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A series of UV-cured AB crosslinked polymers based on vinyl-terminated polyethylene adipate polyurethane and methyl methacrylate were prepared.

用紫外光聚合方法制备出一系列端乙烯基聚己二酸乙二醇酯聚氨酯和甲基丙烯酸甲酯AB交联聚合物。

A series of polyurethane anionomers were synthesized from isophorone diisocyanate, polyneopentanediol adipate and dimethanol propionic acid.

用异佛尔酮二异氰酸酯、聚己二酸新戊二醇酯和二羟甲基丙酸合成了负离子型聚氨酯离聚体。

Results: The disintegrating time of Yushi Weiweining concentrated pill was the shortest when the croscarmellose sodium was used for the disintegrating adminicle.

结果:以交联羧甲基纤维素钠的崩解时间最短,在用量为3%时,崩解时间为38min。

Cellulase activity in adventitious roots of maize during aerenchyma formation induced by flooding was located through Cellulase activity in adventitious roots of maize during aerenchyma formation induced by flooding was located through the reaction of Benedict's reagent with reducing sugars liberated by hydrolysis of carboxymethylcellulose.

采用本氏试剂与羟甲基纤维素水解还原糖反应的细胞化学方法,对玉米不定根淹水诱导形成通气组织过程中,逐步解体的皮层细胞内纤维素酶活性进行了定位观察。

Cellulase activity in adventitious roots of maize during aerenchyma formation induced by flooding was located through the reaction of Benedict's reagent with reducing sugars liberated by hydrolysis of carboxymethylcellulose.

采用本氏试剂与羟甲基纤维素水解还原糖反应的细胞化学方法,对玉米不定根淹水诱导形成通气组织过程中,逐步解体的皮层细胞内纤维素酶活性进行了定位观察。

Phase-transfer catalytic methylation was the best method, and suitable method of aftertreatment was essential.

相转移催化剂能有效控制反应在单甲基化阶段,且合适的后处理方法也能一定程度提高产品质量。

The kinds of compounds with AIE, AIEE and CIEE are summarized, mainly including siloles, substituted ethenes (mainly including fulvene and DPDSB style), CN-MBE, pyran, biphenyl compounds and polymers.

侧重总结了silole型、取代乙烯型(主要包括亚甲基环戊二烯型和DPDSB型)、腈取代二苯乙烯型、吡喃型、联苯型等小分子化合物和少数高分子的结构与AIE性质之间的关系,以及为解释AIE现象所提出的限制分子内的转动、避免非辐射去活、构象扭曲避免形成excimer、J-聚集态以及形成分子间的C-H/π键等理论。

But in the + moiety, the three benzimidazole rings shared the whole space equally, the dihedral angel among them is about 120°, just like three fan blades of an airscrew, the molecular structure appear gear-like shape.

X-射线单晶衍射测试、红外、紫外等方法确定了三(2-苯并咪唑亚甲基)胺的Fe和Co配合物的结构,由晶体结构发现金属配位情况不同、配合物在结构上存在着差异,Fe为八面体构型,而Co为三角双锥构型;其次,两配合物中的苯并咪唑环间夹角不同,配合物中包含N2和N4的两个苯并咪唑环间夹角仅为9.41(0.11),几乎构成一个平面,呈蝴蝶形;后者Co三个苯并咪唑环几乎平分了整个空间,它们之间的夹角约为120,呈三扇叶螺旋桨式构型,为齿轮形。

