甲基溴

The mass concentrations of sodium hydroxide,cetyltrimethyl ammonium bromide,sodium citrate and glycerin in the aqueous stripper are 90～100 g·L-1,10 g·L-1,10 g·L-1 and 10 g·L-1,respectively.

该脱漆剂以氢氧化钠水溶液为主体系，其中氢氧化钠的质量浓度为90~100 g.L-1，溴化十六烷基三甲基胺的质量浓度为10 g.L-1，柠檬酸钠的质量浓度10 g.L-1，甘油的质量浓度为

It is imaginable that the catalytic system could be used in cross-coupling of aryl bromides with other active methylene compounds.

预计该催化体系可以广泛用于溴代芳烃与其它含活泼亚甲基化合物的交叉偶联反应。

The improved method that calcium oxide and magnesium oxide in magnesite are determined by EDTA titrametric method

研究了新显色剂二溴对甲基偶氮磺与钙的反应，建立了直接测定镁砂中钙的光度分析方法。

A new chiral quaternary ammonium salt 1a was synthesized by the reaction of cinchonine and(2,4,6-)trimethyl benzyl chloride.Etherification between 1a and benzyl bromide,allyl chloride,or methyl give corresponding etherified quaternary ammonium salts 1b,1c,and 1d.

由辛可宁和2，4，6-三甲基苄氯，合成了一种新的手性季铵盐(1a)，并进一步用苄基溴、碘甲烷和烯丙基氯对分子中的羟基进行醚化，得到相转移催化剂1b、1c和1d。

New contributions of this work are as follows:(1). Preparation of Spherical MgCl_2-Supported Late-Transition Metal Catalysts for Ethylene PolymerizationFacile and effective immobilization of late-transition metal catalysts. 2,3-bis-(2,6-diisopropylphenyl) butane diimine nickel dibromide (1) and 2,6-bis-[1-(2,4,6-trimethylphenylimino)ethyl]pyridine iron dichloride (2), for ethylene polymerization has been achieved, using spherical MgCl_2 supports obtained by thermal dealcoholization of MgCl_2·2.56C_2H_5OH, and the effects of dealcoholization temperature on supported late-transition metal catalysts and the properties of resultant polymers were studied, the results indicated that:1.Supports with appropriate mechanical strength, high surface area and high porosity could be prepared by thermal dealcoholization of spherical MgCl_2·2.56C_2H_5OH supports; 2.BET, XRD, IR, SEM, GPC and DSC analyses indicate that the activities of the supported late-transition metal catalysts and the properties of resultant polymers are strongly dependent on the dealcoholization temperature.

本工作的新贡献如下：(1)、球形氯化镁负载后过渡金属催化荆催化乙烯聚合本文将配合物2，3-双(2，6-二异丙基苯亚胺)丁烷二溴化镍(1)和配合物2，6-二[1-(2，4，6-三甲基苯亚胺)乙基]吡啶二氯化铁(2)分别直接负载于经不同热脱醇温度处理的球形氯化镁载体上，研究了氯化镁载体的脱醇温度对负载化后过渡金属催化剂及其聚合物的影响，研究表明：1、通过对球形MgCl_2·2.56C_2H_5OH载体进行热脱醇处理，可以获得合适机械强度、较高比表面积和较高孔隙度的球形氯化镁载体；2、BET，XRD，IR，SEM，GPC和DSC研究表明，脱醇温度极大地影响负载后过渡金属催化剂的活性和聚合物的性能。

The phosphorus oxychloride or phosphorus tribromide N, N-dimethylformamide mix and react to form the Vilsmeier reagent used in the reaction. The newly prepared Vilsmeier reagent is added into the reaction bottle provided with the return condenser and the blender; a reaction raw material N, N-dimethylformamide solution expressed in the reaction formula is added into the system; the temperature is risen; the corresponding multi substituting pyridine-2 (1 H)-ketone compound can be made after the column chromatography of the silica gel; the production rate is between 60 and 95 percent according to different reactions.

由三氯氧磷或三溴化磷N，N-二甲基甲酰胺混合获得反应中所用Vilsmeier试剂；将新配制的Vilsmeier试剂加入装有回流冷凝管、搅拌器的反应瓶中，向体系中加入反应通式中表示的一种反应原料的N，N-二甲基甲酰胺溶液，升温，经硅胶柱层析分离得相应的多取代吡啶-2(1H)-酮类化合物，产率视不同反应在60~95％之间。

4 Kinds of methylthiazoline multithioether s were synthesized from the nucleophilic substitution of 5-methyl-thiazolidine-2-thione reacting with bromides,respectively.

通过5-甲基-2-噻唑烷硫酮与溴代物的亲核取代反应合成了四种甲基噻唑啉多头硫醚，利用红外光谱、核磁共振(1H NMR)光谱和元素分析对这四种化合物的结构进行了表征。

Wood packing materials fumigated with methyl bromide should be accompanied with an official certificate attesting to the treatment.

用溴甲烷熏蒸处理过的木质包装应附有官方证书证明进行了这种处理。假定重叠式的几何形是由一个甲基相对另一个甲基做刚体转动而得。

Employing CuI(5 mol%), N,N-dimethylglycine hydrochloride(10 mol%) and K_2CO_3(2 equiv.) in refluxing THF as the optimized reaction conditions,the four-membered 4-alkylidene-2-azatidinones could be efficiently synthesized.

当以3-溴-3-N-苯基-丁烯酰胺为底物，在5 mol%CuI为催化剂，10 mol%N，N-二甲基甘氨酸盐酸盐为配体，2当量K_2CO_3作碱，THF回流的反应条件下，可以高效的合成2-亚甲基-4-氮杂环丁酮类化合物。

M Trifluoromethylacetophenone was synthesized by the reaction of acetic anhydride with the Grignard reagent of 3 bromo benzene prepared from trifluoromethylbenzene , in 40% overall yield.

以三氟甲基苯为原料，经过溴化、格氏反应后与乙酸酐反应合成间三氟甲基苯乙酮，总收率40%。

They weren't aggressive, but I yelled and threw a rock in their direction to get them off the trail and away from me, just in case.

他们没有侵略性，但我大喊，并在他们的方向扔石头让他们过的线索，远离我，以防万一。

In slot 2 in your bag put wrapping paper, quantity does not matter in this case.

在你的书包里槽2把包装纸、数量无关紧要。