甲基剂

The best operational parameters were that the reaction temperature was 105℃, the reaction time was 3 hours, the mixture ratio of n: n=1:2.79, using N,N-dimethyl benzylamine as catalyst, and 2,6-Di-tert-buthyl-p-cresol as inhibitor.

结果表明，合成TGICA的最优化条件为：n/n=l：2.79；催化剂为N，N－二甲基苯胺；阻聚剂为2，6－二叔丁基对甲酚；反应温度(105±2)℃；反应时间3h。丙烯酸的转化率可达到99.7%。

The epoxidised cashew nut shell oil acrylate oligomer for UV curing materials was synthe- sized using epoxidised cashew nut shell oil and acrylic acid as main raw materials,N,N-dimethyl- benzylamine as catalyst and p-hydroxyanisole as inhibitor.

以N，N-二甲基苄胺作催化剂、对羟基苯甲醚作阻聚剂，环氧化腰果壳油和丙烯酸为主要原料合成了一种新型的紫外光固化预聚物——环氧化腰果壳油丙烯酸酯。

Furthermore, benzoic acid, p-toluic acid and p-phthalic acid were transformed slowly in sediment slurries amended with BESA (20 mM) under the condition of 100% CO2 and H2/CO2 (20/80), respectively, and the sediment slurry was dominated by methanogene bacteria.

在底泥含有甲烷菌抑制剂及上层气体分别为100% CO2和H2/CO2 (20ml/80ml)时，苯甲酸、对位甲基苯甲酸及对位苯二酸之分解变慢，且此底泥菌群是以甲烷菌为主要优势菌。

The asymmetric polymerization of methyl methacrylate is carried out using the chiral binaphthyl crown ether macrocyclic compounds binding n-BuLi or t-BuOK as chiral initiator at -78℃.

以手性联萘冠醚为配体，络合n-BuLi，t-BuOK等有机金属化合物形成手性引发剂体系，初步探讨了甲基丙烯酸甲酯单体的聚合反应。

The invention discloses a dielectric hole-microhole composite material and synthesizing method in the inorganic porous material, adsorbing material and catalytic material technical domain, which comprises the following steps: adopting zeolite molecular sieve as raw material; reacting with sodium bisilicate solution under 30-60 deg.c for 10-300 min; disintegrating particle part of zeolite molecular sieve into piece with microhole structure; adding cetyl trimethyl ammonium bromide as molder; adjusting pH value of mother liquid to 10-12; aging 1-8h; adding in the high-pressure autoclave to do water heat synthesizing reaction at 80-130 deg.c for 24-72h; separating solid; washing; drying; sintering under 500-600 deg.c for 5-10h; obtaining the Si-Al porous material with dielectric hole and microhole composite structure.

本发明属于无机多孔材料、吸附材料和催化材料技术领域，涉及具有介孔-微孔复合材料及其合成方法。其特征是以沸石分子筛为原料，用偏硅酸钠的水溶液在30～60℃反应10～300分钟，使沸石分子筛的颗粒部分解离形成具有微孔结构的碎片，加入模板剂十六烷基三甲基溴化铵，然后调节母液pH值为10～12，老化1～8小时，然后加入高压釜于80～130℃进行水热合成反应。反应24～72小时后，分离出固体，水洗、干燥，然后于500～600℃焙烧5～10小时，得到具有介孔和微孔复合结构的硅铝多孔材料。本发明的效果和益处是所发明的合成方法可用于合成多种沸石结构和介孔结构的复合材料，所合成的材料经过质子交换可以具有较强的酸性，在吸附和催化领域具有广泛应用前景。

A mixed indicator composed of bromocresol green, methyl red and phenalphthalein was used as indicator in titration of boron after the inteterience of cobalt was masked by EDTA.

采用甘露醇强化硼酸滴定硼时，以EDTA为掩蔽剂，可消除二价钴对硼分析的干扰；改用溴甲酚绿-甲基红-酚酞三元混合指示剂作为测定硼的指示剂，使滴定终点灵敏，准确。

Results: The best formulation of Picamilon sodium dispersible tablets was composed of Picamilon sodium 50mg, brushite 120mg, Ldisplace-hydroxypropyl cellulose and sodium carboxymethyl starch 16mg and 2% polyvidone k30 queous solution quantity sufficient.

结果：优化处方组成：主药匹卡米隆50mg、磷酸氢钙120mg、崩解剂羧甲基淀粉钠和低取代羟丙基纤维素分别为16mg，粘合剂2%聚维酮K30水溶液适量。

With cerous ammonium nitric-ethylene diamine tetraacetic acid as an initiator, and with the protection of the nitrogen the graft-copolymerization of methylacrylic acid and vinyl acetate on chitosan grafting was studied.

以硝酸铈铵－乙二胺四乙酸为引发剂，在N2气的保护下，研究了壳聚糖与甲基丙烯酸和醋酸乙烯酯两种单体的接技共聚反应。

Mesoporous molecular sieves were synthesized by using natural clay, sodium silicate and aluminum chloride as raw materials and cetyl trimethyl ammonium bromide as template agent at room temperature alkaline condition.

室温条件下以天然黏土、硅酸钠和氯化铝为原料，十六烷基三甲基溴化铵为模板剂合成介孔分子筛。

Using cetyl trimethyl ammoniunm bromide as templating agent, the mesoporous TiO_2 with special performance was synthesized by a tartaric acid sol-gel method. The UV irradiation was used in this process.

以十六烷基三甲基溴化胺为模板剂，采用溶胶-凝胶法，在溶胶-凝胶制备过程中引入紫外光照辐射，制备出具有一定特殊性能的中孔TiO2材料。

I am accused of being overreligious," she said in her quiet, frank manner,"but that does not prevent me thinking the children very cruel who obstinately commit such suicide.""

客人们在卡罗利娜·埃凯家里，举止就文雅一些，因为卡罗利娜的母亲治家很严厉。

Designed by French fashion house Herm è s, this elegant uniform was manufactured in our home, Hong Kong, and was the first without a hat.

由著名品牌 Herm è s 设计，这件高贵的制服是香港本土制造，是我们第一套不配帽子的制服。