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Methoxystilbene and 2-methoxy-4'-nitrostilbene were synthesized from benzyl chloride and nitrobenzyl chloride by the Wittig reaction, and used as intermediates for the synthesis of the final product fluorescent whitener FP4,4'-bis(2-methoxystyrylbiphenyl via reduction and diazotisation of the latter followed by reaction with the former in the presence of NaOH.

以氯化苄和对硝基氯苄为原料,经Wittig反应合成中间体:2-甲氧基-二苯乙烯和2-甲氧基-4'-硝基-二苯乙烯。后者经还原反应、重氮化反应后,在氢氧化钠存在下与前者反应生成最终产品荧光增白剂FP4,4'-双-2-(甲氧基苯乙烯基联苯。为该类荧光增白剂的合成开辟了一条新路线

We have not found any reports that o-toluidine and N,N-dimethylaniline can be used as antiknock. The electrochemical properties of aromatic amine are in line with its' antidetonating quality and actual application.

而实际上采用胺类化合物作抗爆剂时,一般使用N-甲基苯胺、苯胺、邻甲苯胺及间甲苯胺,尚未见到使用对甲苯胺和N,N-二甲基苯胺的报道。

Notes on the Chinese Flea Beetles of the Genus Acrocrypta Baly Coleoptera, Chrysomelidae, Alticinae

球须跳甲属的中国种类鞘翅目,叶甲科,跳甲亚科

The rice water weevil Lissorhoptrus oryzophilus Kuschel, belongs to Erirhininae (Coleoptera: Curculionidae), and it is a dangerous quarantinable pest of rice.

稻水象甲Lissorhoptrus oryzophilus Kuschel属节肢动物门,昆虫纲,鞘翅目,象甲科,象甲亚科,稻水象属,是一种危害巨大的检疫性水稻害虫。

Essential drugs for standard topical treatment drugs include metronidazole,azelaic acid, and sodium sulfacetamide-sulfur. second line drugs include dibenzoyl peroxide, benzoyl peroxide,clindamycin,calcineurin inhibitors,and permethrin.

局部治疗红斑痤疮的基本药物有:甲硝唑,壬二酸,复方硫磺制剂;二线药物包括:过氧化二苯甲酰,过氧苯甲酰,克林霉素,钙神经蛋白抑制剂以及扑灭司林等。

Hydroxy-5, 10-dihydrophenophosphazine 10-oxide (1) reacted with SOCl2, and then with MeONa in MeOH to give a methyl phosphinate (2) which can be converted to a dinitro compound 3 (62%) by nitration and the resulting dinitro compound 3 can further be converted to 2, 8-diamino-10-methoxy-5, 10-dihydrophenophosphazine 10-oxide (4, 71%) by hydrogenation over Pd/C (w = 0.05). And the effect of amount of Pd/C (w = 0.05) on the reduction was also studied.

10-羟基-5,10-二氢磷杂吖嗪-10-氧化物(1)经醯氯化、甲基化得到10-甲氧基-5, 10-二氢磷杂吖嗪-10-氧化物(2),2经硝化得到10-甲氧基-2,8-二硝基-5,10-二氢磷杂吖嗪-10-氧化物(3,62%)。3在Pd/C(w = 0.05)存在下,用氢气还原为2,8二氨基-10-甲氧基-5,10-二氢磷杂吖嗪-10-氧化物(4,71%),考察了Pd/C(w = 0.05)用量对氢化还原反应的影响。

At 25℃, eggs hatched after 3.69±0.25 days, the nymph had three instars, the 1st instar stage was 3~5 days, 2nd instar 3~5days, and 3rd instar 4~5 days; The prepupal stage lasted 8~14 days and the pupal stage lasted 10~15 days at 25℃.

2黑广肩步甲成虫人工饲料研究分别研制了9种成虫人工饲料,以此饲喂黑广肩步甲成虫,结果表明,饲料Ⅲ是室内饲养黑广肩步甲成虫的最佳饲料。

Methods of eating metronidazole along with 20% for part of burn is recommended to be used in treatment. Key words: Metronidazole; 20% of silver nitrate; Recurrent stomatologist RAU

笔者于临床上用甲硝唑(又名灭滴灵、甲硝哒唑、甲硝基羟乙唑)内服配合局部用20%硝酸银溶液点灼,治疗阿弗他性口炎128例进行跟踪观察,收到较理想的效果,而临床上未见有资料报道。

A liquid chromatography-mass spectrometrymethod for determination of 15 anabolic steroids(17β-TS, PG, 17β-NT, MTS, PTS, PN, PNT, DIA, BOL, TRE, STA, TRA, MED, NOG, MPA) in animal urines was established. After the treatment of enzyme hydrolysis, the sample was cleaned up by C18 solid-phase extraction cartridges. The elution was evaporated under nitrogen and redissolved by acetontrile-water(1:1, by volume).

采用液相色谱-电喷雾串联质谱仪(LC-ESIMS/MS),在多反应监测模式下建立了动物尿液中15种甾类同化激素(睾酮、孕酮、诺龙、甲基睾酮、丙酸睾酮、丙酸诺龙、苯丙酸诺龙、大力补、勃地龙、群勃龙、康力龙、醋酸群勃龙、甲炔诺酮、甲羟孕酮、醋酸甲羟孕酮)的快速确证测定方法。

Benzoyl chloride was treated with potassium selenocyanate in dichioromethane by using polyethylene glycal-400 as the solid-liquid phase transfer catalyst to yield the corresponding benzoyl isoselenocyanate. This intermediate did not need to be isolated and directly reacted with arylamines, affording the N-benzoyl-N'-arylselenoureas 2a~2p. These compounds were characterized by IR, 1H NMR spectra and elemental analysis and the single crystal structure of 2k has been confirmed by X-ray crystallographic analysis.

以PEG-400为固液相转移催化剂,通过苯甲酰氯与硒氰酸钾反应合成了中间体苯甲酰基异硒氰酸酯,该中间体不需分离,直接与芳胺反应,得到N-苯甲酰基-N'-芳基硒脲(2a~2p),这些化合物用1H NMR,IR及元素分析进行了表徵,并用X射线单晶衍射确定了化合物2k的单晶结构。

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The split between the two groups can hardly be papered over.

这两个团体间的分歧难以掩饰。

This approach not only encourages a greater number of responses, but minimizes the likelihood of stale groupthink.

这种做法不仅鼓励了更多的反应,而且减少跟风的可能性。

The new PS20 solar power tower collected sunlight through mirrors known as "heliostats" to produce steam that is converted into electricity by a turbine in Sanlucar la Mayor, Spain, Wednesday.

聚光:照片上是建在西班牙桑路卡拉马尤城的一座新型PS20塔式太阳能电站。被称为&日光反射装置&的镜子将太阳光反射到主塔,然后用聚集的热量产生蒸汽进而通过涡轮机转化为电力