吸收系数为377计算每片标示百分含量,可测定重庆医科大学的甲硝哇口颊片的含量均匀度;⑤用紫外分光光度法,在277run波长处分别测定释放溶液20min、50min和90min的吸收度,按甲硝哇(C6H剥303)的吸收系数为377计算释放度,可检查重庆医科大学的甲硝哇口颊片的释放度。

The biological activity tests show that some target compounds have a good activity as plant growth regulator, and N-5-(3-carboxy-1H-1,2,4-triazolyl)-N'-o- chlorophenylfonnyl urea, N-5-(3-carboxy-1H-1,2,4-triazolyl)-N'-o- bromophenylformyl urea, N-5-(3-carboxy-1H-1,2,4-triazolyl)-N'-p- methyl-phenyl formyl urea have excellent activity of auxin.

生测试验证明部分酰基脲类化合物具有良好的植物生长调节活性,其中N-5(3-羧基-1,2,4-三唑基)-N'-o-氯苯甲酰基脲、N-5-(3-羧基-1,2,4-三唑基)-N'-o-溴苯甲酰基脲和N-5-3-羧基-1, 2,4-三唑基)-N'-p(或m-甲基苯甲酰基脲具有优良的生长素活性。

And in the days of Saul they made war with the Haga***tes, who fell by their hand: and they dwelt in their tents throughout all the east land of Gilead.

5:10 扫罗年间,他们与夏甲人争战,夏甲人倒在他们手下,他们就在基列东边的全地,住在夏甲人的帐棚里。

The first hall is JinGangDian, which enriches and worships the door gods in the tradition of four guardians history, which are 1 Oriental Snake Heavenly King: dressed in white, wearing armor piercings and helmets, with knife in left hand and sheath in right hand; 2 southern Sword Heavenly King: dressed in green, wearing armor piercings and helmets, with sword in hand; 3 western Lute Heavenly King: dressed in red, wearing armor piercings and helmets, with sheath in left hand and cable in right hand; 4 northern Umbrella Heavenly King: dressed in gold, wearing golden armor piercings, with tower in left hand and three-fork Qian in right hand and three-night fork ghosts under the feet.

进入本院入口山门即有一尊高大的观音立像,丛远处即可看到,观音像处于一个广场之中,广场的中央是一个放生池,本着人性本善的佛学思想,人们可以将鱼龟等生物在池中放生,即符合禅宗的思想,又达到动物保护的的目的,经过放生池才是寺院的正式入口,里面是按照传统寺院布置的三大殿,均为硬山式砖木结构,第一殿为金刚殿,里面供奉的四大金刚使传统中的门神,四大天王为: 1)东方持国天王:身白色,穿甲戴胄,左手把刀,右手执鞘;2)南方增长天王:身青色,穿甲戴胄,持宝剑: 3)西方广目天王:身红色,穿甲戴胄,左手执鞘,右手把赤索; 4)北方多闻天王:身金色,金甲胄,左手执宝塔,右手执三叉乾,脚踏三夜叉鬼,佛教的四大天王汉化便形成中国罗汉堂中的"四大金刚",成为"风调雨顺"的化身: 1)持国天王魔礼寿:穿紫金龙花狐貂,职顺。

Objective To study the efficacies of quadruple regimens for thetreatment of peptic ulcer disease and eradication of Helicobacter pylori.Methods 102patients with Hp associated peptic ulcer were randomly divided into three groups,groupA(n=98)received sanjiuweitai-based quadruple regimen(Yangweishul.2g,bid+ranitidine150mg,bid+amoxicillin500mg,bid+metronidazole400mg,bid);group B(n=31)received colloidal bisˉmuth subcitrate110mg,bid+ranitidine150mg,bid+amoxicillin500mg,bid+metronidazole400mg,bid;groupC(n=23)received ranitidine150mg,bid+amoxicillin500mg,bid+metronidazole400mg,bid.Antibiotics were griven for two weeks,the other drugs were given for six weeks,the efficacies were determined by gastroendoscopy or 13 C—UBT.