We investigated constituent of triterpenoid saponins ofAlbizzia, two new compounds together with two known compounds were isolated from Albizzia julibrissin Durazz. by using column chromatography (macroreticular resin, silica gel, Sephadex gel, reverse phase silica gel),preparative HPLC methods et al.On the basis of spectroscopic analysis, including IR,ESI-MS,~1H-NMR,~(13)C-NMR,HMBC,HMQC,~1H-~1HCOSY and chemical methods, the structure of two new compounds were identified as 3 - O -[β-D-xylopyranosyl(1→2)-β-D-fucopyranosyl (1→6)-β- D -2- deoxy - 2 - acetoamidoglucopyranosyl] -21-O-[(6S)-2- trans- 2,6-dimethyl - 6 - O-β- D - quinovopyranosyl -2,7- octadienoyl] - acacic acid- 28 - O-β-D-glucopyranosyl(1→3)[α-L-arabinofuranosyl(1→4)]-α-L-rhamnopyranosyl(1→2)-β-D-glucopyranoside acacic acid 3- O -β- D- glucopyranosy(1→3)-β- D- fucopyranosl(1→6) [β-D- xylopyranosyl (1→2)]-β-D-glucopyranoside ;two known compounds were acacic acid lactone 3- O -β-D- xylopyranosyl-(1→2)-β-D-fucopyranosl (1→6)- 2-deoxy -2 -acetoamido -β-D- glucopyranoside ; acacic acid lactone 3- O-β-D-xylopyranosyl(1→2)-α-L- arabinopyranosl (1→6)- 2- deoxy - 2- acetoamido -β-D-glucopyranoside . The study lays chemical foundation and chemical reference substance for enhancing quality standard of Albizzia julibrissin Durazz.

本研究论文在综述国内外对合欢属Albizzia三萜皂苷化学成分和药理作用研究进展的基础上,利用传统植化分离手段和现代分离技术,包括大孔树脂、硅胶、葡聚糖凝胶、反相硅胶等柱色谱,制备高效液相色谱法等技术从中药合欢皮中分离得到了4个化合物,其中,2个新化合物和2个己知化合物,并进一步通过现代分析技术IR,ESI-MS,~1H-NMR,~(13C-NMR,HMBC,HMQC,~1H-~1HCOSY等和化学方法鉴定了2个新化合物的结构分别是:3-O-[β-D-吡喃木糖基(1→2)-β-D-吡喃夫糖基(1→6)-β-D-2-去氧-2-乙酰氨基吡喃葡萄糖基]-21-O-[(6S)-2-反式-2,6-二甲基-6-O-β-D-吡喃鸡纳糖基-2,7-辛二烯酸基]-金合欢酸-28-O-α-L-呋喃阿拉伯糖基(1→4)[β-D-吡喃葡萄糖基(1→3)]-α-L-吡喃鼠李糖基(1→2)-β-D-吡喃葡萄糖苷,金合欢酸3-O-β-D-吡喃葡萄糖基(1→3)-β-D-吡喃夫糖基(1→6)[β-D-吡喃木糖基(1→2)]-β-D-吡喃葡萄糖苷;2个已知化合物结构分别是:金和欢酸内酯3-O-β-D-吡喃木糖基(1→2)-β-D-吡喃夫糖基(1→6)-β-D-2-去氧-2-乙酰氨基吡喃葡萄糖苷,金和欢酸内酯3-O-β-D-吡喃木糖基(1→2)-α-L-吡喃阿拉伯糖基(1→6)-β-D-2-去氧-2-乙酰氨基吡喃葡萄糖苷。

An organic compound in which the hydrogen of the hydroxyl group of methyl alcohol is replaced by a metal.

甲基化产物一种有机合成物,是甲醇的羟基中的氢被一种金属取代

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Now, however, all children continue in "comprehensive" schools, and the eleven-plus determines which courses of study the child will follow.

然而现在,所有的孩子都要在综合学校继续学习,所以这次考试只是决定他们将要学习哪些课程。

Cultivatable land , and led to a general recognition that development must not be carried at the cost of agriculture .

城区的迅速扩大在很多情况下侵占了宝贵的可耕地,使人们普遍认识到发展不能以牺牲农业为代价。

Detailed Intrinsic Reaction Coordination calculations were carried out to guarantee the optimized transition-state structures being connected to the related tautomers.

同时,做了详尽的内禀反应坐标计算,以保证所得到的过渡态连接相应的始末异构体。