甲基剂

The effect of components including tetracholrophthalic acid, phthalazine and antifoggant with tribromomethyl sulfone groups on photographic properties of FTG materials was investigated in different pH, using polyvinyl alcohol as a hydrophilic binder, in situ formed AgBr as light sensitive component.

本文以水性聚乙烯醇为粘合剂，原位法合成的AgBr作为光敏元，考察了组分四氯邻苯二甲酸、酞嗪以及三溴甲基砜类防灰雾剂在体系不同pH值时对PTG材料感光性能的影响。

The invention is characterized in that phthalide of general formula, wherein n and X have the meaning cited in the description, is reacted with nitrogen heterocycles of general formula: H-Z, wherein Z has the meaning cited in the description, or with nitrogen heterocycle metal salts of general formula in the presence of an aprotic polar diluent and optionally in the presence of a basic auxiliary reaction agent.

本发明涉及制备通式的2－杂环基甲基苯甲酸衍生物的新的方法，其中n、X和Z具有说明书中给出的意义，该方法提供高收率和高纯度，其特征是，通式的2－苯并呋喃酮，其中n和x具有说明书中给出的含义，与通式的氮杂环：H－Z，其中Z具有说明书中给出的意义，或与通式的氮杂环的金属盐在质子惰性极性稀释剂中并任选在碱性反应助剂存在下反应。

The synthetic route starts from penicillin G, peroxyacetic acid(8.5%) as Oxidizing Agent to get penicillin G sulfoxide; esterifided with p-nitrobenzyl bromine to synthesize penicillin G sulfoxide ester; we synthesize 3-exomethylenecepham sulfoxide ester with phthalimide potassium and 4A molecular sieve as acid scavenger to open the ring, SnCl_4 as catalyzation to close the ring. The yield is over 60%.

本研究采用的合成路线为：以青霉素G钾盐为原料，选用工业过氧化氢制备的过氧乙酸(22.3%)稀释至8.5%为氧化剂，氧化得青霉素亚砜；采用对硝基溴苄为酯化试剂，制备青霉素亚砜酯；以NCP(N-氯代邻苯二甲酰亚胺)为开环试剂，酞酰亚胺钾和4A型分子筛为酸清除剂，顺利开环；再经无水SnCl_4催化闭环得3-环外亚甲基头孢亚砜酯，最终产率在60%以上。

The electrolyte, which is different from the conventional electrolyte of the ethylene-boric acid system, consists of ethylene, dimethylformamide, ammonium hexandioic and polyhydric alcohol but water.

它是以乙二醇和二甲基甲酰胺为主溶剂，以己二酸铵为溶质，以多元醇为热稳定剂的非水系工作电解液。本文对新型工作电解液和一般工作电解液进行了比较。

The technique comprises the steps as follows: using the waste filtered mud of the sugar-refinery as the material to generate gas which is dehydrated till the water content is less than and equal to 30 percent and through distribution (clay used for of 70.00 to 85.0 percent, dehydrated filtered mud of the sugar-refinery of 15.0 to 30.0 percent, intensifier carboxymethyl cellulose or propyloic fibrin is 0.1 percent of the total dosage of the below material), performaing, moulding with high temperature (800 to 1200 DEG C, 20 to 180min) and acquiring the multi-hole porcelain granule with 20 to 30 percent of poriness, 10 to 20 percent of water absorbing capacity and 1.5 to 7.5/MPa of cylinder pressing intensity.

一种糖厂滤泥生产多孔陶粒技术，是用糖厂废弃物滤泥为发气原料，经脱水至含水≤30％，经配料(陶瓷用黏土70.0～85.0％，糖厂脱水滤泥15.0～30.0％，增强剂羧甲基纤维素或羧乙基纤维素为上述原料总量的0.1％)、制坯、高温(800~1200℃，20～180min)成型，得到孔隙率20~30％、吸水率10~20％、筒压强度1.5~7.5/MPa的多孔陶粒。

The influence of various factors, such as n NCO / n OH , the content of extender and dimethylol propionic acid on the synthesis of water borne polyurethane and its film performance was studied.

研究了 n NCO/n OH、扩链剂及二羟甲基丙酸的含量对水性聚氨酯合成及涂膜性能的影响，确定了较佳的配方。

In this paper,pyromellitic dianhydride,1,2,3,4-cyclobutanetetracarboxylic dianhydride,4[(4-aminophenyl)-bis(4-methoxyphenyl)methyl]benzeneamine,4-hexyloxy-biphenyl-3′,5′-diaminobenzoate,and additive ADD-34 were used to synthesize four PIs.

文章用均苯四甲酸二酐，4[(4-氨基苯基)-二(4-甲氧基苯基)甲基]苯胺，1，2，3，4-环丁烷四羧酸二酐，4-己烷氧基联苯酚-3′，5′-二胺基苯甲酸酯和不同含量的添加剂制备了聚酰亚胺液晶取向剂。

The magnetic polymer complex microspheres with core-shell structure were synthesized by copolymerizing of pyrrolidone acid and methacrylic on surface of Fe3O4 particles modified by OP, using potassium persulfate as a initiator.

以N-乙烯基吡咯烷酮和甲基丙烯酸为原料，过硫酸钾为引发剂，采用乳液聚合的方法共聚包埋自制的磁流体Fe3O4，制得了Fe3O4/P核壳复合微球。

The solid-liquid reaction method was used for the preparation of HPLC aryl-bonded silica gel stationary phases, including 3, 5-dinitrobenzyl, quinolinyl ether and 1, 1'-di(2-naphthol) ether bonded silica gel stationary phases by using N-(β-aminoethy1)-γ-aminopropylmethyldimethoxy silane and 3-glyci-doxypropyl trimethoxylsilane as coupling reagents, respectively.

采用固液相连续反应，以N-－γ-氨丙基甲基二甲氧基硅烷和γ-丙基三甲氧基硅烷为偶联剂，分别制备了二硝基苯甲酰胺基、喹啉醚基和联萘酚醚基三种芳基键合硅胶固定相。

When the resinic demulsifiers is are synthesized using solvent polymerization, it is found that the dosages of butyl acrylate, methacrylic acid and initiating agent in demulsifiers all exist optimum values; with the demulsifiers concentrations' increasing, the dehydration rate increases, however, it increases with the salinity's increasing.

评价溶液聚合方法合成的树脂型破乳剂的破乳效果，得出破乳剂组分中丙烯酸丁酯、甲基丙烯酸和引发剂用量都存在最佳值；脱水率随着破乳剂浓度的增大而增加；随矿化度的增大而增加。

I am accused of being overreligious," she said in her quiet, frank manner,"but that does not prevent me thinking the children very cruel who obstinately commit such suicide.""

客人们在卡罗利娜·埃凯家里，举止就文雅一些，因为卡罗利娜的母亲治家很严厉。

Designed by French fashion house Herm è s, this elegant uniform was manufactured in our home, Hong Kong, and was the first without a hat.

由著名品牌 Herm è s 设计，这件高贵的制服是香港本土制造，是我们第一套不配帽子的制服。