甲的

In this paper,3-methoxy-5,6-diamino-2-nitropyridine was synthesized from 3,5-dichloropyridine by substitution,oxidation,nitration and ammoniation .

研究了以3-氯-5-甲氧基-2，6-二硝基吡啶为原料，通过甲氧化、硝化、氨化合成3-甲氧基-5，6-二氨基-2-硝基吡啶，该化合物的结构通过IR，1H NMR，MS和元素分析进行了表征，确认为目标化合物。

A Heavy Armourer combines the skills of chainmail maker, leatherworker and iron-smith to produce good suits of armour and helms.

重甲工坊汇集各种链甲工匠、皮甲工匠和铁匠，以便制作更为优质的盔甲。

RESULTS: Basilar artery, thoracic aorta and ventricular papillary muscle Resting tension of basilar artery was increased by DL but decreased by niof basilar artery and thoracic aorta induced by noradrenaline bitartrate and KCl can be relaxed by DL in a dose dependant manner, and the half-effective concentration was (6.69±3.12)×10-4,(3.41±1.52)×10-3mmol/L for basilar artery, and (1.49±0.59)×10-3,(2.91±0.99)×10-3 mmol/L for thoracic aorta, displaying stronger inhibition on the constriction of basilar artery induced by noradrenaline bitartrate than on the contraction induced by KCl.

重酒石酸去甲肾上腺素、KCl所致基底动脉及胸主动脉收缩，二氢石蒜碱使之呈剂量依赖性松弛，其半数有效浓度值：对基底动脉分别为(6.69±3.12)×10-，(3.41±1.52)×10-3 mmol/L；对胸主动脉分别为(1.49±0.59)×10-3，(2.91±0.99)×10-3 mmol/L。拮抗重酒石酸去甲肾上腺素所致基底动脉收缩作用明显强于KCl。尼莫地平对KCl所致收缩的抑制显著强于对重酒石酸去甲肾上腺素。

This exhibition consists of 19 beasts skin chain mail braided in stainless steel gaskets and 60 birds chain mails. Among them, the heaviest, a tiger armor, weighs over 200 pounds, and the smallest, a flying bird weighs less than 100 grams.

本次展览由19张用钢垫圈编结的兽皮锁子甲和60张飞鸟锁子甲组成，其中最大的虎皮甲重达200多斤，最小的飞鸟甲不足2两。

①postoperative pain after hemorrhoidectomy can be safely and effectively controlled by Acuepoint inject of lappaconitine hydrobromide ②Using the Ashi-points-injection of lappaconitine hydrobromide after hemorrhoidectomy can reduce the pain for a longtime ③Combined with Yaoshu-point-injection can enhance the anaesthetic effect at the day of surgery④The edema at anal margin can be reduced by using of Ashi-points-injection of lappaconitine hydrobromide

①穴位注射氢溴酸高乌甲素对痔术后镇痛是安全而有效的；②术毕时使用氢溴酸高乌甲素阿是穴注射具有术后长效镇痛作用；③联合使用氢溴酸高乌甲素腰俞穴注射可增强手术当天的镇痛效果；④氢溴酸高乌甲素穴位注射具有防止痔术后肛缘水肿的作用。

To study the bioactive components from water soluble extract of the Chinese eaglewood, various column chromatography of Chinese eaglewood led to the isolation of ten compounds. Their structures were elucidated as 2,3-bis(3-hydroxyphenyl)- propan-1-ol (1), [(2R,3R)-3-(4-amino-3,5-dimethoxyphenyl)oxiran-2-yl]methanol (2), 8-chloro-4'- methoxy-5,6,7,3'-tetrahydroxy-2-(2-phenethyl)-5,6,7,8-tetrahydrochromone (3), 4'-methoxy-5,6,7,3'-tetrahydroxy-2--5,6,7,8-tetrahydrochromone (4), the isomer of 4 (5), 4'-methoxy-5,6,7,8-tetrahydroxy-2-(3'-hydroxyphenethyl)-5,6,7,8- tetrahydrochromenone (6), 4'-methoxyisoagarotetrol (7), 6-hydroxy-2-(2-hydroxy-2- phenethyl)-chromone (8), 6-hydroxy-2-(2-phenethyl)-chromone (9), 6-hydroxy-2-(4'- hydroxy-2-phenethyl)-chromone (10), and Guaiacylacetone (11) by means of spectral analysis and comparison with references.

