甲基溴

Two kinds of di aniline derivative s connected with oxamethylene bridge or azamethylene bridge were synthesizied by condensation of o nitrophenol and ethylene dibromide (1,4 dibromobutane)or 4 chloro 3,5 dinitrobenzotyifluoride and ethylene diamine(1,6 hexandiamine)and consequent reduction.

由邻硝基苯酚和二溴乙烷以及由4－氯－3， 5－二硝基三氟甲苯和乙二胺为原料通过桥接、还原合成两类由氧亚甲基或氮亚甲基桥联的双苯胺衍生物。

A series of the ligands including 6-bromo-piperonal dimethyl acetal, bis (9-fluorenyl) silane, and the dimer of indene have been synthesized and characterized.

合成了溴代胡椒醛二甲基缩醛基配体，合成了手性配体甲基苯基双芴基硅烷，合成了茚的二聚体，对其进行表征，培养单晶并测定了晶体结构。

In the synthesis process of ligands and their rare earth complexes, metal lithium is used to substitute for n-butyllithium, such as the synthesis of fluorenyl lithium, piperonal dimethyl acetal lithium, and bis (9-fluorenyl) silylene lithium.

合成配体和配合物的中间体均采用金属锂代替正丁基锂，如芴锂、溴代胡椒醛二甲基缩醛基锂盐、甲基苯基双芴基硅烷双锂盐的制备，方法简单，操作简便，副反应少，且锂盐的浓度和用量易于控制。

Under the protection of purified water-free, oxygen-free argon, using Schlenk technique, the rare rarth organometallic complexes containing piperonal dimethyl acetal and dicyclopentadienyl and involving silylene-bridged fluorenyl have been synthesized.

合成了含胡椒醛二甲基缩醛基和二茂基稀土金属有机配合物。采用Schlenk技术，在干燥纯氩气保护下进行。将溴代胡椒醛二甲基缩醛基锂盐与二茂基一氯稀土（Ln：Yb，Dy，Pr，La，Sm）反应，形成5个新的文献未曾报道的稀土金属有机配合物。

Methylmercury was extracted from the homogenized tissue with toluene in the presence of copper sulfate, sodium bromide and sulfuric acid

在存在硫酸铜、溴化钠和硫酸的情况下，用甲基从组织匀浆中萃取甲基汞。

In the derivatives of 2-(4-bromobenzyl-amino)-4-methyl-6-trifluoromethyl-1, 3, 5 triazine, the atoms of N(8), C (9) were the important active parts, it was considered to bind to the different amino acid residue at the D1 protein as traditional striazine herbicides.

对于2-（4-溴苄氨基）－4-甲基－6-三氟甲基－1，3，5-三氮苯中，N(8)和C(9)是重要的活性部位，和传统的均三氮苯类除草剂分子相比，与D1蛋白上不同的氨基酸残基发生了键合作用。

The results showed that the unsaturated fatty acid content of pecan kernel oil was 89 0%,and 13 kinds of unknown components such as nonadecaol,8 hexyl pentadecane,10 methyl eicosane,11,14 eicosadienoic acid,1 bromo 8 heptadecyne,9 hexyl heptadecane,tetracosane,13 docosenoic acid,1 bromo 7 nonadecyne,15 tetracosenoic acid,hexacosanoic acid,7 hexyl ei...

研究结果表明：山核桃仁油中的不饱和脂肪酸 w =89 0 %，未知成分是十九醇、8 己基十五烷、10 甲基二十烷、11，14 二十碳二烯酸、1溴 8 十七炔、9 己基十七烷、二十四烷、13 二十二碳烯酸、1 溴代 7 十九炔、15 二十四碳烯酸、二十六酸、7 己基二十烷、二十七烷共 13种，其中13 二十二碳烯酸、15 二十四碳烯酸、十九醇等具有较强的生理活性和药用价值

A process for preparingp-fluo-2-(2-methyl-3-propionyl)-4-oxy-N,3-diphenyl-phenylbutylamide includes such steps as Friedle-Craft acylating of newly prepared phenylacetyl chloride and fluorobenzene under catalysis of AlCl3 to obtain 4-fluoro-phenylbenzyl ketone, brominating at carbonyl alpha position under catalysis of less AlCl3 to obtain alpha-bromo-4-fluo-phenylbenzyl ketone, and condensing with isobutyryl acetanilide under action of sodium ethoxide.

本发明涉及一种制备对氟－2－(2－甲基－3－氧丙基)－4－氧－N，3－二苯基－苯丁酰胺(1)的方法，其包括以下步骤：新制的苯乙酰氯与氟苯在AlCl3催化下进行Friedle－Craft酰化反应，得到对4－氟－苯基苄基酮(4)；化合物(4)在少量AlCl3催化下进行羰基α位溴化，得到α－溴－4－氟－苯基苄基酮(5)；然后(3)异丁酰乙酰苯胺在乙醇钠作用下与化合物(5)进行缩合。

In our work, as a preliminary experiment, the N-phenacylisoquinolinium bromide was reacted with methlhydrazine in refluxed acetic acid. Unexpectedly, 2-methyl-1,2,3-triazole was obtained. The further study of this reaction led to a more simple starting material,α-bromoacetophenone to react with methylhydrazine, obtaining the same product.

我们在研究N-苯乙酰异喹啉溴化物与甲肼在冰醋酸中的反应时，意外地得到了2-甲基-4-苯基-1，2，3-三氮唑，经过进一步的研究发现α-溴代苯乙酮与甲肼也能得到同样的产物。

In the presence of the phase transfer catalysts such as tetramethylammonium bromide, tetraethylammonium bromide or polyethylene glycol(MW 400 and 6,000),lithium hydroxide is the best alkali among lithium hydroxide ,sodium hydroxide and potassium hydroxide.

研究表明在溴化四甲基铵、溴化四乙基铵、聚乙二醇（分子量为6，000）和聚乙二醇（分子量为400）相转移催化体系中，氢氧化锂最好，氢氧化钾次之，氢氧化钠最次。

And discuss some key point of integrated management system design, include hazard identification and risk assessment and risk control in the occupational health and safety management, the measure of satisfaction target of customer, the flawlessness of law system, the integration of the integrated management system and enterprise standardization system, unify lead institution and work orgnization, integreted internal audit and integrated management review.

同时，论述了一体化管理体系构建中的几个主要问题，包括职业健康安全管理中的危险源辨识、风险评价和风险控制、顾客满意度的科学监测、法律、法规体系的完善、一体化管理体系与企业标准化体系的有机结合、统一的领导机构和工作机构、一体化的内部审核和管理评审。

Deepwater Taranaki is investigated for its petroleum potential, using all available seismic data tied to shallow-water wells.

运用与浅水井相关的现有全部震波探测数据考察了深海区塔拉纳基盆地的油藏前景。