甲烷

Uses the Boehm titrate and the XPS experiment method, to the coal tar and the methane around responded coked the superficial structure to carry on the determination.

采用Boehm滴定和XPS实验的方法，对煤焦与甲烷反应前后煤焦表面的结构进行了测定。

A two dimensional photofragment ion-velocity imaging technique coupled with a (2＋1) resonance-enhanced multiphoton ionization scheme was utilized to obtain the angular and translational energy distributions of the nascent Br(2 P 3/2) and Br*(2 P 1/2) atoms.

实验中得到了二溴甲烷光解产生的Br*(2 P 1/2)和Br(2 P 3/2)在不同波长下的角度和平动能分布。

A two dimensional photofragment ion-velocity imaging technique coupled with a (2+1) resonance-enhanced multiphoton ionization scheme was utilized to obtain the angular and translational energy distributions of the nascent Br2P(subscript 3/2 and Br(superscript *)2P(subscript 1/2 atoms.

实验中得到了二溴甲烷光解产生的Br2P(下标 1-2和Br2P(下标 3-2在不同波长下的角度和平动能分布。

As the dichloro methane are mainly used for isododecane, flushing agent and the original material of triacetate fiber rubber sheet.

由于二氯甲烷具有不可燃性和极强渗透性以及易挥发性等优良性能，被誉为多功能超强溶剂的代表。

Four non-ionic europium complexes,〓-phen(11),〓·bipy(12),〓·dia(13) and 〓(14)(TTA=2-thenoyltrifluoroacetone, DBM=dibenzoylmethane, phen=phenanthroline, bipy=2,2'-bipyridine, dia=4,5- diazafluoren-9-one, dmbp=4,4'-dimethyl-2,2,-bipyridine), were synthesised and the triboluminescent phenomena of 12, 13 and 14 were firstly observed. Structure determinations of 11,12 and 14 were carried out. The triboluminescence maxima of 12 and 13 are similar to those of their photoluminescence. X-Ray structure analyses show that Eu atoms all exhibit eight-coordinate tetragonal antiprismatic geometries and complexes 11, 12 and 14 are all centrosymmetric.

二、合成了四个非离子型的铕的配合物：〓、〓、和〓(14)[HTTA=2-噻吩三氟甲酰丙酮，DBM=二苯甲酰基甲烷，phen=邻菲罗啉， bipy=2，2'-联吡啶，dia=4，5-二氮杂芴-9-酮，dmbp=4，4'-二甲基-2，2'-联吡啶]，首次报道了12、13及14的摩擦发光性质，测定了11、12及14的晶体结构，并系统地讨论了晶体结构和摩擦发光活性之间的关系。12及13的摩擦发光光谱的极大值均类似与其相应的光致发光光谱，表明它们有相同的激发态。

Treatment of N-p-tolylsulfonylindole 1 with acetyl chloride in dried dichloromethane gave the title compound, N-p-tolylsulfonyl-3-acetyl-indole 2 C17H15NO3S, M(subscript r=313.36 in 89% yield. Single-crystal structure of 2 was determined by X-ray crystallography.2 crystallizes in the triclinic system, space group P-1 with a=10.0264(13), b=12.5913(16), c=14.1621(18)?

N-对－甲苯磺酰－吲哚(1)在二氯甲烷中与乙酰基氯反应得到产率为89%的N-对－甲苯磺酰－3-乙酰基－吲哚(2)（分子式：C17H15NO3S，分子量：313.36），用单晶X-射线衍射方法测定了2的晶体结构并表明：属三斜晶系，空间群为P-1，单胞参数为a=10.0264(13)，b=12.5913(16)，c=14.1621(18)？

SiO〓 crystal transformation was improved by adding Na〓SO〓, alpha cristobalite but not tridymite was catalytic active support. C〓 selectivity was improved by adding W and P, and suppressed deep oxidation property of SiO〓. W-O in catalyst surface was not active species. The support combined with S, W, P show low activity and high C〓 selectivity.

Na〓SO〓的加入促进了SiO〓晶型的转化，α-方石英是催化活性载体成分，而鳞石英没有甲烷氧化偶联反应活性。W和P的加入改善了C〓烃的选择性，抑制了SiO〓的深度氧化特性；W-O物种不是催化活性物种；由S、W、P及SiO〓组成的载体反应活性较差，但选择性较好；同时S元素对C〓烃的选择性的贡献有限。

The different hexanedichloromethane volumn ratio effection on molecular weight of,molecular weight distribution and weight percent of lowmolecule of polyisobutene by boron trifluoride initiator was studied in this paper by IR and UV.

研究了正己烷—二氯甲烷溶剂配比对BF3引发体系的聚异丁烯分子量及分子量分布、低分子物含量的影响，给出了BF3引发体系聚异丁烯及AlCl3引发体系聚异丁烯的红外光谱及紫外光谱。

The crosslinked PEG-20M glass capillary column was prepared by dynamic coating method with boron trifluoride as catalyst,3-glvcidyl-oxypropyl-trimethoxysilane as crosslinking agent.

以PEG－20M为固定相，三氟化硼为催化剂，3－缩甘油氧丙基三甲氧基硅烷（简称KH－560）为交联剂，二氯甲烷为溶剂，对预先用氯化钠沉积法粗糙化的玻璃毛细管柱进行动态涂渍。

The optimum conditions and the influence factors were investigated, and the composition of ion-association complexes and the reaction mechanism were also discussed. The effects of foreign substances were tested and it is shown that the method has a good selectivity. Based on HgCl2 and basic triphenylmethane dye, the sensitive, simple and rapid method for the determination of trace CTRX was developed.

研究了适宜的反应条件和影响因素，对离子缔合物的组成和离子缔合反应机理进行了探讨，考察了共存物质的影响，表明方法有良好的选择性，据此发展了用HgCl2和碱性三苯甲烷类染料的灵敏、简便、快速测定痕量头孢噻肟钠的新方法。

According to the clear water experiment, aeration performance of the new equipment is good with high total oxygen transfer coefficient and oxygen utilization ratio.

曝气设备的动力效率在叶轮转速为120rpm～150rpm时取得最大值，此时氧利用率和充氧能力也具有较高值。

The environmental stability of that world - including its crushing pressures and icy darkness - means that some of its most famous inhabitants have survived for eons as evolutionary throwbacks, their bodies undergoing little change.

稳定的海底环境─包括能把人压扁的压力和冰冷的黑暗─意谓海底某些最知名的栖居生物已以演化返祖的样态活了万世，形体几无变化。