为了进一步发现沉香中具有生理活性的化学成分，本文对国产沉香的水溶性成分进行了研究，从中分离得到11个化合物，通过红外、紫外、质谱、核磁共振(1H-NMR， 13C-NMR， COSY， HSQC， HMBC， ROESY)波谱解析，分别鉴定为：2，3-二(3-羟基苯基)-丙-1-醇(1)，[(2R，3R)-3-(4-氨基-3，5-二甲氧苯基)-2-氧化烯基]甲醇(2)，8-氯-4'-甲氧基-5，6，7，3'-四羟基-2-(2-苯乙基)-5，6，7，8-四氢色原酮(3)，4'-甲氧基-5，6，7，3'-四羟基-2-(2-苯乙基)-5，6，7，8-四氢色原酮(4)，化合物3的差向异构体(5)，4'-甲氧基-5，6，7，8-四羟基-2-(3'-羟基-2-苯乙基)-5，6，7，8-四氢色原酮(6)，4'-甲氧基异沉香四醇(7)，6-羟基-2-(2-羟基-2-苯乙基)色原酮(8)，6-羟基-2-(2-苯乙基)色原酮(9)，6-羟基-2-(4'-羟基-2-苯乙基)色原酮(10)和Guaiacylacetone (11)。

The total synthese three natural compounds to explore enantioselective synthesis of flavanol: We use phloroglucin and 2, 4, 6-trihydroxyacetophone as starting materials to synthesis distenin in two ways; Resorcin was used to synthsis 2, 5-dimethoxymethoxyacetophone though 3 steps.

对黄烷醇化合物的立体选择性全合成进行了探索：以间苯三酚和2，4，6-三羟基苯乙酮为原料，尝试用两条路线对Distenin化合物进行了全合成研究；以对苯二酚为原料，经三步制得2，5-二甲氧甲氧基苯乙酮，与2，4，6-三甲氧甲氧基苯甲醛反应，经四步反应得到天然产物3，5，7，2′，5′-二五羟基黄烷关键中间体1-（2′，6′-二甲氧甲氧基苯）-3-（2&，4&，6-三甲氧甲氧基苯）丙烷-1R，2R-二醇83及其对映体84；简要介绍了EGCg类化合物的生物活性和研究概况。

Results In cases without complication , the NFC could not be observed within 3 days after operation ; While all the cases with veinous crisis , the NFC appeared within 12 hours. But the NFC did not appear in all cases with artery crisis.

结果断指再植术后顺利的病例，术后3 d 以后才能观察到2～5 条甲襞毛细血管襻出现，7 d 后甲襞毛细血管襻数量和襻内血流状况恢复到正常水平；术后出现静脉危象的病例，均于术后12 h 内观察到较多粗大、无有形物流动的甲襞毛细血管襻；动脉危象则始终不能观察到甲襞毛细血管襻。

Ms. Kaori Kimata will introduce and demonstrate the techniques of medical nail correction in Europe and Japanese nail care technology.

Ms。 Kaori Kimata 将会介绍及示范欧洲治疗嵌甲及日本的护甲技术，更会示范日本最新的潮流甲花，让大家可在自己的美容、美甲店内应用。

Efficacy rates for metoclopramide 10 mg, metoclopramide 20 mg, and metoclopramide-erythromycin were 55%, 62%, and 79%, respectively (P or =.03). Metoclopramide failure occurred in 54% of patients with TBI compared to 35% of patients without TBI, respectively (P or =.02), due to a greater prevalence of tachyphylaxis.

甲氧氯普胺10mg，甲氧氯普胺20mg和甲氧氯普胺—红霉素联合应用的有效率分别为55%，62%和79%（P.03）。54%的合并TBI患者和35%不合并TBI患者由于快速耐受使用甲氧氯普胺无效（P.02）。

Neither the killing of Mr Zarqawi nor any breakthrough on the political front will stop the insurgency and the fratricidal murders in their tracks.

在对危险的南部地区访问时，他斥责什叶派民兵领导人对中央集权的挑衅行为。

In fact,I've got him on the satellite mobile right now.

实际上 我们已接通卫星可视电话了