目的 探讨四联疗法对消化性溃疡的治疗作用及根除幽门螺杆菌的效果方法将102例胃镜证实消化性溃疡者随机分为3组,A组48例给予养胃舒1.2g+雷尼替丁150mg+阿膜西林500mg+甲硝唑400mg,bid;B组31例给予铋剂220mg+雷尼替丁150mg+阿莫西林500mg+甲硝唑400mg,bid;对照组(C组,23例)给予雷尼替丁150mg+阿莫西林500mg+甲硝唑400mg,bid;以上药物除抗菌药物只服用2周外,其余药物服至6周末疗程结束,第7周复查胃镜和 13 C呼气试验。

Detailed analysis have been given for the ~(181)J induced early hypothyroid condition, of which overdosage may be the main cause, while individual sensitivity...

对产生甲低的原因进行了分析;认为早发甲低主要为剂量过大引起,个体敏感性也存在,晚发甲低可能是甲状腺自家免疫疾病的表现。

This thesis includes five parts as follows.1. The backgrounds and some relative concepts of this work are briefly introduced. The photochemistry of benzamides and compounds with thiourea functional group is also concisely reviewed.2. Total of fourteen benzamides with different substituted groups have been synthesized and structurally characterized. Better photoreaction time for that kind of compounds at given concentrations is confirmed by tracking its'UV spectrum and GC chromatogram. A representative dibenzophenone photoproduct has been determined by X-ray crystallography. The mechanisms of photoreaction of benzamide have been proposed.3. Total of seven N-chloro(phenylmethylenebenzenamines with different substituted groups and sixty-one thiourea derivatives have been synthesized and structurally characterized.

论文的主要内容如下:1、简要介绍本论文工作的研究背景,并对苯甲酰胺和具有硫脲官能团类化合物的光化学研究进展进行简要的总结。2、合成与表征了14个具有不同取代基的苯甲酰胺类化合物,利用紫外光谱和气相色谱确定了此类化合物较佳光照时间,测定了一个具有代表性光解产物的单晶结构,提出了苯甲酰胺类化合物的光反应机理。3、合成与表征了7个带有不同取代基的氯代苯甲酰亚胺中间体及61个硫脲衍生物,测定了两个具有代表性化合物的单晶结构。

A novel method for determination of benzoyl peroxide with spectrophotometry was developed. Inclusion ratio of β cyclodextrin to dibenzoy peroxide and benzoic acid is obtained with spectrophotometry.The mechanism of the inclusion was studied,too. The results showed that β-CD react with dibenzoyl peroxide to form a 1:1 or 2:1 host-guest complex, with the apparent formation constants of 5.0× 10~2and 2.5× 10~4 , respectively.β-CD reacts with benzoic acid to form a 1:1 host-guest complex with the apparent formation constant of 6.9 × 10~2 after the dibenzoyl peroxide was reduced by hydroxyl ammonium chloride.

建立了用β环糊精测定过氧化苯甲酰的分光光度法,并测定了β环糊精与过氧化苯甲酰和苯甲酸的包结比,随着β-CD浓度的增大,可与BPO分别形成1:1或2:1的包容络合物,包结常数分别为5.0×10~2和2.5×10~4,与苯甲酸形成1:1的包容络合物,包结常数为6.9×10~2;由于包结物的吸光度值比过氧化苯甲酰的吸光度值大大增加,建立了一种当β-CD存在下,在水溶液中测定过氧化苯甲酰的方法。

Many species of red tide plankton and cysts of dinoflagellate provide the species sources for the frequent occurrence of red tide, and the suitable hydrometeorological conditions, specific living habits of some dinoflagllates and high N/P ratio may be the main causes for the occurrence of dinoflagellate red tide in the sea area, and the eutrophication has less relation to the frequent occurrence of red tide in the sea area in spring.

多种甲藻赤潮生物以及甲藻孢囊的存在为赤潮的频繁发生提供了种源,适宜的水文气象条件、某些甲藻独特的生活习性以及高N/P比有可能是导致该海域甲藻赤潮爆发的主要原因,富营养化与该海域春季赤潮频繁发生的关系较小。

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The split between the two groups can hardly be papered over.

这两个团体间的分歧难以掩饰。

This approach not only encourages a greater number of responses, but minimizes the likelihood of stale groupthink.

这种做法不仅鼓励了更多的反应,而且减少跟风的可能性。

The new PS20 solar power tower collected sunlight through mirrors known as "heliostats" to produce steam that is converted into electricity by a turbine in Sanlucar la Mayor, Spain, Wednesday.

聚光:照片上是建在西班牙桑路卡拉马尤城的一座新型PS20塔式太阳能电站。被称为&日光反射装置&的镜子将太阳光反射到主塔,然后用聚集的热量产生蒸汽进而通过涡轮机转化为电力