甲基溴

Main products: Ifosfamide,Ifosfamide acylate,2-Deoxy-D-Glucose,Vecuronium Bromide, Ceftiofur Hcl,Ceftiofur Sodium,Buflomedil Hcl,Oteracil Potassium,Gimeracil,Cinildipine

主要产品有：异环磷酰胺、异环磷酰胺酰化物、2-脱氧-D-葡萄糖、维库溴铵、头孢噻呋、头孢噻呋钠、氧嗪酸钾、吉莫斯特、西尼地平、马尼地平、培美曲塞、培美曲塞酸、培美曲塞二钠、尼索地平、消旋卡多曲、雷尼酸锶、盐酸丁咯地尔、1-(3-三氟甲基苯基)哌嗪、4-溴-2-甲基苯甲酸。

Main products: Ifosfamide,Ifosfamide acylate,2-Deoxy-D-Glucose,Vecuronium Bromide, Ceftiofur Hcl,Ceftiofur Sodium,Buflomedil Hcl,Oteracil Potassium,Gimeracil,Cinildipine, Manidipine dihydrochloride,Pemetrexed intermediate,Pemetrexed acid,Pemetrexed Disodium, Nisoldipine, Racecadotril, Strontium Ranelate, 1-(3-Trifluoromethylphenyl)piperazine hydrochloride, 4-Bromo-2-methylbenzoic acid.

主营业务：主要产品有：异环磷酰胺、异环磷酰胺酰化物、2-脱氧-D-葡萄糖、维库溴铵、盐酸头孢噻呋、头孢噻呋钠、氧嗪酸钾、吉莫斯特、西尼地平、盐酸马尼地平、培美曲塞、培美曲塞酸、培美曲塞二钠、尼索地平、消旋卡多曲、雷尼酸锶、盐酸丁咯地尔、1-(3-三氟甲基苯基)哌嗪盐酸盐、4-溴-2-甲基苯甲酸。

Waste minimization in ammonolysis process of O,O-dimethylphosphorochloridothioate;2. An Investigation on the Micelle-Catalytic Hydrolysis and Ammonolysis of Carboxylic Acid Esters;3. The final product is generated by ammonolysis of the compound under high pressure.

以4-溴-1，8-萘酐为原料，用2，4-二甲基苯胺在醋酸中与之反应得到N-2′，4′-二甲基苯基-4-溴-1，8-萘酰亚胺，然后将NDNA在高压下用氨水进行氨解得到最终产品。

In the precence of the base catalyst KF/Al2O3, the one - pot reaction of 2 -hydroxybenzaldehyde or 2 - hydroxynaphthaldehyde with ethyl α- bromoacetate,α-bromoacetophenone , 1,4 - dichloromethylbenzene , 4,4'- dichloromethylbiphenyl and 1,5 -dichloromethylnaphthalene gave the benzofuran compounds in 38-89% yield.

本文报道用 KF/Al_2O_3作为碱催化剂，由水杨醛或2-羟基-1-萘醛分别和α-溴代乙酸酯、α-溴代苯乙酮、苄基氯、4，4'-二氯甲基联苯和1，5-二氯甲基萘等进行一锅化缩合反应，以38～89％的产率合成了14种芳并呋喃化合物。

Methods Naloxone was synthesized starting from oxidation of thebaine, followed by hydrogenation, acylation, cyanidation, O-demethylation, hydrolyzation and N-allylation. The alternative method of O-demethylation, methane sulfonic acid/DL-methionine and hydrobromic acid were investigated.

在以蒂巴因为原料，经氧化、氢化、酰化、氰化、去氧甲基、水解、N-烯丙基化得到纳洛酮的合成路线中，分别采用甲磺酸／DL-甲硫氨酸和氢溴酸代替三溴化硼进行去氧甲基化和后续水解反应。

Study on an efficient process for the preparation of trifloxystrobin starting from 2-methylacetophenone bypartial oxidation,esterification,reaction with methoxyamine,bromization and condensation with 3'- acetophenone oxime.

以邻甲基苯乙酮为原料，经过高锰酸钾的碱性氧化，甲醇酯化，再与甲氧基胺盐酸盐肟化后，用N-溴丁二酰亚胺溴化，最后和间三氟甲基苯乙酮肟缩合得到目标产物肟菌酯。

Can also be methyl red - bromocresol green mixture (from 100 said bromocresol green solution in 100 ml 95 alcohol solution, and that 200 mg of methyl red dissolved in 100 ml 95thanol solution, Mixed with 3 1), the titration end changed from light blue

亦可采用甲基红---溴甲酚绿混合剂(称取100溴甲酚绿溶液于100ml 95乙醇溶液中，再称200mg甲基红溶于100ml 95乙醇溶液中，以3 1混合)，滴定终点由品月变

In order to investigate the mechanism for this reac-tion, methyl α-bromoacetate or ethyl α-bromoacetate as starting material was added to the solution of phenyl selenoamide in ethanol in 1∶1 or 2∶1 molar ratio under the neutral condition at room temperature. The results indicated that the same product bis or bis diselenide was formed. Byproduct ethyl benzoate was also separated.

为了研究该反应机理，选择α-溴代乙酸甲酯或α-溴代乙酸乙酯在无催化剂、中性条件下，乙醇溶液中与苯基硒代酰胺室温下反应，投料比为1∶1和2∶1，结果也都生成了同一类产物二甲氧羰基甲基二硒醚或二乙氧羰基甲基二硒醚，同时还分离得到了相应的副产物苯甲酸乙酯。

In order to investigate the mechanism for this reaction, methyl α-bromoacetate or ethyl α-bromoacetate as starting material was added to the solution of phenyl selenoamide in ethanol in 1:1 or 2:1 molar ratio under the neutral condition at room temperature. The results indicated that the same product bis or bis diselenide was formed. Byproduct ethyl benzoate was also separated.

为了研究该反应机理，选择α-溴代乙酸甲酯或α-溴代乙酸乙酯在无催化剂、中性条件下，乙醇溶液中与苯基硒代酰胺室温下反应，投料比为1：1和2：1，结果也都生成了同一类产物二甲氧羰基甲基二硒醚或二乙氧羰基甲基二硒醚，同时还分离得到了相应的副产物苯甲酸乙酯。

The alternative method of O-demethylation,methane sulfonic acid/DL-methionine and hydrobromic acid were investigated.

方法在以蒂巴因为原料，经氧化、氢化、酰化、氰化、去氧甲基、水解、N-烯丙基化得到纳洛酮的合成路线中，分别采用甲磺酸/DL-甲硫氨酸和氢溴酸代替三溴化硼进行去氧甲基化和后续水解反应。

And discuss some key point of integrated management system design, include hazard identification and risk assessment and risk control in the occupational health and safety management, the measure of satisfaction target of customer, the flawlessness of law system, the integration of the integrated management system and enterprise standardization system, unify lead institution and work orgnization, integreted internal audit and integrated management review.

同时，论述了一体化管理体系构建中的几个主要问题，包括职业健康安全管理中的危险源辨识、风险评价和风险控制、顾客满意度的科学监测、法律、法规体系的完善、一体化管理体系与企业标准化体系的有机结合、统一的领导机构和工作机构、一体化的内部审核和管理评审。

Deepwater Taranaki is investigated for its petroleum potential, using all available seismic data tied to shallow-water wells.

运用与浅水井相关的现有全部震波探测数据考察了深海区塔拉纳基盆地的油藏前景。