甲基化的

Goal compound synthesis namely: Take the vanillic acid as outset raw material, obtains 4- hydroxyl - 3- anisole methyl formate with the methyl alcohol reflux conditions, then after the etherification, the nitration, the return to original state, the ring closure response obtains 6- methoxy - 7- animal pen oxygen radical kui zuo lin - 4- alkone, then passes through the chlorination, the substitution aniline, to escape responses again and so on animal pen oxygen radical, etherification to obtain the goal compound; The goal compound and the diethylamine had the amine substitution reaction to obtain TM1, namely 4- benzene amino - 6- methoxy - 7- [2- hydroxyl - 3-(N, N- two ethyl aminos) third oxygen radical] kui zuo lin; Through zuo has the etherification with the Austria niter to respond obtains TM2, namely 4- benzene amino - 6- methoxy - 7- [2- hydroxyl - 3-(2- methyl - 5- nitryl imidazole) third oxygen radical] kui zuo lin.

目标化合物的合成即：以香草酸为起始原料，与甲醇回流条件下得到4-羟基-3-甲氧基苯甲酸甲酯，然后经过醚化、硝化、还原、环合反应得到6-甲氧基-7-苄氧基喹唑啉-4-酮，然后再经氯化、取代苯胺、脱苄氧基、醚化等反应得到目标化合物；目标化合物与二乙胺发生胺取代反应得到了TM1，即4-苯氨基-6-甲氧基-7-[2-羟基-3-丙氧基]喹唑啉；通过与奥硝唑发生醚化反应得到TM2，即4-苯氨基-6-甲氧基-7-[2-羟基-3-(2-甲基-5-硝基咪唑)丙氧基]喹唑啉。

Then esterification of 3, 7-dimethyl-2-pentadecanol with acetic anhydride, the active component of sex pheromone of pine sawfly, 3, 7-dimethyl2-pentadecanyl acetate was obtained in 83. 4％ yield.

最后，用乙酸酐对3，7-二甲基-2-十五碳醇进行酯化，得到松叶蜂性信息素的活性组分--3，7-二甲基-2-十五碳醇乙酸酯，收率为83.4％。

Methylmercury was extracted from the homogenized tissue with toluene in the presence of copper sulfate, sodium bromide and sulfuric acid

在存在硫酸铜、溴化钠和硫酸的情况下，用甲基从组织匀浆中萃取甲基汞。

Formyl-3-acetyl-4-methyl-5-carbobenzoxypyrrole (6) was synthesized via the selective oxidation of 2,4-dimethyl-3-acetyl-5-carbobenzoxypyrrole (5), which was produced from acetylacetic benzylester (1) via nitrosation, reduction and addition-cyclization with acetylacetone. The total yield of the product was about 34%.

以乙酰乙酸苄酯(1)为原料，经过亚硝化、还原、与乙酰丙酮加成环化生成2， 4-二甲基－3-乙酰基－5-苄氧羰基吡咯(5)，通过选择性氧化反应制得目标化合物2-甲酰基－3-乙酰基－4-甲基－5-苄氧羰基吡咯(6)，反应的总收率约为34%。

OBJECTIVE: To observe the biocompatibility and fibrovascular condition of methl-methacrylate modified PHEMA hydrogel orbital implant.

目的：观察通过甲基丙烯酸改性聚甲基丙烯酸β羟乙酯水凝胶义眼台的生物相容性和纤维血管化情况。

The technological conditions with methylacrylic acid and hexadecanol as raw-material and the synthesis of hexadecyl methylacrylate by direct-esterification are studied.

研究了以α-甲基丙烯酸和十六醇为原料采用直接酯化法合成α-甲基丙烯酸十六酯的工艺条件。

A method using α methylstyrene as raw material to prepare β methylene phenethyl alcohol,a new rose flavor ,by chlorination,esterification and saponification was studied.

对α 甲基苯乙烯经氯代、酯化、皂化合成新型玫瑰香料β亚甲基苯乙醇的方法进行了研究，选择PTC1作为相转移催化剂，当m∶m (NaAc·3H2 O)∶m (PTC1 )=1 。0 0 0∶0 30 0∶0 0 2 4时，80℃下反应 6h ，产率为 67 3%。

Mainly engaged in sodium azide, barium azide, three phosphorus nitride Friday, phenyl isothiocyanate, 1 - phenyl -5 - mercapto-tetrazole, 4 - dimethylamino-pyridine, 2 - mercapto--5 -- methyl-1,3,4 thiadiazole, N-hydroxy phthalimide, anhydrous betaine and betaine hydrochloride, such as fine chemical raw materials and medicine, pesticide intermediates of the development, production and sales.

主要从事叠氮化钠，叠氮化钡，五氮化三磷，异硫氰酸苯酯，1-苯基-5-巯基四氮唑，4-二甲氨基吡啶，2-巯基-5-甲基-1，3，4噻二唑，N-羟基邻苯二甲酰亚胺，无水甜菜碱及甜菜碱盐酸盐等精细化工原料及医药、农药中间体的开发、生产和销售。

The stavudine was prepared from 5-methyluridine via six steps in 34% overall yield, in which the key step is the selective acylation of 5-methyluridine by propionyl chloride.

该路线以5-甲基尿苷为起始原料，关键步骤是5-甲基尿苷和丙酰氯的选择性酰化反应，六步反应总收率为34%。

Mercaptopropyl methyldimethoxysilane was synthesized by thiourea in the presence of tetramethylammonium iodine as a catalyst and mixed liquid containing ethylenediamine and trichloroethylene as a neutralizer, without solvent, in which the reaction temperature, catalysts ,neutralizer and their amounts were optimized.

以四甲基碘化铵为催化剂，乙二胺和三氯乙烯的复合液为中和剂，在无溶剂体系中，用硫脲法合成了甲基巯丙基二甲氧基硅烷。

However, as the name（read－only memory）implies, CD disks cannot be written onorchanged in any way.

然而，正如其名字所指出的那样，CD盘不能写，也不能用任何方式改变其内容。

Galvanizes steel pallet is mainly export which suits standard packing of European Union, the North America. galvanizes steel pallet is suitable to heavy rack. Pallet surface can design plate type, corrugated and the gap form, satisfies the different requirements.

镀锌钢托盘多用于出口，替代木托盘，免薰蒸，符合欧盟、北美各国对出口货物包装材料的法令要求；喷涂钢托盘适用于重载上货架之用，托盘表面根据需要制作成平板状、波纹状及间隔形式，满足不同的使用要求。